ChemicalBook > CAS DataBase List > 3,5-Dinitrobenzoic acid

3,5-Dinitrobenzoic acid

Product Name
3,5-Dinitrobenzoic acid
CAS No.
99-34-3
Chemical Name
3,5-Dinitrobenzoic acid
Synonyms
3,5-DINITROBENZOATE;3,5-Dinitrobenzoic acid Solution, 100ppm;3,5-DNBA;3.5-Dinitr;3,5-dinitrobenzoic;RARECHEM AL BO 0231;TIMTEC-BB SBB007840;Dinitrobenzoic acid;DNBA)3,5-Dinitrobenz;3,5-DNBAfreeofsulfur
CBNumber
CB8295480
Molecular Formula
C7H4N2O6
Formula Weight
212.12
MOL File
99-34-3.mol
More
Less

3,5-Dinitrobenzoic acid Property

Melting point:
204-206 °C (lit.)
Boiling point:
351.93°C (rough estimate)
Density 
1.683
refractive index 
1.5300 (estimate)
storage temp. 
Sealed in dry,Room Temperature
solubility 
ethanol: soluble0.5g/10 mL, clear, yellow to very deep greenish-yellow
form 
Solid
pka
pK1:2.85 (25°C)
color 
Yellow crystalline
PH Range
2.7
Water Solubility 
1350 mg/L (25 ºC)
Merck 
14,3276
BRN 
1914286
Stability:
Stable. Contact with strong bases may lead to fire. Incompatible with strong bases, strong oxidizing agents.
LogP
1.51 at 20℃
CAS DataBase Reference
99-34-3(CAS DataBase Reference)
NIST Chemistry Reference
Benzoic acid, 3,5-dinitro-(99-34-3)
EPA Substance Registry System
3,5-Dinitrobenzoic acid (99-34-3)
More
Less

Safety

Hazard Codes 
Xn,F
Risk Statements 
22-36/37/38-68-11
Safety Statements 
26-36/37/39-16
RIDADR 
UN1325
WGK Germany 
3
RTECS 
DG9140700
TSCA 
Yes
HazardClass 
4.1
PackingGroup 
III
HS Code 
29163900
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

H413May cause long lasting harmful effects to aquatic life

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P273Avoid release to the environment.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
121258
Product name
3,5-Dinitrobenzoic acid
Purity
99%
Packaging
100g
Price
$47
Updated
2024/03/01
Sigma-Aldrich
Product number
121258
Product name
3,5-Dinitrobenzoic acid
Purity
99%
Packaging
500g
Price
$147
Updated
2024/03/01
TCI Chemical
Product number
D0824
Product name
3,5-Dinitrobenzoic Acid
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$16
Updated
2024/03/01
TCI Chemical
Product number
D0824
Product name
3,5-Dinitrobenzoic Acid
Purity
>98.0%(GC)(T)
Packaging
500g
Price
$91
Updated
2024/03/01
Alfa Aesar
Product number
A16502
Product name
3,5-Dinitrobenzoic acid, 98+%
Packaging
250g
Price
$44.65
Updated
2024/03/01
More
Less

3,5-Dinitrobenzoic acid Chemical Properties,Usage,Production

Chemical Properties

White to pale yellow monoclinic prismatic crystal. Soluble in alcohol and glacial acetic acid, slightly soluble in water, ether and carbon disulfide. Can be volatile with water vapor.

Uses

3,5-nitrobenzoic acid is an important intermediate for organic synthesis, in the pharmaceutical industry for the synthesis sulfachrysoidine and for the detection of ampicillin.

Uses

3,5-Dinitrobenzoic acid, is used as a reagent used in the derivatization of resins and the determination of ampicillin.

Preparation

3,5-Dinitrobenzoic acid is synthesized by nitration of benzoic acid. Sulfuric acid was added to the dry reaction pot, and benzoic acid was added under stirring. Heat to 60°C, add fuming nitric acid dropwise, and complete the dropwise addition below 85°C. React at 80-85°C for 1 h, 100°C for 0.5-1h, and then heat up to 135°C for 2h. Leave overnight. The reaction solution was put into ice water to separate out crystals, filtered, washed with water and then washed with 50% ethanol to obtain 3,5-dinitrobenzoic acid. Yield 70%.

Application

3,5-Dinitrobenzoic Acid is used in fluorometric analysis of creatinine (which is a determinant of kidney function). Also used as a reagent in the synthesis of several organic compounds including that of rhodanine derivatives that act as aldose reductase inhibitors.

Definition

ChEBI: 3,5-dinitrobenzoic acid is a member of the class of benzoic acids that is benzoic acid in which the hydrogens at positions 3 and 5 are replaced by nitro groups. It is a C-nitro compound and a member of benzoic acids.

