ChemicalBook > CAS DataBase List > 2-Amino-5-nitrobenzophenone
2-Amino-5-nitrobenzophenone
- Product Name
- 2-Amino-5-nitrobenzophenone
- CAS No.
- 1775-95-7
- Chemical Name
- 2-Amino-5-nitrobenzophenone
- Synonyms
- Ro 7-1999;Ro 7-19990;TIMTEC-BB SBB000821;IFLAB-BB F0266-0701;Nitrazepam Impurity 2;Nitrazepam Impurity B;Ciclopirox Impurity 6;LABOTEST-BB LT00000253;2-Benzoyl-4-nitroaniline;Nitrazepam EP Impurity B
- CBNumber
- CB7242568
- Molecular Formula
- C13H10N2O3
- Formula Weight
- 242.23
- MOL File
- 1775-95-7.mol
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2-Amino-5-nitrobenzophenone Property
- Melting point:
- 166-168 °C (lit.)
- Boiling point:
- 385.05°C (rough estimate)
- Density
- 1.2480 (rough estimate)
- refractive index
- 1.5300 (estimate)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly, Heated)
- form
- Solid
- pka
- -2.26±0.36(Predicted)
- color
- Beige
- Water Solubility
- 3 mg/L (20 C)
- InChI
- InChI=1S/C13H10N2O3/c14-12-7-6-10(15(17)18)8-11(12)13(16)9-4-2-1-3-5-9/h1-8H,14H2
- InChIKey
- PZPZDEIASIKHPY-UHFFFAOYSA-N
- SMILES
- C(C1=CC([N+]([O-])=O)=CC=C1N)(C1=CC=CC=C1)=O
- CAS DataBase Reference
- 1775-95-7(CAS DataBase Reference)
- NIST Chemistry Reference
- Methanone, (2-amino-5-nitrophenyl)phenyl-(1775-95-7)
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Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-20/21/22
- Safety Statements
- 26-37/39-36
- WGK Germany
- 3
- RTECS
- PC4935000
- HS Code
- 29223990
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 211737
- Product name
- 2-Amino-5-nitrobenzophenone
- Purity
- ≥98%
- Packaging
- 25g
- Price
- $39.83
- Updated
- 2025/07/31
Sigma-Aldrich
- Product number
- 211737
- Product name
- 2-Amino-5-nitrobenzophenone
- Purity
- ≥98%
- Packaging
- 100g
- Price
- $79
- Updated
- 2025/07/31
TCI Chemical
- Product number
- A1134
- Product name
- 2-Amino-5-nitrobenzophenone
- Purity
- >98.0%(HPLC)
- Packaging
- 25g
- Price
- $62
- Updated
- 2025/07/31
TRC
- Product number
- A618400
- Product name
- 2-Amino-5-nitrobenzophenone
- Packaging
- 10g
- Price
- $135
- Updated
- 2021/12/16
Usbiological
- Product number
- 002415
- Product name
- 5-Amino-2-nitrobenzophenone
- Packaging
- 2.5g
- Price
- $403
- Updated
- 2021/12/16
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2-Amino-5-nitrobenzophenone Chemical Properties,Usage,Production
Chemical Properties
Yellow Solid
Uses
2-Amino-5-nitrobenzophenone was used in the synthesis of [5-(4-nitrophenyl)-2-furyl]acrylic acid substituted benzophenone (anti-malarial agent).
Uses
A metabolite of Nitrazepam
Synthesis Reference(s)
Synthetic Communications, 16, p. 485, 1986 DOI: 10.1080/00397918608057727
General Description
FT-IR and Raman spectra of 2-amino-5-nitrobenzophenone (ANBP) has been reported.
Synthesis
17420-30-3
873-55-2
1775-95-7
2-Cyano-4-nitroaniline (0.3 mmol), sodium benzenesulfinate (0.6 mmol), palladium acetate (10 mol%), 2,2'-bipyridine (20 mol%), p-nitrobenzenesulfonic acid (10 equiv.), tetrahydrofuran (2 mL), and water (1 mL) were sequentially added to a Schlenk tube under the protection of nitrogen atmosphere. The reaction mixture was stirred vigorously at 80 °C for 48 hours. After completion of the reaction, the mixture was poured into ethyl acetate and washed sequentially with saturated sodium bicarbonate solution (2 x 10 mL) and saturated saline (1 x 10 mL). After the aqueous layer was extracted with ethyl acetate, all organic layers were combined and dried with anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure and the residue was purified by fast column chromatography (eluent: hexane/ethyl acetate) to afford the target product 2-amino-5-nitrobenzophenone.
References
[1] Molecules, 2014, vol. 19, # 5, p. 6439 - 6449
2-Amino-5-nitrobenzophenone Preparation Products And Raw materials
Raw materials
N-Methyl-4-nitroaniline
Zinc chloride
4-Chlorobenzoic acid
Benzophenone
Diphenylamine
Benzoyl chloride
Preparation Products
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View Lastest Price from 2-Amino-5-nitrobenzophenone manufacturers
Baoji Guokang Healthchem co.,ltd
- Product
- 2-Amino-5-nitrobenzophenone 1775-95-7
- Price
- US $127.10/g
- Min. Order
- 500g
- Purity
- 99%
- Supply Ability
- 5000g
- Release date
- 2021-06-08
Career Henan Chemical Co
- Product
- 2-Amino-5-nitrobenzophenone 1775-95-7
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2018-12-20
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