Uses
ChemicalBook > CAS DataBase List > 5-Bromo-2-pyridinecarboxylic Acid

5-Bromo-2-pyridinecarboxylic Acid

Uses
Product Name
5-Bromo-2-pyridinecarboxylic Acid
CAS No.
30766-11-1
Chemical Name
5-Bromo-2-pyridinecarboxylic Acid
Synonyms
METHYL 5-BROMOPICOLINATE;5-BROMOPICOLINIC ACID;5-BROMOPYRIDINE-2-CARBOXYLIC ACID METHYL ESTER;5-bromoisonicotinic acid;5-bromo-2-picolonic acid;5-bromopyridine-2-carboxylate;5-Bromopyridine-2-carboxylicaci;5-bromo-2-pyridinecarboxlic acid;5-Bromopyridine-2-carboxylic acid;5-bromo-2-pyridine carboxlic acid
CBNumber
CB2200633
Molecular Formula
C6H4BrNO2
Formula Weight
202.01
MOL File
30766-11-1.mol
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5-Bromo-2-pyridinecarboxylic Acid Property

Melting point:
173-175°C
Boiling point:
319.5±27.0 °C(Predicted)
Density 
1.813±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
Soluble in methanol.
form 
Powder
pka
3.41±0.10(Predicted)
color 
White to off-white
InChI
InChI=1S/C6H4BrNO2/c7-4-1-2-5(6(9)10)8-3-4/h1-3H,(H,9,10)
InChIKey
MNNQIBXLAHVDDL-UHFFFAOYSA-N
SMILES
C1(C(O)=O)=NC=C(Br)C=C1
CAS DataBase Reference
30766-11-1(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
24/25-36-26-37/39
HazardClass 
IRRITANT
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B3188
Product name
5-Bromo-2-pyridinecarboxylic Acid
Purity
>97.0%(GC)(T)
Packaging
1g
Price
$34
Updated
2025/07/31
TCI Chemical
Product number
B3188
Product name
5-Bromo-2-pyridinecarboxylic Acid
Purity
>97.0%(GC)(T)
Packaging
5g
Price
$113
Updated
2025/07/31
TRC
Product number
B686618
Product name
5-BromopicolinicAcid
Packaging
1g
Price
$55
Updated
2021/12/16
TRC
Product number
B686618
Product name
5-BromopicolinicAcid
Packaging
2.5g
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB07708
Product name
5-Bromopyridine-2-carboxylic acid
Packaging
100g
Price
$81
Updated
2021/12/16
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5-Bromo-2-pyridinecarboxylic Acid Chemical Properties,Usage,Production

Uses

5-Bromopyridine-2-carboxylic acid is used as a pharmaceutical intermediate. Store in cool, dry place in a well sealed container. Store away from oxidizing agents.

Chemical Properties

white Cryst

Uses

5-Bromopyridine-2-carboxylic acid is used as a pharmaceutical intermediate.

Synthesis

3430-13-5

30766-11-1

4.1.7 Synthesis of 5-bromopyridine-2-carboxylic acid (11): In a 250 mL three-necked flask assembled with a stirrer, thermometer, and condenser tube, add 150 mL of water and 5-bromo-2-methylpyridine (10) (6.0 g, 35 mmol). After turning on the stirring and heating to 80 °C, potassium permanganate (KMnO4) (24.8 g, 157 mmol) was added in three batches at 1 h intervals. The reaction temperature was maintained at 80 °C and stirring was continued for 3-4 hours. Upon completion of the reaction, filtration was carried out to obtain a clarified filtrate. The pH of the filtrate was adjusted to 4-5 with concentrated hydrochloric acid, at which point a white solid precipitated. The filtrate was filtered to collect a small amount of product (11). The filtrate was concentrated under vacuum and an appropriate amount of ethanol was added to the residue to dissolve compound (11), at which time a large amount of white solid precipitated, the filtrate was again withdrawn and the solid discarded. Finally, the filtrate was concentrated under vacuum to give a light yellow solid product (11) (3.0 g, 39% yield).