General Description

3,5-Dinitrobenzoic acid forms an adduct with 3,5-dimethylpyridine and the crystal structure of adduct has been studied at room temperature and 80K for both undeuterated and deuterated compounds. It forms 1:1 cocrystal with analgesic drug, ethenzamide and exists in two polymorphic forms.

Purification Methods

Crystallise the acid from distilled H2O or 50% EtOH (4mL/g). Dry it in a vacuum desiccator or at 70o over BaO under a vacuum for 6hours. [Beilstein 9 II 279, 9 III 1779, 9 IV 1242.]

3,5-Dinitrobenzoic acid Preparation Products And Raw materials

Raw materials

Nitric acid

Preparation Products

3-AMINO-5-BROMO-BENZOIC ACID Diatrizoic Acid Dihydrate 3-Bromo-5-nitrobenzoic acid 3,5-Dinitrobenzoyl chloride 3-Amino-5-nitrobenzoic acid 3-BROMO-5-IODOBENZOIC ACID
More
Less

3,5-Dinitrobenzoic acid Suppliers

Americas 1 Belgium 1 Canada 2 China 446 Czech Republic 1 Europe 4 Germany 8 India 93 Japan 5 Slovakia 1 South Korea 1 Switzerland 3 Ukraine 4 United Kingdom 16 United States 50 Global 636
Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
HBCChem, Inc.
Tel
+1-510-219-6317
Fax
+1-650-486-1361
Email
sales@hbcchem.com
Country
United States
ProdList
10648
Advantage
60
Alchem Pharmtech,Inc.
Tel
8485655694
Email
sales@alchempharmtech.com
Country
United States
ProdList
63687
Advantage
58
Protheragen-ING
Tel
+16313385890
Email
info@protheragen-ing.com
Country
United States
ProdList
3868
Advantage
58
Aladdin Scientific
Tel
+1-+1(833)-552-7181
Email
sales@aladdinsci.com
Country
United States
ProdList
57505
Advantage
58
Alfa Chemistry
Tel
--
Fax
--
Email
info@Alfa-Chemistry.com
Country
United States
ProdList
6814
Advantage
0
Redox Scientific
Tel
--
Fax
--
Email
info@redoxsci.com
Country
United States
ProdList
2380
Advantage
58
Alichem Inc.
Tel
--
Fax
--
Email
sales@alichem.com
Country
United States
ProdList
6167
Advantage
58
Oakwood Products, Inc.
Tel
--
Fax
--
Email
sales@oakwoodchemical.com
Country
United States
ProdList
6193
Advantage
74
Combi-Blocks Inc.
Tel
--
Fax
--
Email
sales@combi-blocks.com
Country
United States
ProdList
6618
Advantage
69
SynQuest Laboratories, Inc.
Tel
--
Fax
--
Email
info@synquestlabs.com
Country
United States
ProdList
6871
Advantage
62
Riedel-de Haen AG
Tel
--
Fax
--
Country
United States
ProdList
6773
Advantage
87
TCI America
Tel
--
Fax
--
Email
sales@tciamerica.com
Country
United States
ProdList
6909
Advantage
75
Frontier Scientific, Inc.
Tel
--
Fax
--
Email
sales@frontiersci.com
Country
United States
ProdList
6222
Advantage
86
Matrix Scientific
Tel
--
Fax
--
Email
sales@matrixscientific.com
Country
United States
ProdList
6632
Advantage
80
Cambrex Pharma & Biopharmaceuticals
Tel
--
Fax
--
Email
pharma@cambrex.com
Country
United States
ProdList
261
Advantage
75
Labseeker Inc
Tel
--
Fax
--
Email
marketing@labseeker.com
Country
United States
ProdList
1495
Advantage
55
Sisco Research Laboratories Pvt. Ltd.
Tel
--
Fax
--
Email
srlmarketing@dishnetdsl.net
Country
United States
ProdList
1905
Advantage
64
AlliChem, LLC
Tel
--
Fax
--
Email
sales@allichemllc.com
Country
United States
ProdList
6516
Advantage
60
ChemService Inc.
Tel
--
Fax
--
Country
United States
ProdList
6379
Advantage
68
Advanced Synthesis Technologies
Tel
--
Fax
--
Email
sales@advancedsynthesis.com
Country
United States
ProdList
4775
Advantage
61
Ivy Fine Chemicals
Tel
--
Fax
--
Email
sales@ivychem.com
Country
United States
ProdList
6493
Advantage
58
ECA International Corporation
Tel
--
Fax
--
Email
services@ecacorporation.com
Country
United States
ProdList
1062
Advantage
52
Alfa Aesar
Tel
--
Fax
--
Email
tech@alfa.com
