Pipecolamide
- Product Name
- Pipecolamide
- CAS No.
- 19889-77-1
- Chemical Name
- Pipecolamide
- Synonyms
- Pipecolamide;pipecolinamide;piperidinecarboxamide;Revefenacin Impurity 51;piperidine-2-carboxamide;2-Piperidinecarboxamide>Piperidine-2-carboxylic acid aMide
- CBNumber
- CB3947740
- Molecular Formula
- C6H12N2O
- Formula Weight
- 128.17
- MOL File
- 19889-77-1.mol
Pipecolamide Property
- Melting point:
- 138-140°
- Boiling point:
- 311.7±31.0 °C(Predicted)
- Density
- 1.060±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- slightly sol. in Methanol
- form
- powder to crystal
- pka
- 16.77±0.20(Predicted)
- color
- White to Almost white
- InChI
- InChI=1S/C6H12N2O/c7-6(9)5-3-1-2-4-8-5/h5,8H,1-4H2,(H2,7,9)
- InChIKey
- XIMBESZRBTVIOD-UHFFFAOYSA-N
- SMILES
- N1CCCCC1C(N)=O
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- P2028
- Product name
- 2-Piperidinecarboxamide
- Purity
- >98.0%(GC)(T)
- Packaging
- 1g
- Price
- $224
- Updated
- 2025/07/31
- Product number
- B448923
- Product name
- Piperidine-2-carboxamide
- Packaging
- 250mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- B448923
- Product name
- Piperidine-2-carboxamide
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- X0387
- Product name
- Piperidine-2-carboxamide
- Packaging
- 1g
- Price
- $67
- Updated
- 2021/12/16
- Product number
- 043536
- Product name
- 2-Piperidinecarboxamide
- Purity
- 97%
- Packaging
- 5g
- Price
- $49
- Updated
- 2021/12/16
Pipecolamide Chemical Properties,Usage,Production
Chemical Properties
White solid
Synthesis
28697-07-6
19889-77-1
General procedure for the synthesis of 2-piperidinecarboxamide from 1-N-benzyloxycarbonyl-2-piperidinecarboxylic acid:[Ref. Example 19] To a dichloromethane (20 mL) containing N-benzyloxycarbonylpiperidine-2-carboxylic acid (2.0 g), 1-hydroxybenzotriazole (1.6 g), and 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (2.3 g) at room temperature Concentrated ammonia (3 mL) and triethylamine (2 mL) were added to the solution, followed by stirring the reaction mixture for 3 days. Upon completion of the reaction, the mixture was partitioned between water and dichloromethane. The organic layer was dried with anhydrous magnesium sulfate, filtered and the solvent was evaporated under reduced pressure. The residue was dissolved in methanol (30 mL), 10% palladium-carbon catalyst (1 g, 50% wet) was added and stirred under hydrogen atmosphere for 20 hours. At the end of the reaction, the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to give the 2-piperidinecarboxamide solid product (970 mg, quantitative yield). m/z MS (ESI): 128 (M+).
References
[1] Patent: EP1762568, 2007, A1. Location in patent: Page/Page column 37-38
Pipecolamide Preparation Products And Raw materials
Raw materials
Preparation Products
Pipecolamide Suppliers
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View Lastest Price from Pipecolamide manufacturers
- Product
- Piperidine-2-carboxamide 19889-77-1
- Price
- US $15.00-50.00/kg
- Min. Order
- 1kg
- Purity
- NLT98%
- Supply Ability
- 5 ton per month
- Release date
- 2023-04-02
- Product
- Pipecolamide 19889-77-1
- Price
- US $50.00/kg
- Min. Order
- 1kg
- Purity
- 0.99
- Supply Ability
- 10000
- Release date
- 2023-10-09
- Product
- 2-piperidine carboxamide 19889-77-1
- Price
- US $75.00/g
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 5ton/Month
- Release date
- 2021-12-15