METHYL 4-AMINO-3-CHLOROBENZOATE
- Product Name
- METHYL 4-AMINO-3-CHLOROBENZOATE
- CAS No.
- 84228-44-4
- Chemical Name
- METHYL 4-AMINO-3-CHLOROBENZOATE
- Synonyms
- AKOS BB-3098;TIMTEC-BB SBB003712;METHYL 4-AMINO-3-CHLOROBENZOATE;Methyl4-amino-3-chlorobenzoate98%;Methyl 4-AMino-3-Chloro Benzonate;Methyl 4-amino-3-chlorobenzoate 98%;2-Chloro-4-(methoxycarbonyl)aniline;Methyl 4-amino-3-chlorobenzoate,97%;Methyl 4-amino-3-chlorophenylacetate;Methyl 4-aMino-3-chlorobenzoate, 97% 5GR
- CBNumber
- CB1302093
- Molecular Formula
- C8H8ClNO2
- Formula Weight
- 185.61
- MOL File
- 84228-44-4.mol
METHYL 4-AMINO-3-CHLOROBENZOATE Property
- Melting point:
- 107-111 °C
- Boiling point:
- 321.6±22.0 °C(Predicted)
- Density
- 1.2797 (rough estimate)
- refractive index
- 1.5560 (estimate)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 0.52±0.10(Predicted)
- form
- Crystalline Powder
- color
- Beige-brown
- CAS DataBase Reference
- 84228-44-4(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 655902
- Product name
- Methyl 4-amino-3-chlorobenzoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $73.9
- Updated
- 2023/06/20
- Product number
- 655902
- Product name
- Methyl 4-amino-3-chlorobenzoate
- Purity
- 97%
- Packaging
- 5g
- Price
- $215
- Updated
- 2023/06/20
- Product number
- M2698
- Product name
- Methyl 4-Amino-3-chlorobenzoate
- Purity
- >97.0%(GC)
- Packaging
- 1g
- Price
- $45
- Updated
- 2025/07/31
- Product number
- M2698
- Product name
- Methyl 4-Amino-3-chlorobenzoate
- Purity
- >97.0%(GC)
- Packaging
- 5g
- Price
- $157
- Updated
- 2025/07/31
- Product number
- M331928
- Product name
- Methyl 4-Amino-3-chlorobenzoate
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
METHYL 4-AMINO-3-CHLOROBENZOATE Chemical Properties,Usage,Production
Chemical Properties
beige-brown crystals or crystalline powder
Synthesis
67-56-1
2486-71-7
84228-44-4
Concentrated sulfuric acid (2.00 mL) was added slowly and dropwise to a stirred solution of 3-chloro-4-aminobenzoic acid (2.00 g, 11.7 mmol) in methanol (20.0 mL) at 0 °C. The reaction mixture was warmed to 80 °C and kept stirring for 6 hours. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently concentrated under reduced pressure. The concentrated residue was diluted with saturated aqueous sodium bicarbonate and extracted with ethyl acetate (2 x 50 mL). The organic phases were combined, washed with saturated brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give methyl 4-amino-3-chlorobenzoate (2.10 g, 97% yield). The product was confirmed by NMR hydrogen spectroscopy (400 MHz, DMSO-d6): δ 7.70 (d, J = 1.6Hz, 1H), 7.58 (dd, J = 8.4, 2.0Hz, 1H), 6.77 (d, J = 8.8Hz, 1H), 6.24 (s, 2H), 3.73 (s, 3H).
References
[1] Patent: WO2011/128251, 2011, A1. Location in patent: Page/Page column 203
[2] Patent: US2011/257151, 2011, A1. Location in patent: Page/Page column 75
[3] Patent: WO2018/157190, 2018, A1. Location in patent: Paragraph 0337
[4] Journal of Cellular Biochemistry, 2017, vol. 118, # 8, p. 2420 - 2429
[5] Journal of Medicinal Chemistry, 2018, vol. 61, # 3, p. 666 - 680
METHYL 4-AMINO-3-CHLOROBENZOATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from METHYL 4-AMINO-3-CHLOROBENZOATE manufacturers
- Product
- METHYL 4-AMINO-3-CHLOROBENZOATE 84228-44-4
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11
- Product
- METHYL 4-AMINO-3-CHLOROBENZOATE 84228-44-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-12