Synthesis
ChemicalBook > CAS DataBase List > 2-Amino-5-iodobenzoic acid

2-Amino-5-iodobenzoic acid

Synthesis
Product Name
2-Amino-5-iodobenzoic acid
CAS No.
5326-47-6
Chemical Name
2-Amino-5-iodobenzoic acid
Synonyms
TIMTEC-BB SBB001006;5-iodoanthranil acid;5-Iodoanthanilic acid;5-iodo-anthranilicaci;2-Amino-5-iodobenzoic;5-IODOANTHRANILIC ACID;5-Iodoanthranillic acid;5-IodoanthranilicAcid>5-lodo anthranillic acid;2-amino-5-iodo-benzoicaci
CBNumber
CB2207900
Molecular Formula
C7H6INO2
Formula Weight
263.03
MOL File
5326-47-6.mol
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2-Amino-5-iodobenzoic acid Property

Melting point:
219-221 °C (dec.) (lit.)
Boiling point:
383.2±37.0 °C(Predicted)
Density 
1.8886 (estimate)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
DMSO (Slightly), Methanol (Slightly)
pka
4.59±0.10(Predicted)
form 
Crystalline Powder
color 
Beige or gray to purple
Water Solubility 
Soluble in alcohol. Insoluble in water.
Sensitive 
Light Sensitive
BRN 
639029
InChI
InChI=1S/C7H6INO2/c8-4-1-2-6(9)5(3-4)7(10)11/h1-3H,9H2,(H,10,11)
InChIKey
GOLGILSVWFKZRQ-UHFFFAOYSA-N
SMILES
C(O)(=O)C1=CC(I)=CC=C1N
CAS DataBase Reference
5326-47-6(CAS DataBase Reference)
EPA Substance Registry System
5-Iodoanthranilic acid (5326-47-6)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36-37/39
WGK Germany 
3
RTECS 
DG2802000
Hazard Note 
Irritant
TSCA 
T
HazardClass 
IRRITANT, LIGHT SENSITIVE
HS Code 
29224995
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
A59603
Product name
2-Amino-5-iodobenzoic acid
Purity
97%
Packaging
5g
Price
$68.8
Updated
2023/06/20
Sigma-Aldrich
Product number
A59603
Product name
2-Amino-5-iodobenzoic acid
Purity
97%
Packaging
25g
Price
$160
Updated
2023/06/20
TCI Chemical
Product number
I0049
Product name
5-Iodoanthranilic Acid
Purity
>98.0%(T)
Packaging
5g
Price
$30
Updated
2025/07/31
TCI Chemical
Product number
I0049
Product name
5-Iodoanthranilic Acid
Purity
>98.0%(T)
Packaging
25g
Price
$98
Updated
2025/07/31
TRC
Product number
A630513
Product name
2-Amino-5-iodobenzoic acid
Packaging
5g
Price
$70
Updated
2021/12/16
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2-Amino-5-iodobenzoic acid Chemical Properties,Usage,Production

Synthesis

To the mixture of 2.89 g (18.2 mmol) sodium 2- aminobenzoate, 40 mL acetic acid and 2.31 g (9.1 mmol) molecular iodine, 5 mL (44.1 mmol, 30 wt %) aqueous hydrogen peroxide was added drop wise. The S3 reaction mixture was stirred at 50 °C for 3 h and poured into 400 mL water. The formed crystals were filtered and recrystallized from benzene to give 2-azido-5- iodobenzoic acid . IR (suspension in nujol, cm−1 ): 3500, 3387, 1670, 1612, 1580, 1541, 1419, 1377, 1319, 1290, 1163, 1125, 813, 688, 619.

Chemical Properties

white to light yellow crystal powder

Uses

2-Amino-5-iodobenzoic acid is used in wide range of medicals industrial applications as well as in human and animal nutrition products such as pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals.

reaction suitability

reaction type: solution phase peptide synthesis

References

[1] Tetrahedron Letters, 2006, vol. 47, # 28, p. 4793 - 4796
[2] Synlett, 2014, vol. 25, # 1, p. 148 - 152
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006, vol. 45, # 11, p. 2558 - 2565
[4] Medicinal Chemistry Research, 2016, vol. 25, # 6, p. 1125 - 1139
[5] Synthetic Communications, 2008, vol. 38, # 11, p. 1792 - 1798

2-Amino-5-iodobenzoic acid Preparation Products And Raw materials

Raw materials

Potassium hydroxide Sodium bisulfite Iodine chloride solution (Wijs' chloride) Iodine Acetic acid Iodine monochloride Anthranilic acid

Preparation Products

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View Lastest Price from 2-Amino-5-iodobenzoic acid manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
2-Amino-5-iodobenzoic acid 5326-47-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1ton
Release date
2022-10-10
Hebei Chuanghai Biotechnology Co., Ltd
Product
2-Amino-5-iodobenzoic acid 5326-47-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
5tons
Release date
2025-03-14
Hebei Chuanghai Biotechnology Co,.LTD
Product
2-Amino-5-iodobenzoic acid 5326-47-6
Price
US $5.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-21

5326-47-6, 2-Amino-5-iodobenzoic acidRelated Search:

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  • TIMTEC-BB SBB001006
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  • 2-Amino-5-iodobenzoic acid,98%
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  • 5-Iodo anthranilic acid [5-Iodo-2-amino benzoic acid]
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  • 2-Amino-5-iodobenzoic acid, 96%
  • 2-Amino-5-iodobenzoic
  • 5326-47-6
  • 26-47-6
  • H2NC6H3ICO2H
  • C7H6INO2
  • C7H6NO2I
  • C7H5INO2
  • Peptide Synthesis
  • Specialty Synthesis
  • Unnatural Amino Acid Derivatives
  • Aromatic Amino Acids
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
  • Carboxylic Acids
  • Phenyls & Phenyl-Het
  • Benzoic acid
  • Organic acids
  • API intermediates
  • Acids & Esters
  • Anilines, Amides & Amines
  • Iodine Compounds
  • Carboxylic Acids
  • Phenyls & Phenyl-Het