Country
United States
ProdList
6814
Advantage
81
Waterstone Technology, LLC
Tel
--
Fax
--
Email
sales@waterstonetech.com
Country
United States
ProdList
6786
Advantage
30
Naugra Export
Tel
--
Fax
--
Country
United States
ProdList
1332
Advantage
47
Finornic Chemicals (I) Pvt. Ltd.
Tel
--
Fax
--
Country
United States
ProdList
50
Advantage
60
HONEST JOY HOLDINGS LIMITED
Tel
--
Fax
--
Email
sales@honestjoy.cn
Country
United States
ProdList
6675
Advantage
54
3B Scientific Corporation
Tel
--
Fax
--
Email
sales@3bsc.com
Country
United States
ProdList
6718
Advantage
47
Aagile Labs Division of Tyger Scientific
Tel
--
Fax
--
Email
tygersci@yahoo.com
Country
United States
ProdList
6568
Advantage
68
Sciencelab.com, Inc.
Tel
--
Fax
--
Email
accounting@sciencelab.com
Country
United States
ProdList
4159
Advantage
82
Advance Scientific & Chemical
Tel
--
Fax
--
Email
sales@advance-scientific.com
Country
United States
ProdList
6419
Advantage
71
Loba Chemie Pvt. Ltd.
Tel
--
Fax
--
Country
United States
ProdList
1945
Advantage
71
ChromaDex
Tel
--
Fax
--
Email
sales@chromadex.com
Country
United States
ProdList
2501
Advantage
76
AK Scientific, Inc.
Tel
--
Fax
--
Email
sales@aksci.com
Country
United States
ProdList
6347
Advantage
65
Skylead Chemicals Limited
Tel
--
Fax
--
Email
skylead@rediffmail.com
Country
United States
ProdList
35
Advantage
46
Eastern Chemical Corp.
Tel
--
Fax
--
Email
eastern@u-g.com
Country
United States
ProdList
2786
Advantage
34
City Chemicals Corporation
Tel
--
Fax
--
Country
United States
ProdList
6460
Advantage
72
Wilshire Chemical Company Inc.
Tel
--
Fax
--
Email
WilshrChem@AOL.COM
Country
United States
ProdList
3498
Advantage
58
ChemPacific Corporation
Tel
--
Fax
--
Email
sales@chempacific.com
Country
United States
ProdList
6891
Advantage
51
Richman Chemical Inc.
Tel
--
Fax
--
Email
kac@richmanchemical.com
Country
United States
ProdList
692
Advantage
67
ASDI Incorporated
Tel
--
Fax
--
Email
customerservice@asdi.net
Country
United States
ProdList
6922
Advantage
67
EMD Biosciences, Inc.
Tel
--
Fax
--
Email
technical@calbiochem.com
Country
United States
ProdList
6529
Advantage
66
Aakash Chemicals and Dye-Stuffs, Inc.
Tel
--
Fax
--
Email
info@aakashchemicals.com
Country
United States
ProdList
1012
Advantage
54
Spectrum Chemicals & Laboratory Products
Tel
--
Fax
--
Email
sales@spectrumchemical.com
Country
United States
ProdList
6699
Advantage
77
Crescent Chemical Co., Inc.
Tel
--
Fax
--
Email
sales@creschem.com
Country
United States
ProdList
4597
Advantage
68
MP Biomedicals, Inc.
Tel
--
Fax
--
Country
United States
ProdList
6561
Advantage
81
Charkit Chemical Corporation
Tel
--
Fax
--
Email
sales@charkit.com
Country
United States
ProdList
2993
Advantage
65
Pfaltz & Bauer, Inc.
Tel
--
Fax
--
Email
sales@pfaltzandbauer.com
Country
United States
ProdList
6828
Advantage
72
TimTec Corporation
Tel
--
Fax
--
Email
info@timtec.net
Country
United States
ProdList
6891
Advantage
68
More
Less

View Lastest Price from 3,5-Dinitrobenzoic acid manufacturers

Asia Chem I and E (Jiangsu) Co Ltd
Product
3,5-Dinitrobenzoic acid 99-34-3
Price
US $22.33/Kg/Drum
Min. Order
25Kg/Drum
Purity
99.5%HPLC
Supply Ability
20tons/month
Release date
2021-09-23
Jinan Finer Chemical Co., Ltd
Product
3,5-Dinitrobenzoic acid 99-34-3
Price
US $0.00/Kg/Drum
Min. Order
1KG
Purity
99%
Supply Ability
200mt/year
Release date
2021-08-03
Hebei Zhuanglai Chemical Trading Co Ltd
Product
3,5-Dinitrobenzoic acid 99-34-3
Price
US $10.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 ton
Release date
2024-12-17

99-34-3, 3,5-Dinitrobenzoic acidRelated Search:

