4-Amino-N-methylbenzamide
- Product Name
- 4-Amino-N-methylbenzamide
- CAS No.
- 6274-22-2
- Chemical Name
- 4-Amino-N-methylbenzamide
- Synonyms
- 4-(Methylc;4-Amino-N<;4-Amino-N-methylbenz;4-Amino-N-methylbenzamide;4-Aminobenzoylmethylamide;4-(Methylcarbamoyl)aniline;Benzamide, 4-amino-N-methyl-;4-Amino-N-methylbenzamide >4-Amino-N-methylbenzamide 98%;4-Amino-N-methylbenzamide
- CBNumber
- CB21054022
- Molecular Formula
- C8H10N2O
- Formula Weight
- 150.18
- MOL File
- 6274-22-2.mol
4-Amino-N-methylbenzamide Property
- Melting point:
- 181 °C
- Boiling point:
- 364.1±25.0 °C(Predicted)
- Density
- 1.137
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 15.84±0.46(Predicted)
- color
- White to Light yellow to Light orange
- CAS DataBase Reference
- 6274-22-2(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 29242990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- A2064
- Product name
- 4-Amino-N-methylbenzamide
- Purity
- >98.0%(GC)(T)
- Packaging
- 1g
- Price
- $16
- Updated
- 2025/07/31
- Product number
- A2064
- Product name
- 4-Amino-N-methylbenzamide
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $23
- Updated
- 2025/07/31
- Product number
- M328590
- Product name
- N-Methyl4-Aminobenzamide
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 025850
- Product name
- 4-Amino-N-methylbenzamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
- Product number
- 025850
- Product name
- 4-Amino-N-methylbenzamide
- Purity
- 97%
- Packaging
- 5g
- Price
- $14
- Updated
- 2021/12/16
4-Amino-N-methylbenzamide Chemical Properties,Usage,Production
Synthesis
Ammonium chloride (29.6 g, 55.4 mmol) in water (200 mL) and methanol (200 mL) was added to a solution of N-methyl-4-nitro-benzamide (10 g, 55.4 mmol) in THF (160 mL). Zinc powder (29 g, 44.4 mmol) was added portion wise and the mixture stirred for 15 minutes. The reaction mixture was filtered over celite, the filtrate was then concentrated and extracted with ethyl acetate. The organics were washed with brine solution, dried over Na2SO4 and concentrated to afford 7.2 g (86percent) of 4-Amino-N-methylbenzamide. 1H NMR: (DMSO-d6): δ 7.9 (s, 1H), 7.6 (d, 2H), 6.5 (d, 2H), 5.6 (s, 2H), 2.7 (s, 3H).
References
[1] Patent: US2009/239848, 2009, A1. Location in patent: Page/Page column 24
[2] Patent: WO2010/133672, 2010, A1. Location in patent: Page/Page column 30
[3] Journal of Chemical Research, 2006, # 4, p. 223 - 224
[4] Journal of Medicinal Chemistry, 1984, vol. 27, # 6, p. 779 - 782
[5] Journal of the American Chemical Society, 1938, vol. 60, p. 1081
4-Amino-N-methylbenzamide Preparation Products And Raw materials
Raw materials
Preparation Products
4-Amino-N-methylbenzamide Suppliers
- Tel
- --
- Fax
- --
- enamine@enamine.net
- Country
- Ukraine
- ProdList
- 6216
- Advantage
- 67
View Lastest Price from 4-Amino-N-methylbenzamide manufacturers
- Product
- 4-Amino-N-methylbenzamide 6274-22-2
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-11-22
- Product
- 4-Amino-N-methylbenzamide 6274-22-2
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 0.99
- Supply Ability
- 20tons
- Release date
- 2023-10-12
- Product
- 4-Amino-N-methylbenzamide 6274-22-2
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 95%-99%
- Supply Ability
- as request
- Release date
- 2018-12-24