4-PIPERAZIN-1-YL-PHENYLAMINE
- Product Name
- 4-PIPERAZIN-1-YL-PHENYLAMINE
- CAS No.
- 67455-41-8
- Chemical Name
- 4-PIPERAZIN-1-YL-PHENYLAMINE
- Synonyms
- TIMTEC-BB SBB010619;4-PIPERAZINOANILINE;4-PIPERAZIN-1-YLANILINE;4-(1-Piperazinyl)aniline;4-(4-AMinophenyl)piperazine;4-PIPERAZIN-1-YL-PHENYLAMINE;4-(1-Piperazinyl)aniline, 97%;1-(4-AMINO-PHENYL)-PIPERAZINE;1-(4-AMinophenyl)piperazine 97%;BenzenaMine, 4-(1-piperazinyl)-
- CBNumber
- CB9452907
- Molecular Formula
- C10H15N3
- Formula Weight
- 177.25
- MOL File
- 67455-41-8.mol
4-PIPERAZIN-1-YL-PHENYLAMINE Property
- Melting point:
- 119-123 °C (lit.)
- Boiling point:
- 380.2±27.0 °C(Predicted)
- Density
- 1.107±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C, protect from light
- form
- Powder
- pka
- 9.12±0.10(Predicted)
- color
- White to purple
Safety
- Hazard Codes
- Xn
- Risk Statements
- 22-37/38-41
- Safety Statements
- 26-39
- WGK Germany
- 2
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H302Harmful if swallowed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- A615655
- Product name
- 1-(4-Aminophenyl)piperazine
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 3H30-1-WD
- Product name
- 4-Piperazin-1-ylaniline
- Purity
- 96%
- Packaging
- 1g
- Price
- $96
- Updated
- 2021/12/16
- Product number
- 0375AC
- Product name
- 4-(Piperazin-1-yl)aniline
- Packaging
- 1g
- Price
- $104
- Updated
- 2021/12/16
- Product number
- 081179
- Product name
- 1-(4-Aminophenyl)piperazine
- Purity
- 97%
- Packaging
- 1g
- Price
- $147
- Updated
- 2021/12/16
- Product number
- 3H30-1-WD
- Product name
- 4-Piperazin-1-ylaniline
- Purity
- 96%
- Packaging
- 5G
- Price
- $288
- Updated
- 2021/12/16
4-PIPERAZIN-1-YL-PHENYLAMINE Chemical Properties,Usage,Production
Uses
4-Piperazinoaniline(CAS#67455-41-8)is a important organic intermediate. It can be used in agrochemical, pharmaceutical and dyestuff field.
Synthesis
6269-89-2
67455-41-8
General procedure for the synthesis of 1-(4-aminophenyl)piperazine from 1-(4-nitrophenyl)piperazine: 1-(4-nitrophenyl)piperazine (414 mg, 2 mmol) was dissolved in a mixed solvent of ethanol (15 mL) and tetrahydrofuran (15 mL), and 10% palladium/carbon catalyst (50 mg) was added. The reaction was stirred for 3 h at room temperature under hydrogen atmosphere. The progress of the reaction was monitored by thin layer chromatography (TLC) during the reaction. Upon completion of the reaction, the reaction mixture was filtered through a diatomaceous earth pad to remove the catalyst. The filtrate was concentrated under reduced pressure to afford the target product 1-(4-aminophenyl)piperazine (319 mg, 90.0% yield).
References
[1] Synthetic Communications, 2012, vol. 42, # 2, p. 213 - 222
[2] RSC Advances, 2015, vol. 5, # 113, p. 93433 - 93437
[3] Green Chemistry, 2017, vol. 19, # 14, p. 3400 - 3407
[4] Tetrahedron Letters, 1999, vol. 40, # 31, p. 5655 - 5659
[5] Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, 2011, vol. 41, # 1, p. 114 - 119
4-PIPERAZIN-1-YL-PHENYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
4-PIPERAZIN-1-YL-PHENYLAMINE Suppliers
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- --
- Fax
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- info@chemstep.com
- Country
- Europe
- ProdList
- 6143
- Advantage
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View Lastest Price from 4-PIPERAZIN-1-YL-PHENYLAMINE manufacturers
- Product
- 1-(4-Aminophenyl)piperazine 67455-41-8
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27