rac 4-Hydroxy Ephedrine Hydrochloride

ChemicalBook > CAS DataBase List > rac 4-Hydroxy Ephedrine Hydrochloride

rac 4-Hydroxy Ephedrine Hydrochloride

Product Name: rac 4-Hydroxy Ephedrine Hydrochloride
CAS No.: 365-26-4
Chemical Name: rac 4-Hydroxy Ephedrine Hydrochloride
Synonyms: Suprifen;Supriphen;Oxyephedrin;Oxyephedrine;MethylsyMpatol;4-Hydroxyephedrine;METHYLSYNEPHRINE(P);1-Hydroxypholedrine;(±)-Hydroxyephedrine;rac 4-Hydroxy Ephedrine
CBNumber: CB6889490
Molecular Formula: C10H15NO2
Formula Weight: 181.23
MOL File: 365-26-4.mol

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rac 4-Hydroxy Ephedrine Hydrochloride Property

Melting point:: 152-154°
Boiling point:: 314.35°C (rough estimate)
Density: 1.0918 (rough estimate)
refractive index: 1.5464 (estimate)
solubility: Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
form: Powder
pka: 9.97±0.26(Predicted)
InChI: InChI=1S/C10H15NO2/c1-7(11-2)10(13)8-3-5-9(12)6-4-8/h3-7,10-13H,1-2H3
InChIKey: OXFGTKPPFSCSMA-UHFFFAOYSA-N
SMILES: C1(=CC=C(O)C=C1)C(O)C(C)NC

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Usbiological

Product number: 300632
Product name: Methylsynephrine Hydrochloride
Packaging: 20mg
Price: $277
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: API0010553
Product name: 4-[1-HYDROXY-2-(METHYLAMINO)PROPYL]PHENOL
Purity: 95.00%
Packaging: 10MG
Price: $750.75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: API0010553
Product name: 4-[1-HYDROXY-2-(METHYLAMINO)PROPYL]PHENOL
Purity: 95.00%
Packaging: 100MG
Price: $1963.5
Updated: 2021/12/16

Arctom

Product number: CFN92450
Product name: MethylsynephrineHydrochloride
Packaging: 5mg
Price: $288
Updated: 2021/12/16

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rac 4-Hydroxy Ephedrine Hydrochloride Chemical Properties,Usage,Production

Originator

Carnigen, Aventis Pharma Deutschland

Manufacturing Process

The p-benzyloxypropiophenone used for the transformation is prepared by adding to a solution of 6.9 g of sodium in 230 ml of absolute alcohol 45.0 g of p-hydroxypropiophenone and 54.0 g of benzyl bromide, and boiling for 1 h in a reflux apparatus. The excess of alcohol is then distilled and the residue is extracted with ether and water. After drying it the ethereal solution is evaporated and the residue is recrystallized from alcohol of 95% strength. The yield amounts to 60.0 g. The p-benzyloxypropiophenone melts at 100°-101°C.
55.0 g of p-benzyloxypropiophenone are dissolved in 250 ml of methylene chloride and brominated with 38.0 g of bromine. As soon as all of the bromine has been introduced drop by drop, the methylene chloride solution is washed with caustic soda solution and water. The solvent is eliminated in a vacuum and the residue is dissolved in petroleum ether. The crystalline mass which soon separates is filtered by suction and washed with petroleum ether. When recrystallized from hexahydrobenzene the p-benzyloxybromopropiophenone melts at 80°C.
40.0 g of p-benzyloxybromopropiophenone are then transformed in an alcoholic solution with 30.0 g of methylbenzylamine. After the whole has been allowed to stand for 1 day, the excess of alcohol is distilled in a vacuum and the residue is dissolved with ether. By washing with water, the benzylmethylamine hydrobrornide then formed is eliminated and the ether is removed by evaporation. The ether residue soon begins to crystallize and the p-benzyloxymethylbenzylaminopropriophenone is obtained with a good yield; when recrystallized from petroleum ether of low boiling point it melts at 58°60°C.
15.0 g of p-benzyloxymethylbenzylaminopropriophenone are dissolved in alcohol and the solution is hydrogenated with palladium and hydrogen. As soon as the required quantity of hydrogen has been absorbed the palladium is filtered by suction and the alcohol is evaporated in a vacuum The residue is recrystallized and the p-hydroxyphenylmethylaminopropanol is obtained.

Therapeutic Function

Sympathomimetic, Analeptic

rac 4-Hydroxy Ephedrine Hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from rac 4-Hydroxy Ephedrine Hydrochloride manufacturers

Hong Kong Excellence Biotechnology Co., Ltd.

Product: Oxyephedrin 365-26-4
Price: US $100.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 20tons
Release date: 2023-10-12

Shanghai Aosiris new Material Technology Co., LTD

Product: rac 4-Hydroxy Ephedrine Hydrochloride 365-26-4
Price: US $3.00-1.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 10 tons
Release date: 2024-04-19

Sigma Audley

Product: Oxyephedrin 365-26-4
Price: US $25.00-10.00/kg
Min. Order: 1kg
Purity: 99.8%
Supply Ability: 200tons/year
Release date: 2024-02-22

365-26-4, rac 4-Hydroxy Ephedrine HydrochlorideRelated Search:

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365-26-4

7427-54-9