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(R)-(-)-2-Methoxypropanol

Product Name
(R)-(-)-2-Methoxypropanol
CAS No.
6131-59-5
Chemical Name
(R)-(-)-2-Methoxypropanol
Synonyms
(R)-2-Methoxy-1-propanol;(R)-2-Methoxypropan-1-ol;(R)-(-)-2-Methoxypropanol;344(R)-(-)-2-Methoxypropanol;1-Propanol, 2-methoxy-, (2R)-
CBNumber
CB6853974
Molecular Formula
C4H10O2
Formula Weight
90.12
MOL File
6131-59-5.mol
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(R)-(-)-2-Methoxypropanol Property

Boiling point:
130.0±0.0 °C(Predicted)
Density 
0.912±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Store in freezer, under -20°C
pka
14.44±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H225Highly Flammable liquid and vapour

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P243Take precautionary measures against static discharge.

P273Avoid release to the environment.

P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CCH0008346
Product name
(R)-(-)-2-METHOXYPROPANOL
Purity
95.00%
Packaging
5MG
Price
$503.87
Updated
2021/12/16
Medical Isotopes, Inc.
Product number
35030
Product name
(R)-2-Methoxypropan-1-ol
Purity
95+%
Packaging
1g
Price
$1250
Updated
2021/12/16
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(R)-(-)-2-Methoxypropanol Chemical Properties,Usage,Production

Synthesis

23943-96-6

6131-59-5

General procedure for the synthesis of (R)-2-methoxy-1-propanol from (R)-2-methoxypropionic acid:[1239] 858 μL (8.39 mmol, 1.8 eq.) of borane/dimethyl sulfide complex was slowly added to a solution containing 500 mg (4.66 mmol) of (R)-(+)-2-methoxypropionic acid under argon protection and at 0 °C. The reaction mixture was stirred overnight at room temperature and then 2M aqueous sodium hydroxide solution was added dropwise. After completion of the reaction, phase separation was carried out and the aqueous phase was extracted with dichloromethane. The organic phases were combined, dried over sodium sulfate, filtered, concentrated under reduced pressure (water bath temperature controlled at 300 mbar) and finally dried to give the product. Yield: 490 mg (quantitative). [1240] 1H-NMR (400 MHz, DMSO-d6): δ [ppm] = 4.55 (t, 1H), 3.40-3.31 (m, 1H), 3.30-3.20 (m, 2H), 3.24 (s, 3H), 1.02 (d, 3H).

References

[1] Patent: US2016/52884, 2016, A1. Location in patent: Paragraph 1238-1240

(R)-(-)-2-Methoxypropanol Preparation Products And Raw materials

Raw materials

Preparation Products

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  • (R)-(-)-2-Methoxypropanol
  • 344(R)-(-)-2-Methoxypropanol
  • (R)-2-Methoxypropan-1-ol
  • 1-Propanol, 2-methoxy-, (2R)-
  • (R)-2-Methoxy-1-propanol
  • 6131-59-5