ChemicalBook > CAS DataBase List > 2-Iodo-4-methoxy-1-nitrobenzene

2-Iodo-4-methoxy-1-nitrobenzene

Product Name: 2-Iodo-4-methoxy-1-nitrobenzene
CAS No.: 214279-40-0
Chemical Name: 2-Iodo-4-methoxy-1-nitrobenzene
Synonyms: 3-Iodo-4-nitroanisol;4-NITRO-3-IODOANISOLE;3-IODO-4-NITROANISOLE;3-Iodo-4-nitroanisole,97%;2-iodine-4-methoxynitrobenzene;3-Iodo-4-nitroanisole, 97% 5GR;2-Iodo-4-Methoxy-1-nitrobenzene;Benzene, 2-iodo-4-methoxy-1-nitro-;2-iodo-4-methoxy-1-nitrobenzene 95%min(HPLC);2-Iodo-4-methoxy-1-nitrobenzene, 3-Iodo-4-nitrophenyl methyl ether
CBNumber: CB7397572
Molecular Formula: C7H6INO3
Formula Weight: 279.03
MOL File: 214279-40-0.mol

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2-Iodo-4-methoxy-1-nitrobenzene Property

Melting point:: 68-73 °C
Boiling point:: 352.1±27.0 °C(Predicted)
Density: 1.9259 (estimate)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: Crystals or Crystalline Powder
color: Yellow to orange-brown
InChI: InChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3
InChIKey: NLTAHTYBZZSCIT-UHFFFAOYSA-N
SMILES: C1([N+]([O-])=O)=CC=C(OC)C=C1I

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Safety

Hazard Codes: Xn
Risk Statements: 36-33-20/21/22
Safety Statements: 36/37-22
HS Code: 29093090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: ANV00227
Product name: 2-Iodo-4-methoxy-1-nitrobenzene
Purity: AldrichCPR
Packaging: 1G
Price: $107
Updated: 2025/07/31

TRC

Product number: B448863
Product name: 2-Iodo-4-methoxy-1-nitrobenzene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: B448863
Product name: 2-Iodo-4-methoxy-1-nitrobenzene
Packaging: 500mg
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-H-X6
Product name: 3-Iodo-4-nitroanisole
Purity: 98%
Packaging: 5G
Price: $60
Updated: 2021/12/16

Apolloscientific

Product number: OR13079
Product name: 3-Iodo-4-nitroanisole
Purity: 98%
Packaging: 1g
Price: $27
Updated: 2021/12/16

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2-Iodo-4-methoxy-1-nitrobenzene Chemical Properties,Usage,Production

Chemical Properties

yellow to orange-brown crystals or

Synthesis

Silak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent.

References

[1] Patent: CN107325002, 2017, A. Location in patent: Paragraph 0133
[2] Organic and Biomolecular Chemistry, 2018, vol. 16, # 30, p. 5416 - 5421
[3] Journal of Organic Chemistry, 2016, vol. 81, # 7, p. 2794 - 2803

2-Iodo-4-methoxy-1-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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214279-40-0, 2-Iodo-4-methoxy-1-nitrobenzeneRelated Search:

3-Iodoanisole 4-Nitroanisole 4-IODO-2-NITROANISOLE 2-Iodo-3-nitroanisole 2-IODO-4-NITROANISOLE 2-IODO-5-NITROANISOLE,2-IODO-5-NITROANISOLE 97% 4-IODO-3-NITROANISOLE,4-Iodo-3-Nitroanisole 3-Nitro-4-Iodoanisole,4-IODO-3-NITROANISOLE, 98+% 1-Iodo-2-nitrobenzene 3-IODO-4-NITROANISOLE 2-IODO-4-METHOXYPHENYLAMINE N-(2-IODOPHENYL)-HYDROXYLAMINE 5-IODO-6-NITRO-1,3-BENZODIOXOLE

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Aromatic Ethers