7-METHOXY-ISOQUINOLINE

Uses

Product Name: 7-METHOXY-ISOQUINOLINE
CAS No.: 39989-39-4
Chemical Name: 7-METHOXY-ISOQUINOLINE
Synonyms: 7-METHOXY-ISOQUINOLINE;Isoquinoline, 7-methoxy-;7-Methoxyisoquinoline 96%;7-Methoxy-2-azanaphthalene;7-Methoxyisoquinoline - [M9820];7-METHOXY-ISOQUINOLINE ISO 9001：2015 REACH
CBNumber: CB9828663
Molecular Formula: C10H9NO
Formula Weight: 159.18
MOL File: 39989-39-4.mol

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7-METHOXY-ISOQUINOLINE Property

Melting point:: 49°C
Boiling point:: 284.68°C (rough estimate)
Density: 1.1202 (rough estimate)
refractive index: 1.6070 (estimate)
storage temp.: Sealed in dry,Room Temperature
pka: 5.54±0.10(Predicted)
Appearance: Off-white to light brown Solid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
Hazard Note: Irritant
HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M268545
Product name: 7-Methoxyisoquinoline
Packaging: 100mg
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4656-1-Z8
Product name: 7-Methoxyisoquinoline
Packaging: 1g
Price: $77
Updated: 2021/12/16

Matrix Scientific

Product number: 188671
Product name: 7-Methoxyisoquinoline
Packaging: 5g
Price: $413
Updated: 2021/12/16

AK Scientific

Product number: Y5421
Product name: 7-Methoxyisoquinoline
Packaging: 10g
Price: $537
Updated: 2021/12/16

Matrix Scientific

Product number: 188671
Product name: 7-Methoxyisoquinoline
Packaging: 10g
Price: $660
Updated: 2021/12/16

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7-METHOXY-ISOQUINOLINE Chemical Properties,Usage,Production

Uses

7-Methoxyisoquinoline is a useful research chemical for organic synthesis and other chemical processes.

Synthesis

591-31-1

22483-09-6

407-25-0

39989-39-4

General steps: 1. dissolve 60.8 mL of 3-methoxybenzaldehyde in 600 mL of toluene and add 81.9 mL of aminoacetaldehyde dimethyl acetal. 2. Install a Dean-Stark manifold and reflux the reaction mixture for 5 hours, followed by cooling to 5 °C. 3. 209 mL of trifluoroacetic anhydride and 185 mL of boron trifluoride ether compound were slowly added dropwise under nitrogen protection, with the rate of dropwise acceleration controlled to maintain the reaction temperature below 10 °C. The reaction temperature was then increased to 10 °C. The reaction temperature was then increased to 10 °C. 4. After the dropwise addition was completed, the reaction mixture was continued to be stirred at room temperature for 3 days. 5. The reaction mixture was slowly poured into ice water, 250 mL of 2N hydrochloric acid was added, and the organic layer was extracted with 1N hydrochloric acid. 6. Combine the aqueous phases and adjust the pH to 9 with concentrated ammonia. 7. extracted the aqueous phase with ethyl acetate, combined the organic phases, dried and concentrated the solvent under reduced pressure. 8. 66.9 g (84% yield) of 7-methoxyisoquinoline was obtained as a light brown oil. EI-MS: 159 (M+).

References

[1] Patent: US6194409, 2001, B1

7-METHOXY-ISOQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-METHOXY-ISOQUINOLINE Suppliers

China 97 Germany 1 India 2 United Kingdom 2 United States 12 Global 114

HBCChem, Inc.

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ChemPacific Corporation

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View Lastest Price from 7-METHOXY-ISOQUINOLINE manufacturers

Career Henan Chemical Co

Product: 7-METHOXY-ISOQUINOLINE 39989-39-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: G/KG/T
Release date: 2019-12-24

39989-39-4, 7-METHOXY-ISOQUINOLINERelated Search:

7-methoxyquinoline 7-Methoxy-1H-indole 7-methoxyindoline-2,3-dione 6,7-DIMETHOXYISOQUINOLINE 7-Hydroxy-6-methoxy-3,4-dihydroisoquinoline 6,7-DIMETHOXY-1-(3,4,5-TRIETHOXYPHENYL)ISOQUINOLINE CORALYNE CHLORIDE HYDRATE, 98+% BERBERINE SULFATE TRIHYDRATE Coptisine chloride BERBERINE CHLORIDE CHELERYTHRINE CHLORIDE BERBERINE ACID SULFATE SANGUINARINE CHLORIDE Papaverine hydrochloride R-Tetrahydropapaverine N-acetyl-L-leucinate 5-methoxyisoquinoline 3,4-Dihydro-6-methoxyisoquinoline hydrochloride 1-Methyl-6-methoxyisoquinolinol

7-Methoxyisoquinoline 96%

7-METHOXY-ISOQUINOLINE

7-Methoxy-2-azanaphthalene

Isoquinoline, 7-methoxy-

7-METHOXY-ISOQUINOLINE ISO 9001：2015 REACH

7-Methoxyisoquinoline - [M9820]

39989-39-4

blocks

Heterocycles

Quinolines

Quinoline&Isoquinoline