3-IODO-4-METHOXYANILINE
- Product Name
- 3-IODO-4-METHOXYANILINE
- CAS No.
- 74587-12-5
- Chemical Name
- 3-IODO-4-METHOXYANILINE
- Synonyms
- 3-Iodo-p-anisidine;4-Amino-2-iodoanisole;3-IODO-4-METHOXYANILINE;3-Iodo-4-methoxyaniline>3-Iodo-4-methoxybenzenamine;3-Iodo-4-methoxyaniline,98%;3-Iodo-4-methoxy-phenylamine;BenzenaMine,3-iodo-4-Methoxy-;4-Amino-2-iodoanisole, 3-Iodo-p-anisidine;(3-iodo-4-methoxyphenyl)amine hydrochloride
- CBNumber
- CB3335451
- Molecular Formula
- C7H8INO
- Formula Weight
- 249.05
- MOL File
- 74587-12-5.mol
3-IODO-4-METHOXYANILINE Property
- Melting point:
- 74 °C
- Boiling point:
- 321℃
- Density
- 1.807
- Flash point:
- 148℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 4.24±0.10(Predicted)
- color
- White to Gray to Brown
- InChIKey
- UHPNLGCUIGEZRB-UHFFFAOYSA-N
- CAS DataBase Reference
- 74587-12-5(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2922290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- I0716
- Product name
- 3-Iodo-4-methoxyaniline
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $90
- Updated
- 2025/07/31
- Product number
- I0716
- Product name
- 3-Iodo-4-methoxyaniline
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $302
- Updated
- 2025/07/31
- Product number
- B448743
- Product name
- 3-iodo-4-methoxyaniline
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- B448743
- Product name
- 3-iodo-4-methoxyaniline
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- AK-61933
- Product name
- 3-Iodo-4-methoxyaniline
- Purity
- 98%
- Packaging
- 5g
- Price
- $34
- Updated
- 2021/12/16
3-IODO-4-METHOXYANILINE Chemical Properties,Usage,Production
Synthesis
5399-03-1
74587-12-5
General procedure for the synthesis of 3-iodo-4-methoxyaniline from 2-iodo-4-nitroanisole: To a 250 mL round-bottomed flask were added 2-iodo-1-methoxy-4-nitrobenzene (6 g, 21.50 mmol, 1.00 eq.), iron powder (3.61 g, 64.50 mmol, 3.00 eq.), ammonium chloride (3.42 g, 63.94 mmol , 3.00 equiv), ethanol (50 mL) and water (10 mL). The reaction mixture was stirred at 85 °C for 1 hour. Upon completion of the reaction, the solid insoluble material was removed by filtration and the filtrate was concentrated under reduced pressure. The brown solid product 3-iodo-4-methoxyaniline (5.35 g, 100% yield) was obtained. The product was analyzed by liquid chromatography-mass spectrometry (LC-MS): (electrospray ionization, m/z) retention time (RT) = 0.847 min, LCMS 53: m/z = 250 [M + 1].
References
[1] Patent: WO2018/118842, 2018, A1. Location in patent: Paragraph 0421-0424
[2] Patent: WO2016/199943, 2016, A1. Location in patent: Paragraph 0303
[3] Patent: WO2013/14039, 2013, A1. Location in patent: Page/Page column 45-46
[4] Patent: WO2014/152029, 2014, A2. Location in patent: Paragraph 00230
[5] Journal of the American Chemical Society, 1941, vol. 63, p. 2482,2484
3-IODO-4-METHOXYANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
3-IODO-4-METHOXYANILINE Suppliers
- Tel
- --
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- Country
- Sweden
- ProdList
- 2
- Advantage
- 58
- Tel
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- Fax
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- sales@syntastic.se
- Country
- Sweden
- ProdList
- 181
- Advantage
- 38
View Lastest Price from 3-IODO-4-METHOXYANILINE manufacturers
- Product
- 3-IODO-4-METHOXYANILINE 74587-12-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-07-11