BOC-LYS(TFA)-OH

Product Name: BOC-LYS(TFA)-OH
CAS No.: 16965-06-3
Chemical Name: BOC-LYS(TFA)-OH
Synonyms: NSC 164662;BOC-LYS(TFA)-OH;BOC-L-LYS(TFA)-OH;BOC-LYSINE(TFA)-OH;BOC-N-E-TFA-L-LYSINE;BOC-LYS(TFA)-OH USP/EP/BP;N-ALPHA-T-BOC-NE-TFA-L-LYS;BOC-N-EPSILON-TFA-L-LYSINE;Boc-(Trifluoroacetyl) Lysine;(Tert-Butoxy)Carbonyl Lys(Tfa)-OH
CBNumber: CB8226628
Molecular Formula: C13H21F3N2O5
Formula Weight: 342.31
MOL File: 16965-06-3.mol

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BOC-LYS(TFA)-OH Property

Melting point:: 102-105 °C
Boiling point:: 485.6±45.0 °C(Predicted)
Density: 1.254±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Store in freezer, under -20°C
solubility: Soluble in DMSO.
form: Powder
pka: 3.97±0.21(Predicted)
color: White
optical activity: -12.72°(C=0.87g/100mI, DMF, 20°C, 589nm)

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Safety

WGK Germany: 3
F: 10-21
HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B657083
Product name: Boc-Lys(Tfa)-OH
Packaging: 5g
Price: $110
Updated: 2021/12/16

Usbiological

Product number: 264823
Product name: N-alpha-Boc-Nε-trifluoroacetyl-L-lysine
Packaging: 5g
Price: $395
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB47811
Product name: N-alpha-Boc-Nepsilon-trifluoroacetyl-L-lysine
Packaging: 10g
Price: $126.6
Updated: 2021/12/16

Iris Biotech GmbH

Product number: BAA5790
Product name: Boc-L-Lys(TFA)-OH
Packaging: 25g
Price: $303.75
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: AAA0001597
Product name: N-ALPHA-T-BOC-N-EPSILON-TRIFLUOROACETYL-L-LYSINE
Purity: 95.00%
Packaging: 0.5G
Price: $638
Updated: 2021/12/16

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BOC-LYS(TFA)-OH Chemical Properties,Usage,Production

Chemical Properties

White powder

Uses

Boc-Lys(Tfa)-OH (cas# 16965-06-3) is a compound useful in organic synthesis.

Synthesis

24424-99-5

10009-20-8

96561-04-5

The general procedure for the synthesis of N2-(tert-butoxycarbonyl)-N6-(2,2,2-trifluoroacetyl)-D-lysine from di-tert-butyl dicarbonate and trifluoroacetyl-lysine was as follows: trifluoroacetyl-lysine (3.63 g, 0.015 mol) was suspended in 40 ml of N,N-dimethylformamide (DMF), to which was added triethylamine (TEA, 3.03 g , 0.03 mol) and di-tert-butyl dicarbonate (3.6 g, 0.0165 mol). The reaction mixture was stirred at room temperature for 3 hours. After completion of the reaction, the mixture was diluted with water to three times the original volume and acidified with hydrochloric acid to pH 2. The product was extracted with ethyl acetate (EtOAc, 100 ml), the organic phase was washed with water and saturated brine sequentially and dried with anhydrous magnesium sulfate (MgSO4). The solvent was removed by distillation under reduced pressure to afford (S)-2-((tert-butoxycarbonyl)amino)-6-(2,2,2-trifluoroacetamido)hexanoic acid (4.7 g, 92% yield). The analytical data of the product (3) were in agreement with literature reports.

References

[1] Patent: WO2009/114809, 2009, A1. Location in patent: Page/Page column 7-8
[2] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 1, p. 255 - 258

BOC-LYS(TFA)-OH Preparation Products And Raw materials

Raw materials

Preparation Products

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BOC-LYS(TFA)-OH Suppliers

China 100 France 2 Germany 4 India 1 Japan 4 South Korea 1 Switzerland 2 United Kingdom 3 United States 15 Global 132

Chembest Research Laboratories Limited

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Alfa Aesar

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GL Biochem (Shanghai) Ltd

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Adamas Reagent, Ltd.

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Shanghai Hanhong Scientific Co.,Ltd.

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Chemsky (shanghai) International Co.,Ltd

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Shanghai Sphchem Co., Ltd.

