BOC-D-ABU-OH
- Product Name
- BOC-D-ABU-OH
- CAS No.
- 45121-22-0
- Chemical Name
- BOC-D-ABU-OH
- Synonyms
- BOC-D-ABU;BOC-D-ABU-OH;BOC-D-2-ABU-OH;BOC-D-ABU(2)-OH;BOC-D-ALPHA-ABU-OH;BOC-D-ABU(ALPHA)-OH;BOC-D-ABU-OH USP/EP/BP;BOC-D-AMINOBUTYRIC ACID;BOC-D-NHCH(CH2CH3)-COOH;BOC-D-2-AMINOBUTYRIC ACID
- CBNumber
- CB9690640
- Molecular Formula
- C9H17NO4
- Formula Weight
- 203.24
- MOL File
- 45121-22-0.mol
BOC-D-ABU-OH Property
- Boiling point:
- 334.5±25.0 °C(Predicted)
- Density
- 1.101
- storage temp.
- Sealed in dry,2-8°C
- solubility
- Soluble in DMF (1mmol in 1ml DMF).
- form
- Liquid
- pka
- 4.00±0.10(Predicted)
- color
- Yellow
Safety
- HazardClass
- IRRITANT
- HS Code
- 2924190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 265235
- Product name
- Boc-D-a-aminobutyric acid
- Packaging
- 2g
- Price
- $353
- Updated
- 2021/12/16
- Product number
- 041454
- Product name
- Boc-D-Abu-OH
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
- Product number
- B252
- Product name
- Boc-D-2-aminobutanoicacid
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
- Product number
- 11351
- Product name
- Boc-D-a-aminobutyricacid,≥98%(HPLC)
- Purity
- ≥98%(HPLC)
- Packaging
- 1G
- Price
- $17.47
- Updated
- 2021/12/16
- Product number
- 041454
- Product name
- Boc-D-Abu-OH
- Packaging
- 5g
- Price
- $29
- Updated
- 2021/12/16
BOC-D-ABU-OH Chemical Properties,Usage,Production
Chemical Properties
White powder
Uses
(R)-2-(Boc-amino)butyric acid is used in coupling reaction. Also used in preparation of dyes.
Synthesis
2623-91-8
24424-99-5
45121-22-0
[Step 1] Synthesis of (R)-2-((tert-butoxycarbonyl)amino)butanoic acid Di-tert-butyl dicarbonate (4.7 g, 21 mmol) was slowly added to a mixed solution of (R)-2-aminobutyric acid (2.0 g, 19 mmol) and sodium bicarbonate (1.6 g, 19 mmol) in a mixture of 1,4-dioxane and water (3:10 v/v/v, total 26 mL) under ice bath cooling. The reaction mixture was stirred at room temperature for 120 hours and then concentrated under reduced pressure. The resulting crude product was dissolved in chloroform, to which 1N hydrochloric acid was subsequently added and extracted with chloroform. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 2.0 g (quantitative yield) of the title compound (hereinafter referred to as Reference Example Compound 27).
References
[1] Patent: EP2832724, 2015, A1. Location in patent: Paragraph 0169
[2] European Journal of Organic Chemistry, 2002, # 23, p. 3995 - 4004
[3] Journal of the American Chemical Society, 1997, vol. 119, # 4, p. 656 - 673
[4] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 22, p. 3237 - 3242
[5] Tetrahedron, 2006, vol. 62, # 42, p. 9966 - 9972
BOC-D-ABU-OH Preparation Products And Raw materials
Raw materials
Preparation Products
BOC-D-ABU-OH Suppliers
- Tel
- --
- Fax
- --
- Country
- Japan
- ProdList
- 4811
- Advantage
- 42
View Lastest Price from BOC-D-ABU-OH manufacturers
- Product
- BOC-D-ABU-OH 45121-22-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-10-09
- Product
- BOC-D-ABU-OH 45121-22-0
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2018-12-22