2-Iodo-4-methoxy-1-nitrobenzene Property

Melting point:

68-73 °C

Boiling point:

352.1±27.0 °C(Predicted)

Density 

1.9259 (estimate)

storage temp. 

Keep in dark place,Sealed in dry,Room Temperature

form 

Crystals or Crystalline Powder

color 

Yellow to orange-brown

InChI

InChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3

InChIKey

NLTAHTYBZZSCIT-UHFFFAOYSA-N

SMILES

C1([N+]([O-])=O)=CC=C(OC)C=C1I

Safety

Hazard Codes 

Xn

Risk Statements 

36-33-20/21/22

Safety Statements 

36/37-22

HS Code 

29093090

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

2-Iodo-4-methoxy-1-nitrobenzene Chemical Properties,Usage,Production

Chemical Properties

yellow to orange-brown crystals or

Synthesis

Silak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent.