ChemicalBook > CAS DataBase List > Diethyl 2,6-pyridinedicarboxylate

Diethyl 2,6-pyridinedicarboxylate

Product Name
Diethyl 2,6-pyridinedicarboxylate
CAS No.
15658-60-3
Chemical Name
Diethyl 2,6-pyridinedicarboxylate
Synonyms
Nsc78907;RARECHEM AL BI 0203;DIETHYL DIPICOLINATE;pyridine-2,6-dicarboxyL;2,6-Dicarbethoxypyridine;DIPICOLINIC ACID DIETHYL ESTER;DIETHYL 2,6-PYRIDINEDICARBOXYLATE;diethyl pyridine-2,6-dicarboxylate;Diethyl pyridine-1,6-dicarboxylate;Diethyl2,6-Pyridinedicarboxylate>
CBNumber
CB8150484
Molecular Formula
C11H13NO4
Formula Weight
223.23
MOL File
15658-60-3.mol
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Diethyl 2,6-pyridinedicarboxylate Property

Melting point:
44°C
Boiling point:
188 °C / 12mmHg
Density 
1.165±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
form 
powder to crystal
pka
-0.20±0.10(Predicted)
color 
White to Light yellow to Light orange
CAS DataBase Reference
15658-60-3(CAS DataBase Reference)
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
P1240
Product name
Diethyl 2,6-Pyridinedicarboxylate
Purity
min. 98.0 %
Packaging
5G
Price
$78
Updated
2024/03/01
TCI Chemical
Product number
P1240
Product name
Diethyl 2,6-Pyridinedicarboxylate
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$219
Updated
2024/03/01
TRC
Product number
D444763
Product name
Diethyl 2,6-Pyridinedicarboxylate
Packaging
500mg
Price
$65
Updated
2021/12/16
AK Scientific
Product number
J98984
Product name
Diethylpyridine-2,6-dicarboxylate
Packaging
25g
Price
$70
Updated
2021/12/16
Matrix Scientific
Product number
083393
Product name
Diethyl pyridine-2,6-dicarboxylate
Purity
97%
Packaging
1g
Price
$102
Updated
2021/12/16
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Diethyl 2,6-pyridinedicarboxylate Chemical Properties,Usage,Production

Chemical Properties

Yellow to red crystalline powder

Synthesis

Pyridine-2,6-dicarboxylic acid (10.0g, 59.9mmol) was added into ethanol (120mL), then 3 drops of concentrated sulfuric acid were added. The mixture was heated to reflux for 8 hours. After evaporation of the solvent, the solid residue was washed with saturated Na2CO3 aqueous solution and extracted with chloroform for 3 times. The organic phase was dried with small amount of MgSO4. The solvent was removed to afford 1 as white powder (12.6g, 56.3mmol, yield = 94%). 1 H-NMR (400MHz, CDCl3) |? ppm 8.29 (d, J = 7.80 Hz, 2H), 8.01 (t, J = 7.80, 7.80 Hz, 1H), 4.50 (q, J = 7.12, 7.12, 7.12 Hz, 2H), 1.47 (t, J = 7.13, 7.13 Hz, 3H). 13C-NMR (100 MHz, CDCl3) |? ppm 164.6, 148.6, 138.2,127.8, 62.3,14.2,14.2. ESI MS: m/z = 224.1 [M+H]+ , 246.1 [M+Na]+ .

Diethyl 2,6-pyridinedicarboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Diethyl 2,6-pyridinedicarboxylate manufacturers

Dideu Industries Group Limited
Product
Diethyl 2,6-pyridinedicarboxylate 15658-60-3
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-10-28
Career Henan Chemical Co
Product
Diethyl 2,6-pyridinedicarboxylate 15658-60-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2019-07-02

15658-60-3, Diethyl 2,6-pyridinedicarboxylateRelated Search:

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