ChemicalBook > CAS DataBase List > Ethyl N-cyanoethanimideate

Ethyl N-cyanoethanimideate

Product Name
Ethyl N-cyanoethanimideate
CAS No.
1558-82-3
Chemical Name
Ethyl N-cyanoethanimideate
Synonyms
(E)-Ethyl N-cyanoacetiMidate;Cyanoethyl ester;CYANO ETHYL ACETAMIDATE;ETHYLN-CYANOACETOIMIDATE;Ethyl N-cyanoacetiMidate;ethyl N-cyanoethanimidoate;Ethyl N-cyanoethanimideate;ETHYL N-CYANO ETHANIMIDATE;Ethyl (E)-N-cyanoacetimidate;N-CYANOETHANIMIDIC ETHYL ESTER
CBNumber
CB8682134
Molecular Formula
C5H8N2O
Formula Weight
112.13
MOL File
1558-82-3.mol
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Ethyl N-cyanoethanimideate Property

Melting point:
78-81 °C(Solv: ethyl ether (60-29-7))
Boiling point:
133.2±23.0 °C(Predicted)
Density 
0.94
refractive index 
1.45
Flash point:
34°
storage temp. 
2-8°C
pka
-2.94±0.50(Predicted)
Appearance
Colorless to light yellow Liquid
InChI
InChI=1S/C5H8N2O/c1-3-8-5(2)7-4-6/h3H2,1-2H3
InChIKey
PLVWUINOWYHRAA-UHFFFAOYSA-N
SMILES
C(=NC#N)(OCC)C
CAS DataBase Reference
1558-82-3(CAS DataBase Reference)
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Safety

RIDADR 
UN3273
HS Code 
2926.90.5050
HazardClass 
3, 6.1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H226Flammable liquid and vapour

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P311Call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TCI Chemical
Product number
E1331
Product name
Ethyl N-Cyanoacetimidate
Packaging
5G
Price
$34
Updated
2025/07/31
TCI Chemical
Product number
E1331
Product name
Ethyl N-Cyanoacetimidate
Packaging
25G
Price
$97
Updated
2025/07/31
TRC
Product number
B124878
Product name
EthylN-Cyanoethanimidoate
Packaging
500mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC37261
Product name
Cyano ethyl acetamidate
Packaging
5G
Price
$78.1
Updated
2021/12/16
AK Scientific
Product number
J99262
Product name
Cyanoethylacetamidate
Packaging
100g
Price
$90
Updated
2021/12/16
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Ethyl N-cyanoethanimideate Chemical Properties,Usage,Production

Preparation

To a flask equipped as in Preparation 2-6 is added 162.0 gm (1.0 mole) of ethyl orthoacetate, 42.0 gm (1.0 mole) of cyanamide, and 134.0 gm (2.0 moles) of acetic anhydride. The reaction mixture is heated to 130-140°C and the ethyl acetate and acetic acid are distilled over. The heat is removed until the initial vigorous reaction subsides and then the heat­ing is continued at 135-140°C until most of the remaining ethyl acetate and acetid acid have distilled over (approx. 1 hr). The residue is then distilled under reduced pressure to afford 100.8 gm (90%), b.p. 90-95°C (20 mm Hg).

Synthesis

420-04-2

78-39-7

1558-82-3

General methodology: The compound was synthesized with reference to literature methods. The standard procedure we used is detailed below: the mixed system of the original triethyl acetate (0.12 mol), cyanamide (0.1 mol) and a small amount of acetic acid (a few drops) was refluxed for 6 hours, followed by distillation and purification under reduced pressure (14 mmHg).

References

[1] Phosphorus, Sulfur and Silicon and the Related Elements, 2016, vol. 191, # 5, p. 759 - 764
[2] Patent: US5750545, 1998, A
[3] Patent: WO2008/42928, 2008, A2. Location in patent: Page/Page column 33
[4] Patent: WO2008/42928, 2008, A2. Location in patent: Page/Page column 33
[5] Journal of Organic Chemistry, 1963, vol. 28, p. 1816 - 1821

Ethyl N-cyanoethanimideate Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethyl N-cyanoethanimideate Suppliers

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View Lastest Price from Ethyl N-cyanoethanimideate manufacturers

Career Henan Chemical Co
Product
Ethyl N-cyanoethanimideate 1558-82-3
Price
US $1.00/KG
Min. Order
1KG
Purity
95%-99.99%
Supply Ability
1kg-10MT
Release date
2019-05-24

1558-82-3, Ethyl N-cyanoethanimideateRelated Search:

Ethyl acrylate Ethyl formate Ethanol ISOXADIFEN-ETHYL Methylene dithiocyanate Tris(trimethylsilyl)phosphate ETHYL 2-CYANOACRYLATE Ethyl cyanoformate Sodium cyanoborohydride Ethyl isocyanoacetate Methyl acrylate 2-Ethoxyethanol 2-Cyanoacetamide Ethylparaben Ethyl pyruvate Trinexapac-ethyl Dimethyl succinate Methyl 4-cyanobenzoate

  • n-cyanoethanimidic acid ethyl ester
  • N-CYANOETHANIMIDIC ETHYL ESTER
  • ETHYLN-CYANOACETOIMIDATE
  • ETHYL N-CYANO ETHANIMIDATE
  • Ethyl N-cyanoethanimideate
  • CYANO ETHYL ACETAMIDATE
  • N-cyanoacetimidic acid ethyl ester
  • Ethyl N-cyanoacetiMidate
  • (E)-Ethyl N-cyanoacetiMidate
  • ethyl N-cyanoethanimidoate
  • Ethyl N-cyanoethanecarboximidate
  • Cyanoethyl ester
  • 2-(cyanoamino)-2-oxoacetic acid ethyl ester
  • Ethanimidic acid, N-cyano-, ethyl ester
  • Ethyl (1E)-N-cyanoethanimidate
  • Ethyl (E)-N-cyanoacetimidate
  • 1558-82-3
  • john's