3-(METHOXYMETHYL)BENZOIC ACID

Product Name: 3-(METHOXYMETHYL)BENZOIC ACID
CAS No.: 32194-76-6
Chemical Name: 3-(METHOXYMETHYL)BENZOIC ACID
Synonyms: Benzoic acid, 3-(MethoxyMethyl)-;3-(methoxymethyl)benzoic acid(SALTDATA: FREE)
CBNumber: CB71490557
Molecular Formula: C9H10O3
Formula Weight: 166.17
MOL File: 32194-76-6.mol

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3-(METHOXYMETHYL)BENZOIC ACID Property

Melting point:: 64-66 °C
Boiling point:: 120-126 °C(Press: 0.1 Torr)
Density: 1.177±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 4.12±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HazardClass: IRRITANT
HS Code: 2918999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 3575AB
Product name: 3-(Methoxymethyl)benzoicacid
Packaging: 1g
Price: $334
Updated: 2021/12/16

Matrix Scientific

Product number: 053776
Product name: 3-(Methoxymethyl)benzoic acid
Packaging: 1g
Price: $350
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0085476
Product name: 3-(METHOXYMETHYL)BENZOIC ACID
Purity: 95.00%
Packaging: 1G
Price: $852.55
Updated: 2021/12/16

Matrix Scientific

Product number: 053776
Product name: 3-(Methoxymethyl)benzoic acid
Packaging: 5g
Price: $975
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0085476
Product name: 3-(METHOXYMETHYL)BENZOIC ACID
Purity: 95.00%
Packaging: 2.5G
Price: $1227.82
Updated: 2021/12/16

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3-(METHOXYMETHYL)BENZOIC ACID Chemical Properties,Usage,Production

Synthesis

124-41-4

1129-28-8

32194-76-6

a) Synthesis of 3-(methoxymethyl)benzoic acid: Sodium methanol (0.74 g, 13.8 mmol) was added to a solution of methyl 3-bromomethylbenzoate (1129-28-8, 1.05 g, 4.6 mmol) in anhydrous methanol (30 mL) under argon protection and room temperature. The resulting suspension was stirred and reacted at 50 °C for 2 h. Subsequently, 5 M aqueous potassium hydroxide solution was added and stirring was continued for 1.5 h at 50 °C. The reaction mixture was cooled to room temperature and the pH was adjusted to 2-3 with aqueous hydrochloric acid.The aqueous phase was extracted with ethyl acetate, the organic phases were combined and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to give the target product 3-(methoxymethyl)benzoic acid as a colorless oil (749 mg, 96% yield).LCMS analysis: retention time RtB = 2.47 min; [M + H]+ = 167.0.

References

[1] Patent: US2012/101110, 2012, A1. Location in patent: Page/Page column 70
[2] Patent: US2012/165331, 2012, A1. Location in patent: Page/Page column 27-28
[3] Patent: WO2012/101487, 2012, A1. Location in patent: Page/Page column 65; 66

3-(METHOXYMETHYL)BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(methoxymethyl)benzoic acid(SALTDATA: FREE)

Benzoic acid, 3-(MethoxyMethyl)-

32194-76-6