ChemicalBook > CAS DataBase List > 3-IODO-4-METHOXYANILINE

3-IODO-4-METHOXYANILINE

Product Name
3-IODO-4-METHOXYANILINE
CAS No.
74587-12-5
Chemical Name
3-IODO-4-METHOXYANILINE
Synonyms
3-Iodo-p-anisidine;4-Amino-2-iodoanisole;3-IODO-4-METHOXYANILINE;3-Iodo-4-methoxyaniline>3-Iodo-4-methoxybenzenamine;3-Iodo-4-methoxyaniline,98%;3-Iodo-4-methoxy-phenylamine;BenzenaMine,3-iodo-4-Methoxy-;4-Amino-2-iodoanisole, 3-Iodo-p-anisidine;(3-iodo-4-methoxyphenyl)amine hydrochloride
CBNumber
CB3335451
Molecular Formula
C7H8INO
Formula Weight
249.05
MOL File
74587-12-5.mol
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3-IODO-4-METHOXYANILINE Property

Melting point:
74 °C
Boiling point:
321℃
Density 
1.807
Flash point:
148℃
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
soluble in Methanol
form 
powder to crystal
pka
4.24±0.10(Predicted)
color 
White to Gray to Brown
InChIKey
UHPNLGCUIGEZRB-UHFFFAOYSA-N
CAS DataBase Reference
74587-12-5(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
HS Code 
2922290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
I0716
Product name
3-Iodo-4-methoxyaniline
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$90
Updated
2025/07/31
TCI Chemical
Product number
I0716
Product name
3-Iodo-4-methoxyaniline
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$302
Updated
2025/07/31
TRC
Product number
B448743
Product name
3-iodo-4-methoxyaniline
Packaging
1g
Price
$75
Updated
2021/12/16
TRC
Product number
B448743
Product name
3-iodo-4-methoxyaniline
Packaging
250mg
Price
$55
Updated
2021/12/16
Ark Pharm
Product number
AK-61933
Product name
3-Iodo-4-methoxyaniline
Purity
98%
Packaging
5g
Price
$34
Updated
2021/12/16
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3-IODO-4-METHOXYANILINE Chemical Properties,Usage,Production

Synthesis

5399-03-1

74587-12-5

General procedure for the synthesis of 3-iodo-4-methoxyaniline from 2-iodo-4-nitroanisole: To a 250 mL round-bottomed flask were added 2-iodo-1-methoxy-4-nitrobenzene (6 g, 21.50 mmol, 1.00 eq.), iron powder (3.61 g, 64.50 mmol, 3.00 eq.), ammonium chloride (3.42 g, 63.94 mmol , 3.00 equiv), ethanol (50 mL) and water (10 mL). The reaction mixture was stirred at 85 °C for 1 hour. Upon completion of the reaction, the solid insoluble material was removed by filtration and the filtrate was concentrated under reduced pressure. The brown solid product 3-iodo-4-methoxyaniline (5.35 g, 100% yield) was obtained. The product was analyzed by liquid chromatography-mass spectrometry (LC-MS): (electrospray ionization, m/z) retention time (RT) = 0.847 min, LCMS 53: m/z = 250 [M + 1].

References

[1] Patent: WO2018/118842, 2018, A1. Location in patent: Paragraph 0421-0424
[2] Patent: WO2016/199943, 2016, A1. Location in patent: Paragraph 0303
[3] Patent: WO2013/14039, 2013, A1. Location in patent: Page/Page column 45-46
[4] Patent: WO2014/152029, 2014, A2. Location in patent: Paragraph 00230
[5] Journal of the American Chemical Society, 1941, vol. 63, p. 2482,2484

3-IODO-4-METHOXYANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-IODO-4-METHOXYANILINE Suppliers

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View Lastest Price from 3-IODO-4-METHOXYANILINE manufacturers

Career Henan Chemical Co
Product
3-IODO-4-METHOXYANILINE 74587-12-5
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-11

74587-12-5, 3-IODO-4-METHOXYANILINERelated Search:

2-Iodoanisole 4-Iodo-2-methoxyaniline 2-Iodo-3-methoxyaniline 4-IODO-3-METHOXYANILINE HYDROCHLORIDE 3-IODO-5-METHOXYANILINE 2-iodo-4-methoxyaniline 5-IODO-2-METHOXYANILINE,5-Iodo-2-methoxyaniline,97% 2-IODO-5-METHOXYANILINE 3-IODO-4-HYDROXYANILINE 3-Iodo-4-methoxyaniline HCl,3-IODO-4-METHOXYANILINE HYDROCHLORIDE 2-Iodo-4-nitroanisole 3-IODO-4-METHOXYANILINE 1,3-Diiodo-2-methoxy-5-nitrobenzene

  • 3-IODO-4-METHOXYANILINE
  • 3-Iodo-4-methoxy-phenylamine
  • 3-Iodo-4-methoxyaniline,98%
  • 4-Amino-2-iodoanisole
  • 3-Iodo-p-anisidine
  • 4-Amino-2-iodoanisole, 3-Iodo-p-anisidine
  • 3-Iodo-4-methoxybenzenamine
  • 4-AMino-2-iodoanisole[3-Iodo-4-Methoxyaniline]
  • BenzenaMine,3-iodo-4-Methoxy-
  • (3-iodo-4-methoxyphenyl)amine hydrochloride
  • 3-Iodo-4-methoxyaniline&gt
  • 74587-12-5
  • Iodine Compounds
  • Anilines, Aromatic Amines and Nitro Compounds
  • Anilines, Amides & Amines
  • Anisoles, Alkyloxy Compounds & Phenylacetates