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(Carbethoxymethyl)triphenylphosphonium bromide

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(Carbethoxymethyl)triphenylphosphonium bromide Basic information

Product Name:
(Carbethoxymethyl)triphenylphosphonium bromide
Synonyms:
  • (Carboxymethyl)triphenylphosphonium bromide ethyl ester
  • NSC 60450
  • (Ethoxycarbonylmethyl)triphenylphosphonium bromide 98%
  • (ethoxycarbonylmethyl)triphenyl-phosphoniubromide
  • (CarbethoxyMethyl)triphenylpho
  • Ethoxycarbonyltriphenylphosphoniumbromide
  • (CARBETHOXYMETHYL)TRIPHENYLPHOSP
  • (Carbethoxymethyl)tr...
CAS:
1530-45-6
MF:
C22H22BrO2P
MW:
429.29
EINECS:
216-230-1
Product Categories:
  • Phosphonium Compounds
  • Synthetic Organic Chemistry
  • Wittig & Horner-Emmons Reaction
  • Wittig Reaction
  • C-C Bond Formation
  • Olefination
  • Wittig Reagents
Mol File:
1530-45-6.mol
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(Carbethoxymethyl)triphenylphosphonium bromide Chemical Properties

Melting point:
145-150 °C (dec.) (lit.)
storage temp. 
Inert atmosphere,Room Temperature
solubility 
Chloroform (Slightly), Methanol (Slightly)
form 
Crystalline Powder
color 
White
Water Solubility 
It is soluble in water.
Sensitive 
Hygroscopic
BRN 
3581273
CAS DataBase Reference
1530-45-6(CAS DataBase Reference)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36-24/25
WGK Germany 
3
RTECS 
TA2299500
9
HS Code 
29310095

MSDS

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(Carbethoxymethyl)triphenylphosphonium bromide Usage And Synthesis

Chemical Properties

WHITE CRYSTALLINE POWDER

Uses

suzuki reaction

Uses

(Ethoxycarbonylmethyl)triphenylphosphonium bromide, is used as a pharmaceutical intermediate.

Purification Methods

Wash it with pet ether (b 40-50o) and recrystallise it from CHCl3/Et2O and dry it in a high vacuum at 65o. [Isler et al. Helv Chim Acta 40 1242 1957, Wittig & Haag Chem Ber 88 1654, 1664 1955.]

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