2-Iodobenzyl bromide
Application- Product Name
- 2-Iodobenzyl bromide
- CAS No.
- 40400-13-3
- Chemical Name
- 2-Iodobenzyl bromide
- Synonyms
- 2-Iodobenzyl bromid;2-IODOBENZYL BROMIDE;O-IODOBENZYL BROMIDE;à-bromo-2-iodotoluene;a-Bromo-2-iodotoluene;α-Bromo-2-iodotoluene;o-Iodobenzoyl Bromide;2-IodobenzylBromide>2-Iodobenzylbromide,96%;ALPHA-BROMO-2-IODOTOLUENE
- CBNumber
- CB4180430
- Molecular Formula
- C7H6BrI
- Formula Weight
- 296.93
- MOL File
- 40400-13-3.mol
2-Iodobenzyl bromide Property
- Melting point:
- 54-60 °C(lit.)
- Boiling point:
- 125 °C / 4mmHg
- Density
- 2.105±0.06 g/cm3(Predicted)
- Flash point:
- >230 °F
- storage temp.
- Keep in dark place,Inert atmosphere,2-8°C
- solubility
- soluble in Methanol
- form
- Crystalline Powder
- color
- White to cream
- Sensitive
- Light Sensitive
- BRN
- 2079736
- CAS DataBase Reference
- 40400-13-3(CAS DataBase Reference)
Safety
- Hazard Codes
- C,N,T
- Risk Statements
- 22-34-43-51/53-63-42/43-36/37/38
- Safety Statements
- 26-36/37/39-61-45-23
- RIDADR
- UN 3261 8/PG 2
- WGK Germany
- 2
- HazardClass
- 8
- PackingGroup
- Ⅱ
- HS Code
- 29039990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H314Causes severe skin burns and eye damage
H318Causes serious eye damage
H334May cause allergy or asthma symptoms or breathing difficulties if inhaled
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 634603
- Product name
- 2-Iodobenzyl bromide
- Purity
- 97%
- Packaging
- 5g
- Price
- $78.3
- Updated
- 2022/05/15
- Product number
- I0635
- Product name
- 2-Iodobenzyl Bromide
- Packaging
- 1G
- Price
- $23
- Updated
- 2025/07/31
- Product number
- I0635
- Product name
- 2-Iodobenzyl Bromide
- Packaging
- 5G
- Price
- $66
- Updated
- 2025/07/31
- Product number
- I737230
- Product name
- 2-Iodobenzyl bromide
- Packaging
- 2.5g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- JK203317
- Product name
- 2-Iodobenzyl bromide
- Purity
- 96%
- Packaging
- 1g
- Price
- $31
- Updated
- 2021/12/16
2-Iodobenzyl bromide Chemical Properties,Usage,Production
Application
2-Iodobenzylmethyl bromide is a halocarbon compound mainly used in laboratory research and development processes and chemical production processes.
Chemical Properties
White solid
Synthesis
5159-41-1
40400-13-3
General procedure for the synthesis of 2-iodobenzyl bromide from 2-iodobenzyl alcohol: 48% hydrobromic acid (10 mL) and 98% sulfuric acid (2 mL) were added to 2-iodobenzyl alcohol (0.94 g, 4.0 mmol). The resulting suspension was placed in an oil bath and heated and stirred at 150 °C for 2 hours. After completion of the reaction, the mixture was cooled to room temperature and extracted with dichloromethane (2 x 10 mL). The organic layers were combined, dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by fast column chromatography (silica gel, 0-20% dichloromethane/hexane gradient elution) to afford the target compound 2-iodobenzyl bromide (1.0 g, 84% yield).
References
[1] Tetrahedron, 2005, vol. 61, # 13, p. 3311 - 3324
[2] Journal of Organic Chemistry, 2012, vol. 77, # 13, p. 5705 - 5713
[3] Helvetica Chimica Acta, 1995, vol. 78, p. 765 - 771
[4] Tetrahedron, 1993, vol. 49, # 20, p. 4439 - 4446
[5] Tetrahedron, 2002, vol. 58, # 44, p. 9007 - 9018
2-Iodobenzyl bromide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Iodobenzyl bromide manufacturers
- Product
- 2-Iodobenzyl bromide 40400-13-3
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-07
- Product
- 2-Iodobenzyl bromide 40400-13-3
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20ton
- Release date
- 2024-06-07
- Product
- 2-Iodobenzyl bromide 40400-13-3
- Price
- US $100.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-26