ChemicalBook > CAS DataBase List > 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

Product Name: 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride
CAS No.: 57196-62-0
Chemical Name: 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride
Synonyms: 6-Methoxy-1,2,3,4-tetrahydrois;6-METHOXY-1,2,3,4-TETRAHYDROISOQUINOLINE HCL;ISOQUINOLINE 1,2,3,4-TETRAHYDRO-6-METHOXY HCL SALT;6-METHOXY-1,2,3,4-TETRAHYDROISOQUINOLINE HYDROCHLORIDE;1,2,3,4-tetrahydro-6-methoxyisoquinoline hydrochloride;6-Methoxy-1,2,3,4-tetraihydroisoquinoline hydrochloride;6-Methoxy-1,2,3,4-tetrahydroisoquinolinehydrochloride,95%;Isoquinoline, 1,2,3,4-tetrahydro-6-Methoxy-, hydrochloride;Isoquinoline,1,2,3,4-tetrahydro-6-methoxy-,hydrochloride(1:1);Better offer for 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride
CBNumber: CB2501596
Molecular Formula: C10H14ClNO
Formula Weight: 199.68
MOL File: 57196-62-0.mol

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6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride Property

Melting point:: 230-232.5°C
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
Appearance: White to off-white Solid
CAS DataBase Reference: 57196-62-0

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22-51
HazardClass: IRRITANT
HS Code: 2933491090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M268803
Product name: 6-Methoxy-1,2,3,4-tetrahydroisoquinolineHydrochloride
Packaging: 500mg
Price: $110
Updated: 2021/12/16

TRC

Product number: M268803
Product name: 6-Methoxy-1,2,3,4-tetrahydroisoquinolineHydrochloride
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M268803
Product name: 6-Methoxy-1,2,3,4-tetrahydroisoquinolineHydrochloride
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Ark Pharm

Product number: P000066897
Product name: 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride
Purity: 97%
Packaging: 250mg
Price: $9
Updated: 2021/12/16

AK Scientific

Product number: J96311
Product name: 6-Methoxy-1,2,3,4-tetrahydroisoquinolinehydrochloride
Packaging: 250mg
Price: $18
Updated: 2021/12/16

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6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride Chemical Properties,Usage,Production

Synthesis

50-00-0

55-81-2

57196-62-0

To a stirred suspension of 4-methoxyphenethylamine (50.4 g, 0.33 mol, 1.0 eq.) in water (40 mL) was slowly added 37% aqueous formaldehyde (27.5 mL, 1.1 eq.) with continuous stirring for 20 minutes. Subsequently, concentrated hydrochloric acid (80 mL) was added dropwise to the reaction mixture and the mixture was heated to reflux and maintained for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated to dryness in a rotary evaporator. The resulting residue was purified by recrystallization from acetone to afford 6-methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride as a white solid (60.1 g, 90% yield). The product did not require further purification and could be used directly in the subsequent reaction. Mass spectrometry analysis showed that the MH+ peak was located at 164.

References

[1] Patent: WO2003/99786, 2003, A2. Location in patent: Page 35

6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride Preparation Products And Raw materials

Raw materials

Ethanol (3-Methoxyphenyl)acetonitrile Paraformaldehyde Tetrahydrofuran Lithium Aluminum Hydride Hydrochloric acid

Preparation Products

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View Lastest Price from 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride 57196-62-0
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-09-28

Career Henan Chemical Co

Product: 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride 57196-62-0
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000kgs
Release date: 2020-01-09

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Better offer for 6-Methoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride

57196-62-0

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