Sodium 3-nitrobenzoate Ethyl 2-(Chlorosulfonyl)acetate 4-METHYL-3,5-DINITROBENZOIC ACID 4-Nitrophenyl chloroformate Glycine 3,5-DINITROBENZOIC ACID METHYL ESTER Folic acid 4-Nitrobenzoic acid 3,5-Dimethylbenzoic acid 3,5-Dinitro-o-Toluic Acid 2-Methyl-3,5-Dinitrobenzoic acid,2-METHYL-3,5-DINITROBENZOIC ACID 3,5-Dinitrobenzonitrile 3,5-Dinitrobenzamide 3,5-Dibromo-4-hydroxybenzaldehyde 3 5-DINITROBENZOIC ACID ETHYLSTER,3,5-DINITROBENZOIC ACID ETHYL ESTER 2,4-Dinitrophenylhydrazine 2 4-DICHLORO-3 5-DINITROBENZOIC ACID 9&,2,4-DICHLORO-3,5-DINITROBENZOIC ACID 95+%,2,4-DICHLORO-3,5-DINITROBENZOIC ACID 1,3-Dinitrobenzene 2-Chloro-3,5-dinitrobenzoic acid

  • 3,5-Dinitrobenzoic acid Solution, 100ppm
  • 3,5-nitrobenzoic acid
  • 3, 5-2 nitro benzoic acid
  • 3.5-Dinitr
  • DINITROBENZOIC-3,5 ACID
  • DINITROBENZOIC ACID,3,5-
  • 3-CARBOXY-1,5-DINITROBENZENE
  • 3,5-DINITROBENZOIC ACID
  • RARECHEM AL BO 0231
  • 3,5-Dinitrobenzoic acid (DNBA)
  • 3,5-Dinitrobenzoic acid manufacturer CAS NO.99-34-3
  • Top quality 3,5-Dinitrobenzoic acid with factory price
  • 3,5-Dinitrobenzoic acid CAS: 99-34-3
  • 3,5-Dinitrobenzoic acid CAS: 99-34-3 with best price
  • High purity CAS:99-34-3 3,5-Dinitrobenzoic acid
  • 99% 3,5-Dinitrobenzoic acid CAS:99-34-3
  • 3,5-DINITROBENZOIC ACID 118-97-4 98.5% CAS:99-34-3
  • High purity CAS:99-34-3 99% 3,5-Dinitrobenzoic acid with competitive price
  • TIMTEC-BB SBB007840
  • 3,5-dinitrobenzoic
  • 3,5-dinitro-benzoicaci
  • DNBA)3,5-Dinitrobenz
  • Dinitrobenzoic acid
  • 3,5-DINITROBENZOIC ACID*PHOTOGRAPHIC GRA DE
  • 3-5-DINITROBENZOIC ACID CRYSTALLINE
  • 3,5-DINITROBENZOIC ACID OEKANAL, 250 MG
  • 3,5-DinitrobenzoicAcidGr
  • 3,5-DNBAfreeofsulfur
  • Benzoic acid, 3,5-dinitro-
  • 3,5-DINITROBENZOICACID,REAGENT
  • DINITROBENZOIC ACID,3,5-(RG)
  • 3,5-DINITROBENZOICAICD
  • 3,5-Dinitrobenzoic acid, synthesis grade
  • 3,5-Dinitrobenzoic a
  • 2-nitryl-4-fluoro benzoicacide
  • 3,5-Dinitrobenzoic acid, 99% 100GR
  • 3,5-Dinitrobenzoic acid, 99% 500GR
  • 3,5-Dinitrobenzoic acid anion
  • 3,5-Dinitrobenzoic acid, 98+%
  • 3,5-DINITROBENZOIC ACID extrapure AR
  • 3,5-DINITROBENZOATE
  • 3,5-DINITROBENZOIC ACID 99+%
  • 3,5-DINITROBENZOIC ACID SOLUTION [FOR SPRAY]
  • 99% 3,5-Dinitrobenzoic acid
  • 3,5-Dinitrobenzoic Acid &gt
  • 3,5-dinitrobenzanic acid
  • 3,5-Dinitrobenzoic acid ISO 9001：2015 REACH
  • Vitamin D2 Impurity 8
  • 3,5-Dinitrobenzoic acid, GR 99%+
  • 3,5-Dinitrobenzoic Acid extrapure AR, ExiPlus, Multi-Compendial, 99%
  • 3,5-Dinitrobenzoic Acid extrapure, 98%
  • 3,5-DINITROBENZOIC ACID For Synthesis
  • 3,5-DNBA
  • 3,5 -Dinitrobenzoic Acid 98% For Synthesis
  • 3,5-Dinitrobenzoic acid 100 μg/ml Acetonitrile
  • C12783600 3,5-DinitrobenzoiCacid
  • Deferasirox Impurity 34
  • 99-34-3