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Phenyl chlorothionocarbonate

Product Name
Phenyl chlorothionocarbonate
CAS No.
1005-56-7
Chemical Name
Phenyl chlorothionocarbonate
Synonyms
O-Phenyl carbonochloridothioate;PHENYL CHLOROTHIONOFORMATE;O-PHENYL CHLOROTHIONOFORMATE;PHENYL THIONOCHLOROFORMATE;phenylcarbonochloridothioate;phenyl thioxochloroformate;Phenoxythiocarbonyl chloride;O-phenyl chloromethanethioate;NSC 99103;Phenoxythiocar
CBNumber
CB7480281
Molecular Formula
C7H5ClOS
Formula Weight
172.63
MOL File
1005-56-7.mol
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Phenyl chlorothionocarbonate Property

Melting point:
51 °C
Boiling point:
81-83 °C/6 mmHg (lit.)
Density 
1.248 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.581(lit.)
Flash point:
179 °F
storage temp. 
Inert atmosphere,2-8°C
solubility 
Chloroform, Ethyl Acetate
form 
Liquid
Specific Gravity
1.248
color 
Clear yellow
Water Solubility 
decomposes
Sensitive 
Moisture Sensitive
BRN 
774830
CAS DataBase Reference
1005-56-7(CAS DataBase Reference)
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Safety

Hazard Codes 
C
Risk Statements 
34
Safety Statements 
26-36/37/39-45
RIDADR 
UN 3265 8/PG 2
WGK Germany 
3
F 
10-21
HazardClass 
8
PackingGroup 
II
HS Code 
29309070
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
234524
Product name
O-Phenyl chlorothionoformate
Purity
99%
Packaging
5g
Price
$96.8
Updated
2024/03/01
Sigma-Aldrich
Product number
234524
Product name
O-Phenyl chlorothionoformate
Purity
99%
Packaging
1g
Price
$28.2
Updated
2023/06/20
TCI Chemical
Product number
P1236
Product name
Phenyl Chlorothionoformate
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$32
Updated
2024/03/01
TCI Chemical
Product number
P1236
Product name
Phenyl Chlorothionoformate
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$97
Updated
2024/03/01
Alfa Aesar
Product number
L00838
Product name
Phenyl chlorothionoformate, 98+%
Packaging
1g
Price
$28.65
Updated
2024/03/01
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Phenyl chlorothionocarbonate Chemical Properties,Usage,Production

Chemical Properties

CLEAR YELLOW LIQUID

Uses

O-Phenyl chlorothionoformate has been used in:

  • stereodirected synthesis of optically active, (?)-mintlactone
  • synthesis of peptide α-thioesters having a variety of C-terminal amino acids
  • synthesis of scyllo-inositol derivatives
  • thionocarbonylation of unprotected thymine nucleosides
  • preparation of phenoxythiocarbonyl esters of protected ribonucleosides

Uses

Phenyl Chlorothionoformate is used in the preparation of an bicyclic thymidine analogs as selective inhibitors of Thymidine monophosphate kinase Mycobacterium tuberculosis (TMPKmt).

Purification Methods

Purify it by dissolving in CHCl3, washing with H2O, drying (CaCl2), filtering, evaporating and distilling twice under a vacuum to give a clear yellow liquid. It is reactive and POISONOUS—work in a fume cupboard. Store it in sealed ampoules under N2. A possible impurity is O,O'-diphenyl thiocarbonate which has m 106o and remains behind in the distilling flask. [B.gemann et al. in Methoden Der Organischen Chemie (Houben-Weyl) 4th edn (E. Müller Ed.) Vol 9 Schwefel-Selen-Tellur Verbindungen pp. 807-808 1955, Rivier & Schalch Helv Chim Acta 6 612 1923, Kalson Chem Ber 20, 2384 1987, Rivier & Richard Helv Chim Acta 8 490 1925, Sch.nberg & Varga Justus Liebigs Ann Chem 483 176 1930, Sch.nberg & Vargha Chem Ber 64 1390 1931, Beilstein 6 III 609.]

Phenyl chlorothionocarbonate Preparation Products And Raw materials

Raw materials

Preparation Products

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Phenyl chlorothionocarbonate Suppliers

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View Lastest Price from Phenyl chlorothionocarbonate manufacturers

Career Henan Chemical Co
Product
Phenyl chlorothionocarbonate 1005-56-7
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
as request
Release date
2018-12-25

1005-56-7, Phenyl chlorothionocarbonateRelated Search:

Diphenyl ether Benzyl benzoate Benzyl chloroformate PHENYL ACETATE Phenyl chloroformate Dimethyl phthalate Thiobenzoic acid Phenyl butyrate Phenyl salicylate Phenyl dichlorophosphate Diisononyl phthalate PHENYL VALERATE 3-Chloroperoxybenzoic acid Triethyl phosphonoacetate Phenyl benzoate Phenyl bromoacetate PHENYL RESIN Potassium di-tert-butyl phosphate

  • phenylcarbonochloridothioate
  • Phenyl thiochloroformate.
  • Phenoxythiocarbonyl chloride
  • Phenyl chlorothionoformate, 98+%
  • Formic acid, chlorothio-, O-phenyl ester
  • O-Phenyl carbonochloridothioate
  • (Phenoxy)thioformyl chloride
  • Chloridothiocarbonic acid O-phenyl ester
  • Chloridothiocarbonic acid phenyl ester
  • Phenyl chlorothionocarbonate,99%
  • 2-Phenyl chlorothionoformate
  • Phenyl chlorothionocarbonate, 99% 5GR
  • NSC 99103
  • Phenoxythiocar
  • Chlorothioformic Acid O-Phenyl Ester Phenyl Thionochloroformate
  • O-Phenyl chlorothionoforMate 99%
  • Chlorothioformic Acid O-Phenyl Ester,Phenyl Thionochloroformate,Phenyl Chlorothionoformate Phenyl chlorothionocarbonate
  • O-Phenyl chlorothioformate for synthesis
  • Carbonochloridothioicacid,O-phenylester
  • O-PHENYL CHLOROTHIOCARBONATE
  • O-PHENYL CHLOROTHIOFORMATE
  • O-PHENYL CHLOROTHIONOFORMATE
  • PHENYL CHLOROTHIONOCARBONATE
  • PHENYL CHLOROTHIONOFORMATE
  • PHENYL CHLOROTHIOXOFORMATE
  • PHENYL THIONOCHLOROFORMATE
  • CHLOROTHIOFORMIC ACID O-PHENYL ESTER
  • CHLOROTHIOFORMIC ACID PHENYL ESTER
  • phenyl thioxochloroformate
  • HENYL CHLOROTHIONOCARBONATE
  • Phenylchlorothionocarbonate~Phenylthionochloroformate
  • PhenylChlorothionoformate&gt
  • orothionoformate
  • phenyl chloromethanethioate
  • O-Phenyl chlorotionoformate
  • O-phenyl chloromethanethioate
  • 1005-56-7
  • ClCSOC6H5
  • C7H5ClOS
  • Building Blocks
  • Thiocarbonyl Compounds
  • Sulfur Compounds
  • Organic Building Blocks
  • Sulfur Compounds (for Synthesis)
  • Building Blocks
  • Chemical Synthesis
  • Organic Building Blocks
  • Sulfur Compounds
  • Thiocarbonyl Compounds
  • Sulfur Compounds (for Synthesis)
  • Synthetic Organic Chemistry