ChemicalBook > CAS DataBase List > 1-Diphenylmethylazetidine

1-Diphenylmethylazetidine

Product Name: 1-Diphenylmethylazetidine
CAS No.: 107128-00-7
Chemical Name: 1-Diphenylmethylazetidine
Synonyms: RMA-298;1-benzhydrylazetane;1-Benzhydrylazetidine;N-Benzhydrylazetidine;LABOTEST-BB LT00159241;N-(Diphenylmethyl)azetidine;1-(DIPHENYLMETHYL)AZETIDINE;1-(DiphenylMethyl)azetidine7.;Azetidine, 1-(diphenylmethyl)-;1-Diphenylmethylazetidine ISO 9001：2015 REACH
CBNumber: CB7184080
Molecular Formula: C16H17N
Formula Weight: 223.31
MOL File: 107128-00-7.mol

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1-Diphenylmethylazetidine Property

Melting point:: 109-112 °C (lit.)
Boiling point:: 307.7±11.0 °C(Predicted)
Density: 1.093±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 7.44±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 406031
Product name: 1-(Diphenylmethyl)azetidine
Purity: 98%
Packaging: 25g
Price: $182
Updated: 2023/06/20

TRC

Product number: B194850
Product name: 1-Benzhydrylazetidine
Packaging: 1g
Price: $130
Updated: 2021/12/16

AK Scientific

Product number: I813
Product name: 1-(Diphenylmethyl)azetidine
Packaging: 5g
Price: $123
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB18193
Product name: 1-Benzhydrylazetidine
Packaging: 500mg
Price: $125
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB18193
Product name: 1-Benzhydrylazetidine
Packaging: 1g
Price: $218.1
Updated: 2021/12/16

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1-Diphenylmethylazetidine Chemical Properties,Usage,Production

Uses

Azetidine derivatives as antiarrhythmic agents

Uses

1-(Diphenylmethyl)azetidine may be used in the preparation of monofunctional poly(tetrahydrofuran), (poly(THF)), having a 1-(diphenylmethyl)azetidinium end group.

Synthesis Reference(s)

Synthetic Communications, 18, p. 205, 1988 DOI: 10.1080/00397918808077346

General Description

1-(Diphenylmethyl)azetidine is a N-containing heterocyclic building block.

Synthesis

109-70-6

91-00-9

71-36-3

107128-00-7

Example 1 Synthesis of N-diphenylmethylazetidine: To a 7.5 liter aqueous solution containing 6.9 kg (50 moles) of potassium carbonate, 18.5 liters of n-butanol, 7.85 kg (50 moles) of 1-bromo-3-chloropropane, and 5.18 kg (25 moles, 97% purity, with 10% toluene as a residual solvent) of dibenzidine were sequentially added. The reaction mixture was heated to 100 °C with external steam under nitrogen protection and stirred slowly overnight. Upon completion of the reaction, about 12 liters of water were added to the mixture to dissolve the inorganic salt precipitate formed. The organic and aqueous layers were separated and about 18 liters of n-butanol and water were removed from the organic layer by distillation under reduced pressure. To the distillation residue 1.5 liters of methanol was added, slowly stirred and cooled to room temperature. The precipitated white solid was collected by filtration, washed twice with 700 mL of methanol and finally dried in a vacuum oven to give 4.2 kg (75% yield) of N-diphenylmethylazetidine with a melting point of 205°C (literature value: 107°-109°).

References

[1] Patent: US4870189, 1989, A

1-Diphenylmethylazetidine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-Diphenylmethylazetidine manufacturers

PNP Biotech Co. Ltd

Product: 1-benzhydrylazetane 107128-00-7
Price: US $0.00/KG
Min. Order: 25KG
Purity: 98%
Supply Ability: Inquiry
Release date: 2022-09-19

Henan Fengda Chemical Co., Ltd

Product: 1-Diphenylmethylazetidine 107128-00-7
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-26

107128-00-7, 1-DiphenylmethylazetidineRelated Search:

Azetidine TRIMETHYLENE OXIDE Hexamethyldisilazane 5-Methyl-1H-benzotriazole Toluene (-)-2-[METHYLAMINO]-1-PHENYLPROPANE 1-(Diphenylmethyl)-3-hydroxyazetidine 1-Benzhydrylazetidine-3-carboxylic acid 1-benzhydrylazetidin-3-Ol 1-Benzhydrylazetane-3-carbonitrile 3-Amino-1-diphenylmethylazetidine 1-BENZHYDRYLAZETIDIN-3-ONE Azelnidipine 1-(Diphenylmethyl)-3-azetidinyl methanesulfonate METHYL 1-(DIPHENYLMETHYL)AZETIDINE-3-CARBOXYLATE 1-BENZHYDRYLAZETAN-3-OL tert-Butyl 1-benzhydryl-3-azetidinylcarbamate 1-(DIPHENYLMETHYL)-3-AZETIDINONE HYDROCHLORIDE

LABOTEST-BB LT00159241

1-(DIPHENYLMETHYL)AZETIDINE

N-Benzhydrylazetidine

1-Benzhydrylazetidine

N-(Diphenylmethyl)azetidine

1-(DiphenylMethyl)azetidine7.

Azetidine, 1-(diphenylmethyl)-

1-Diphenylmethylazetidine ISO 9001：2015 REACH

1-benzhydrylazetane

RMA-298

107128-00-7

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