Basic information Safety Supplier Related

1-METHOXY-4-NITRONAPHTHALENE

Basic information Safety Supplier Related

1-METHOXY-4-NITRONAPHTHALENE Basic information

Product Name:
1-METHOXY-4-NITRONAPHTHALENE
Synonyms:
  • 1-METHOXY-4-NITRONAPHTHALENE
  • 4-Methoxy-1-nitronaphthalene
  • 1-Methoxy-4-nitronaphthalene,99%
  • 1-Methoxy-4-nitronaphthalene 99%
  • 1-Methoxy-4-nitronaphthalin
  • 1-Nitro-4-methoxynaphthalene
  • methyl4-nitronaphthylether
  • Naphthalene,1-methoxy-4-nitro-
CAS:
4900-63-4
MF:
C11H9NO3
MW:
203.19
EINECS:
225-528-0
Product Categories:
  • Naphthalene derivatives
  • Nitro Compounds
  • Nitrogen Compounds
  • Organic Building Blocks
Mol File:
4900-63-4.mol
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1-METHOXY-4-NITRONAPHTHALENE Chemical Properties

Melting point:
83-85 °C (lit.)
Boiling point:
341.49°C (rough estimate)
Density 
1.2621 (rough estimate)
refractive index 
1.4950 (estimate)
storage temp. 
Sealed in dry,Room Temperature
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39
WGK Germany 
3

MSDS

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1-METHOXY-4-NITRONAPHTHALENE Usage And Synthesis

Chemical Properties

yellow to orange crystalline powder

Uses

1-Methoxy-4-nitronaphthalene is used as a reagent in the synthesis of UMI-77 (U700850); a small molecule inhibitor of Mcl-1 which blocks and attenuates pancreatic cell cancer growth. Also an anticancer agent.

Synthesis Reference(s)

Synthesis, p. 70, 1985 DOI: 10.1055/s-1985-31110

Purification Methods

Purify it by chromatography on silica gel, then recrystallise it from MeOH or EtOH (yellow needles). [Hodgson & Habeshaw J Chem Soc 47 1942, Bunce et al. J Org Chem 52 4214 1987, Beilstein 6 H 616, 6 III 2938.]

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