3-BROMOPHENETHYLAMINE
- Product Name
- 3-BROMOPHENETHYLAMINE
- CAS No.
- 58971-11-2
- Chemical Name
- 3-BROMOPHENETHYLAMINE
- Synonyms
- 2-(3-BROMOPHENYL)ETHANAMINE;RARECHEM AL BW 0207;3-BROMOPHENETHYLAIME;3-BROMOPHENETHYLAMINE;3-Bromophenethanamine;3-broMophenylethanaMine;3-Bromobenzeneethylamine;3-Bromophenethylamine,99%;3-BROMOPHENETHYLAMINE 99%;3-BroMo-benzeneethanaMine
- CBNumber
- CB7703997
- Molecular Formula
- C8H10BrN
- Formula Weight
- 200.08
- MOL File
- 58971-11-2.mol
3-BROMOPHENETHYLAMINE Property
- Boiling point:
- 239-240 °C (lit.)
- Density
- 1.406 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.5740(lit.)
- Flash point:
- >230 °F
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- Liquid
- pka
- 9.83±0.10(Predicted)
- color
- Clear colorless to light yellow
Safety
- Hazard Codes
- C
- Risk Statements
- 34
- Safety Statements
- 26-27-36/37/39-45
- RIDADR
- UN 2735 8/PG 2
- WGK Germany
- 3
- HazardClass
- 8
- PackingGroup
- Ⅱ
- HS Code
- 29214200
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P363Wash contaminated clothing before reuse.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 534080
- Product name
- 3-Bromophenethylamine
- Purity
- 97%
- Packaging
- 5g
- Price
- $174
- Updated
- 2025/07/31
- Product number
- 534080
- Product name
- 3-Bromophenethylamine
- Purity
- 97%
- Packaging
- 10g
- Price
- $231
- Updated
- 2025/07/31
- Product number
- B3947
- Product name
- 2-(3-Bromophenyl)ethylamine
- Purity
- >95.0%(GC)(T)
- Packaging
- 5g
- Price
- $141
- Updated
- 2025/07/31
- Product number
- B700225
- Product name
- 2-(3-Bromophenyl)ethanamine
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- JK280863
- Product name
- 3-Bromophenethylamine
- Packaging
- 1g
- Price
- $51
- Updated
- 2021/12/16
3-BROMOPHENETHYLAMINE Chemical Properties,Usage,Production
Chemical Properties
clear colorless to light yellow liquid
Synthesis
31938-07-5
58971-11-2
General procedure for the synthesis of 3-bromophenethylamine from 3-bromocyanobenzyl: An anhydrous THF (100 mL) suspension of LiAlH4 (3.04 g, 80 mmol) was cooled to -5°C. Concentrated H2SO4 (3.9 g, 40 mmol) was added slowly dropwise and the resulting mixture was stirred for 1 h at -5°C. The reaction system was then brought to room temperature. Subsequently, a THF (5 mL) solution of 3-bromobenzeneacetonitrile (9.80 g, 50 mmol) was added slowly dropwise, and the reaction system was slowly warmed to room temperature after the dropwise addition. The reaction was continued to be stirred for 1 h at room temperature, then cooled to 0 °C and the reaction was quenched by addition of a 1:1 THF:H2O mixture (12.4 mL). Et2O (50 mL) was added, followed by 3.6 M NaOH solution (24.4 mL). The mixture was filtered through diatomaceous earth and the solids were washed well with additional Et2O. The organic phases were combined, dried over Na2SO4, filtered and concentrated in vacuum to give 3-bromophenethylamine (9.7 g, 97% yield). The crude product was used directly in the subsequent reaction.1H NMR (400 MHz, CDCl3) δ 7.38-7.30 (m, 2H), 7.20-7.10 (m, 2H), 2.96 (t, J = 7.2 Hz, 2H), 2.72 (t, J = 7.2 Hz, 2H), 1.35 (br s, 2H). m/z MS (ESI): calculated value: 199; measured value: 200/202 (M+-).
References
[1] Patent: WO2007/61458, 2007, A2. Location in patent: Page/Page column 44; 78
[2] Patent: WO2004/60882, 2004, A1. Location in patent: Page 29-30
[3] Patent: US2010/204214, 2010, A1. Location in patent: Page/Page column 109-110
[4] Patent: CN103880745, 2018, B. Location in patent: Paragraph 0019; 0020; 0021; 0030; 0039
[5] Patent: US2008/171754, 2008, A1. Location in patent: Page/Page column 101-102
3-BROMOPHENETHYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
3-BROMOPHENETHYLAMINE Suppliers
- Tel
- 320-37350700
- Fax
- +32 (0)37350701
- sales@tcieurope.eu
- Country
- Europe
- ProdList
- 23671
- Advantage
- 75
View Lastest Price from 3-BROMOPHENETHYLAMINE manufacturers
- Product
- 3-BROMOPHENETHYLAMINE 58971-11-2
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-26
- Product
- 3-BROMOPHENETHYLAMINE 58971-11-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-01-02