4-Fluoro-3-methoxybenzonitrile
- Product Name
- 4-Fluoro-3-methoxybenzonitrile
- CAS No.
- 243128-37-2
- Chemical Name
- 4-Fluoro-3-methoxybenzonitrile
- Synonyms
- BUTTPARK 22\01-64;5-Cyano-2-fluoroanisole;4-Fluoro-3-methoxybenzonitri;3-methoxy-fluorobenzonitrile;4-FLUORO-3-METHOXYBENZONITRILE;3-Methoxy-4-Fluorobenzonitrile;Benzonitrile, 4-fluoro-3-methoxy-;4-Fluoro-3-methoxybenzonitrile99%;4-Fluoro-3-methoxybenzonitrile 99%;Benzonitrile, 4-fluoro-3-methoxy- (9CI)
- CBNumber
- CB8132169
- Molecular Formula
- C8H6FNO
- Formula Weight
- 151.14
- MOL File
- 243128-37-2.mol
4-Fluoro-3-methoxybenzonitrile Property
- Melting point:
- 109 °C
- Boiling point:
- 96-98°C 1,5mm
- Density
- 1.18±0.1 g/cm3(Predicted)
- Flash point:
- 96-98°C/1.5mm
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Light yellow to Light orange
- BRN
- 2965042
- CAS DataBase Reference
- 243128-37-2(CAS DataBase Reference)
Safety
- Hazard Codes
- T,Xi,Xn
- Risk Statements
- 20/21/22-36/37/38-22
- Safety Statements
- 26-36/37/39-36/37-9
- RIDADR
- 3439
- Hazard Note
- Toxic
- HazardClass
- 6.1
- PackingGroup
- III
- HS Code
- 29269090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H331Toxic if inhaled
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- F0408
- Product name
- 4-Fluoro-3-methoxybenzonitrile
- Packaging
- 1g
- Price
- $24
- Updated
- 2025/07/31
- Product number
- F0408
- Product name
- 4-Fluoro-3-methoxybenzonitrile
- Packaging
- 5g
- Price
- $89
- Updated
- 2025/07/31
- Product number
- 002363
- Product name
- 4-Fluoro-3-methoxybenzonitrile
- Purity
- 99%
- Packaging
- 100g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- 4637-3-43
- Product name
- 4-Fluoro-3-methoxybenzonitrile
- Purity
- 99%
- Packaging
- 25g
- Price
- $95
- Updated
- 2021/12/16
- Product number
- 002363
- Product name
- 4-Fluoro-3-methoxybenzonitrile
- Purity
- 99%
- Packaging
- 25g
- Price
- $50
- Updated
- 2021/12/16
4-Fluoro-3-methoxybenzonitrile Chemical Properties,Usage,Production
Chemical Properties
White powder
Synthesis
946713-86-6
57-13-6
243128-37-2
Cu(TFA)2 (20 mmol) was added to a pressure-sealed tube containing 0.75 mL of DMSO with 4-fluoro-3-methoxyphenylacetic acid (0.5 mmol) and urea (1.5 mmol). The reaction system was oxygenated and stirred at 130 °C for about 20 h. The reaction process was monitored by TLC and GC (the exact reaction time was determined based on GC and TLC monitoring results). Upon completion of the reaction, the reaction was cooled to room temperature. To the reaction mixture, 20 mL of ethyl acetate was added and washed sequentially with NaHCO3 solution (20 mL x 2) and water. The organic phases were combined and dried over anhydrous sodium sulfate. The aqueous phase was then extracted with ethyl acetate (20 mL x 2) and all organic phases were combined. The solvent was removed by rotary evaporator to obtain the crude product. The crude product was purified by silica gel column chromatography with the eluent ratio of ethyl acetate:petroleum ether=50:1. 4-fluoro-3-methoxybenzonitrile was finally obtained in 84% yield.
References
[1] Patent: CN103772236, 2016, B. Location in patent: Paragraph 0021; 0022; 0023; 0054; 0055; 0056; 0057
4-Fluoro-3-methoxybenzonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
4-Fluoro-3-methoxybenzonitrile Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 847-367-3680
- Fax
- 847-367-3681
- sales@arkpharminc.com
- Country
- United States
- ProdList
- 1670
- Advantage
- 56
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 0311-89250318 031166536426
- Fax
- 4000311741
- master@sjzsdyn.com
- Country
- China
- ProdList
- 2806
- Advantage
- 65
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 010-010-82967028 13522913783
- Fax
- +86-10-82967029
- 2355560935@qq.com
- Country
- China
- ProdList
- 12000
- Advantage
- 60
- Tel
- 13817811078
- Fax
- 86-021-50426522,50426273
- sales@jingyan-chemical.com
- Country
- China
- ProdList
- 9976
- Advantage
- 60
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
View Lastest Price from 4-Fluoro-3-methoxybenzonitrile manufacturers
- Product
- 4-Fluoro-3-methoxybenzonitri 243128-37-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 10 tons
- Release date
- 2020-01-10