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Beijing HuaMeiHuLiBiological Chemical

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Finetech Industry Limited

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Email: sales@finetechnology-ind.com
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ProdList: 9637
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Sichuan Ampebiochem Co., Ltd.

Tel: 028-65294243 13981822079;18682730901
Email: sales@ampebiochem.com
Country: China
ProdList: 1000
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View Lastest Price from BOC-LYS(TFA)-OH manufacturers

Career Henan Chemical Co

Product: BOC-LYS(TFA)-OH 16965-06-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-11

16965-06-3, BOC-LYS(TFA)-OHRelated Search:

N-Boc-L-alaninol L(+)-Lysine monohydrate BOC-LYS(AC)-OH 6-Acetamidohexanoic acid N-Methyl-2,2,2-trifluoroacetamide BOC-NVA-OH tert-Butyl carbamate Trifluoroacetamide BOC-LYS(TFA)-OH Boc-DL-alanine BOC-Glycine BOC-L-NORLEUCINE N-6-Trifluoroacetyl-L-lysine TERT-BUTYL N-(2-HYDROXYETHYL)CARBAMATE L-Lysine N-BOC-D/L-NORVALINOL BOC-DL-2-AMINOBUTYRIC ACID BOC-LYS(TFA)-OSU

BOC-L-LYS(TFA)-OH

BOC-LYS(TFA)-OH

BOC-LYSINE(TFA)-OH

BOC-N-EPSILON-TRIFLUOROACETYL-L-LYSINE

BOC-N-EPSILON-TFA-L-LYSINE

N-ALPHA-BOC-N-EPSILON-TRIFLUOROACETYL-L-LYSINE

N-ALPHA-T-BUTYLOXYCARBONYL-N-EPSILON-TRIFLUORACETYL-L-LYSINE

N-ALPHA-T-BUTOXYCARBONYL-N-EPSILON-TRIFLUOROACETYL-L-LYSINE

N-ALPHA-T-BOC-N-EPSILON-TRIFLUOROACETYL-L-LYSINE

N-ALPHA-T-BOC-NE-TFA-L-LYS

N-α-Boc-N-ε-trifluoroacetyl-L-lysine

2-[[(2-methylpropan-2-yl)oxy-oxomethyl]amino]-6-[(2,2,2-trifluoro-1-oxoethyl)amino]hexanoic acid

(2S)-2-{[(tert-butoxy)carbonyl]amino}-6-(trifluoroacetamido)hexanoic acid

N-ALPHA-TERT-BUTYLOXYCARBONYL-N-EPSILON-TRIFLUORACETYL-L-LYSINE

NALPHA-tert-Butoxycarbonyl-NEPSILON-trifluoroacetyl-L -lysine

Boc-(Trifluoroacetyl) Lysine

BOC-N-E-TFA-L-LYSINE

(S)-2-((tert-Butoxycarbonyl)aMino)-6-(2,2,2-trifluoroacetaMido)hexanoic acid

(S)-6-(Trifluoroacetylamino)-2-(tert-butoxycarbonylamino)hexanoic acid

N2-[(1,1-Dimethylethoxy)carbonyl]-N6-(2,2,2-trifluoroacetyl)-L-lysine

NSC 164662

N^a-Boc-N^e-trifluoroacetyl-L-lysine, 95%

N2-tert-Butoxycarbonyl-N6-trifluoroacetyl-L-lysine

N2-Boc-N6-(2,2,2-trifluoroacetyl)-L-lysine

Nα-Boc-Nε-trifluoroacetyl-L-lysine≥ 99% (HPLC)

(Tert-Butoxy)Carbonyl Lys(Tfa)-OH

(2S)-2-{[(tert-butoxy)carbonyl]amino}-6-(2,2,2-trifluoroacetamido)hexanoic acid

L-Lysine, N2-[(1,1-dimethylethoxy)carbonyl]-N6-(2,2,2-trifluoroacetyl)-

N^a-Boc-N^e-trifluoroacetyl-L-lysine,95%

(S)-2-((tert-Butoxycarbonyl)amino)-6-(2,2,2-trifluoroacetamido)hexanoicaci

BOC-LYS(TFA)-OH USP/EP/BP

Nα-Boc-Nε-trifluoroacetyl-L-lysine

16965-06-3

Amino Acid Derivatives

Lysine

Peptide Synthesis

Specialty Synthesis

Amino Acids

AMINOACIDS DERIVATIVES