Diethyl 2,6-pyridinedicarboxylate
- Product Name
- Diethyl 2,6-pyridinedicarboxylate
- CAS No.
- 15658-60-3
- Chemical Name
- Diethyl 2,6-pyridinedicarboxylate
- Synonyms
- Nsc78907;RARECHEM AL BI 0203;DIETHYL DIPICOLINATE;pyridine-2,6-dicarboxyL;2,6-Dicarbethoxypyridine;DIPICOLINIC ACID DIETHYL ESTER;DIETHYL 2,6-PYRIDINEDICARBOXYLATE;diethyl pyridine-2,6-dicarboxylate;Diethyl pyridine-1,6-dicarboxylate;Diethyl2,6-Pyridinedicarboxylate>
- CBNumber
- CB8150484
- Molecular Formula
- C11H13NO4
- Formula Weight
- 223.23
- MOL File
- 15658-60-3.mol
Diethyl 2,6-pyridinedicarboxylate Property
- Melting point:
- 44°C
- Boiling point:
- 188 °C / 12mmHg
- Density
- 1.165±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- powder to crystal
- pka
- -0.20±0.10(Predicted)
- color
- White to Light yellow to Light orange
- CAS DataBase Reference
- 15658-60-3(CAS DataBase Reference)
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 29333990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- P1240
- Product name
- Diethyl 2,6-Pyridinedicarboxylate
- Purity
- min. 98.0 %
- Packaging
- 5G
- Price
- $78
- Updated
- 2024/03/01
- Product number
- P1240
- Product name
- Diethyl 2,6-Pyridinedicarboxylate
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $219
- Updated
- 2024/03/01
- Product number
- D444763
- Product name
- Diethyl 2,6-Pyridinedicarboxylate
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FD67424
- Product name
- Diethyl 2,6-pyridinedicarboxylate
- Packaging
- 25g
- Price
- $65
- Updated
- 2021/12/16
- Product number
- J98984
- Product name
- Diethylpyridine-2,6-dicarboxylate
- Packaging
- 25g
- Price
- $70
- Updated
- 2021/12/16
Diethyl 2,6-pyridinedicarboxylate Chemical Properties,Usage,Production
Chemical Properties
Yellow to red crystalline powder
Synthesis
Pyridine-2,6-dicarboxylic acid (10.0g, 59.9mmol) was added into ethanol (120mL),
then 3 drops of concentrated sulfuric acid were added. The mixture was heated to
reflux for 8 hours. After evaporation of the solvent, the solid residue was washed with
saturated Na2CO3 aqueous solution and extracted with chloroform for 3 times. The
organic phase was dried with small amount of MgSO4. The solvent was removed to
afford 1 as white powder (12.6g, 56.3mmol, yield = 94%). 1
H-NMR (400MHz,
CDCl3) |? ppm 8.29 (d, J = 7.80 Hz, 2H), 8.01 (t, J = 7.80, 7.80 Hz, 1H), 4.50 (q, J =
7.12, 7.12, 7.12 Hz, 2H), 1.47 (t, J = 7.13, 7.13 Hz, 3H). 13C-NMR (100 MHz, CDCl3)
|? ppm 164.6, 148.6, 138.2,127.8, 62.3,14.2,14.2. ESI MS: m/z = 224.1 [M+H]+
, 246.1
[M+Na]+
.
Diethyl 2,6-pyridinedicarboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
Diethyl 2,6-pyridinedicarboxylate Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
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- Advantage
- 75
View Lastest Price from Diethyl 2,6-pyridinedicarboxylate manufacturers
- Product
- Diethyl 2,6-pyridinedicarboxylate 15658-60-3
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-28
- Product
- Diethyl 2,6-pyridinedicarboxylate 15658-60-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-07-02