ChemicalBook > CAS DataBase List > 6-CHLORO-2-CYANO-3-NITROPYRIDINE

6-CHLORO-2-CYANO-3-NITROPYRIDINE

Product Name
6-CHLORO-2-CYANO-3-NITROPYRIDINE
CAS No.
93683-65-9
Chemical Name
6-CHLORO-2-CYANO-3-NITROPYRIDINE
Synonyms
6-Chloro-3-nitropicolinonitrile;C90144;6-Chloro-2-cyano-3-nitropyidine;6-CHLORO-2-CYANO-3-NITROPYRIDIN;6-CHLORO-2-CYANO-3-NITROPYRIDINE;2-cyano-6-chloro-3-nitropyridine;6-chloro-3-nitro-2-pyridinecarbonitrile;6-CHLORO-3-NITROPYRIDINE-2-CARBONITRILE;2-Pyridinecarbonitrile, 6-chloro-3-nitro-;6-Chloro-3-nitro-2-cyanopyridine≥ 97.0% (HPLC)
CBNumber
CB8689052
Molecular Formula
C6H2ClN3O2
Formula Weight
183.55
MOL File
93683-65-9.mol
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6-CHLORO-2-CYANO-3-NITROPYRIDINE Property

Melting point:
118-120 °C
Boiling point:
347.2±42.0 °C(Predicted)
Density 
1.57±0.1 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
solid
pka
-10.14±0.10(Predicted)
Appearance
White to light yellow Solid
InChI
InChI=1S/C6H2ClN3O2/c7-6-2-1-5(10(11)12)4(3-8)9-6/h1-2H
InChIKey
XVIHGTRTKQZJAC-UHFFFAOYSA-N
SMILES
C1(C#N)=NC(Cl)=CC=C1[N+]([O-])=O
CAS DataBase Reference
93683-65-9(CAS DataBase Reference)
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Safety

Hazard Codes 
T
RIDADR 
UN2811
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR6409
Product name
6-Chloro-3-nitropyridine-2-carbonitrile
Purity
98%
Packaging
1g
Price
$21
Updated
2021/12/16
SynQuest Laboratories
Product number
4H55-5-X2
Product name
6-Chloro-3-nitropyridine-2-carbonitrile
Purity
98%
Packaging
1g
Price
$23
Updated
2021/12/16
AK Scientific
Product number
X8410
Product name
6-Chloro-2-cyano-3-nitropyridine
Packaging
1g
Price
$54
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC06230
Product name
6-Chloro-2-cyano-3-nitropyridine
Packaging
2g
Price
$60
Updated
2021/12/16
ChemScene
Product number
CS-0022422
Product name
6-Chloro-3-nitropicolinonitrile
Purity
98.85%
Packaging
5g
Price
$69
Updated
2021/12/16
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6-CHLORO-2-CYANO-3-NITROPYRIDINE Chemical Properties,Usage,Production

Chemical Properties

Light yellow Cryst

Synthesis

16013-85-7

544-92-3

93683-65-9

General procedure for the preparation of 2-cyano-3-nitro-6-chloropyridine: 1. 2,6-dichloro-3-nitropyridine (5.0 g, 25.9 mmol) and cuprous(I) cyanide (2.55 g, 28.5 mmol) were mixed in N-methylpyrrolidone (19 mL). 2. the mixture was heated to 180 °C and maintained for 15 min. 3. After completion of the reaction, cooled to room temperature, the reaction mixture was poured into ice water and stirred for 10 minutes. 4. The aqueous layer was separated and the organic layer was extracted with boiling toluene followed by re-extraction with ethyl acetate. 5. The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. 6. The residue was ground with ether and filtered to give 2-cyano-3-nitro-6-chloropyridine (1.76 g, 39% yield). 1H-NMR (CDCl3, 300MHz) data: δ 7.78 (d, J = 8.9Hz, 1H), 8.54 (d, J = 8.9Hz, 1H).

References

[1] Journal of Heterocyclic Chemistry, 1984, vol. 21, # 5, p. 1521 - 1525
[2] Patent: WO2005/97805, 2005, A1. Location in patent: Page/Page column 48-49
[3] Journal of Medicinal Chemistry, 1998, vol. 41, # 23, p. 4533 - 4541

6-CHLORO-2-CYANO-3-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-CHLORO-2-CYANO-3-NITROPYRIDINE Suppliers

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View Lastest Price from 6-CHLORO-2-CYANO-3-NITROPYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
6-CHLORO-2-CYANO-3-NITROPYRIDINE 93683-65-9
Price
US $1.10/g
Min. Order
1g
Purity
99.0% min
Supply Ability
100 tons min
Release date
2021-05-12
Career Henan Chemical Co
Product
6-CHLORO-2-CYANO-3-NITROPYRIDINE 93683-65-9
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-11

93683-65-9, 6-CHLORO-2-CYANO-3-NITROPYRIDINERelated Search:

2-Chloro-3-cyanopyridine 2-chloro-5-cyanopyridine 4-CHLORO-PYRIDINE-2-CARBONITRILE 2,3,6-Trichloropyridine 2-Chloro-3-nitropyridine 5-CHLORO-2-CYANO-3-NITROPYRIDINE,5-CHLORO-2-CYANO-3-NITROPYRIDINE 98+% 3-Amino-6-chloro-2-picoline 3-Amino-6-chloropyridine-2-carbonitrile 2-Methyl-3-nitropyridine hydrochloride 6-Chloro-2-methyl-3-nitropyridine 2-Chloro-6-cyanopyridine 3-Amino-2-pyridinecarbonitrile 6-CHLORO-2-CYANO-3-NITROPYRIDINE 2-Cyano-3-nitropyridine

  • 6-CHLORO-2-CYANO-3-NITROPYRIDINE
  • 6-CHLORO-3-NITROPYRIDINE-2-CARBONITRILE
  • 6-Chloro-2-cyano-3-nitropyidine
  • 6-Chloro-3-nitropicolinonitrile
  • 6-chloro-3-nitro-2-pyridinecarbonitrile
  • C90144
  • 6-Chloro-2-cyano-3-nitropyridine, 6-Chloro-3-nitropicolinonitrile
  • 6-Chloro-3-nitro-2-cyanopyridine≥ 97.0% (HPLC)
  • 2-Pyridinecarbonitrile, 6-chloro-3-nitro-
  • 6-CHLORO-2-CYANO-3-NITROPYRIDINE ISO 9001：2015 REACH
  • 2-cyano-6-chloro-3-nitropyridine
  • 6-CHLORO-2-CYANO-3-NITROPYRIDIN
  • 93683-65-9
  • Pyridine series
  • Halides
  • Pyridines
  • pyridine