References

[1] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 13, p. 3228 - 3236
[2] Journal fuer Praktische Chemie (Leipzig), 1932, vol. <2> 133, p. 36,49
[3] Heterocycles, 1981, vol. 15, # 1, p. 213 - 223
[4] Synthesis, 2003, # 4, p. 551 - 554
[5] Patent: US2005/113374, 2005, A1. Location in patent: Page/Page column 8

5-Bromo-2-pyridinecarboxylic Acid Preparation Products And Raw materials

Raw materials

Copper(I) Cyanide Hexane N,N-Dimethylformamide Ethyl chloroformate 2,5-Dibromopyridine n-Butyllithium

Preparation Products

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View Lastest Price from 5-Bromo-2-pyridinecarboxylic Acid manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
5-Bromo-2-pyridinecarboxylic Acid 30766-11-1
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99.0%
Supply Ability
10000KGS
Release date
2025-05-29
Hebei Chuanghai Biotechnology Co., Ltd
Product
5-Bromopyridine-2-carboxylic acid 30766-11-1
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-22
Henan Aochuang Chemical Co.,Ltd.
Product
5-Bromopyridine-2-carboxylic acid 30766-11-1
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-10-10

30766-11-1, 5-Bromo-2-pyridinecarboxylic AcidRelated Search:

Quinolinic acid 2-Chloro-3-cyanopyridine EPA 1-Hexadecylpyridinium bromide 2,6-Lutidine 2,5-PYRIDINEDICARBOXYLIC ACID Chromium picolinate 2-Picolinic acid 5-Bromo-2-iodobenzoic acid 6-BROMOPYRIDINE-2-CARBOXYLIC ACID 6-BROMOPYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER 6-ACETAMIDO-3-BROMOPYRIDINE-2-CARBOXYLIC ACID 96%6-ACETAMIDO-3-BROMOPICOLINIC ACID 6-BROMO-3-PYRIDAZINECARBOXYLIC ACID 5-BROMOPYRIDINE-3-CARBOXYLIC ACID HYDRAZIDE 4-BROMOPYRIDINE-2-CARBOXYLIC ACID,4-Bromopyridine-2-carboxylic acid 97% 2-BROMOPYRIDINE-5-CARBOXYLIC ACID,6-BROMOPYRIDINE-3-CARBOXYLIC ACID 6-BROMOPYRIDINE-2-CARBOXYLIC ACID METHYL ESTER,6-BROMOPYRIDINE-2-CARBOXYLIC ACID METHYL ESTER Methyl 5-bromonicotinate

  • METHYL 5-BROMOPICOLINATE
  • METHYL 5-BROMO-2-PYRIDINECARBOXYLATE
  • 5-BROMOPYRIDINE-2-CARBOXYLIC ACID METHYL ESTER
  • 5-bromo-2-pyridine carboxlic acid
  • 5-bromo-2-pyridinecarboxlic acid
  • 5-Bromopyridine-2-carboxylic acid
  • 5-bromoisonicotinic acid
  • 5-Bromopyridine-2-carboxylic acid ,98%
  • 5-BROMO-2-PICOLINIC ACID5-BROMO-2-PYRIDINECARBOXYLIC ACID
  • 5-Bromo-2-pyridinecaroboxylic acid
  • 5-Bromopicolinic acid, 5-Bromo-2-carboxypyridine
  • 5-Bromo-2-pyridinecarboxylic Acid &gt
  • 5-Bromopyridine-2-carboxylicaci
  • 5-Bromopyiridine-2-carboxylic acid
  • 5-bromopyridine-2-carboxylate
  • 5-BROMOPICOLINIC ACID
  • 5-bromo-2-picolonic acid
  • 5-BROMO-2-PYRIDINECARBOXYLIC ACID
  • 5-Bromopyridine-2-carboxylic acid, 96%
  • 30766-11-1
  • 29681-15-3
  • C6H4B2NO2
  • Carboxylic Acids
  • Carboxy
  • Organohalides
  • Bromopyridines
  • Halopyridines
  • Pyridine Series
  • Carboxylic Acids
  • pharmacetical
  • Pyridines, Pyrimidines, Purines and Pteredines
  • blocks
  • Bromides
  • Carboxes
  • Pyridines
  • Pyridine
  • bc0001