METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE
Preparation- Product Name
- METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE
- CAS No.
- 70264-94-7
- Chemical Name
- METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE
- Synonyms
- METHYL 3-METHOXY-4-BROMOMETHYLBENZOATE;)-3-methoxybenzoate;Methyl 4-(Bromomethyl)-m-anisate;4-(bromomethyl)-3-methoxybenzoate;METHYL4-BROMOETHYL-3-METHOXYBENZOATE;METHYL3-METHOXY-4-(BROMOMETHYL)BENZONATE;METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE;Methyl 4-(bromomethyl)-3-methoxybenzonate;Methyl4-(Bromomethyl)-3-methoxybenzoate>4-(Bromomethyl)-m-anisic Acid Methyl Ester
- CBNumber
- CB4342137
- Molecular Formula
- C10H11BrO3
- Formula Weight
- 259.1
- MOL File
- 70264-94-7.mol
METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Property
- Melting point:
- 92-94°C
- Boiling point:
- 324.2±32.0 °C(Predicted)
- Density
- 1.432
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- Chloroform (Sparingly), Methanol (Slightly)
- form
- powder to crystal
- color
- White to Light yellow
- CAS DataBase Reference
- 70264-94-7(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,N
- Risk Statements
- 36/37/38-50/53-43-41-38
- Safety Statements
- 26-36/37/39-61-60
- RIDADR
- UN 2811 6.1/PG 3
- WGK Germany
- 3
- HazardClass
- IRRITANT
- PackingGroup
- Ⅲ
- HS Code
- 2918999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H317May cause an allergic skin reaction
H318Causes serious eye damage
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 681180
- Product name
- Methyl 4-(bromomethyl)-3-methoxybenzoate
- Purity
- 97%
- Packaging
- 5g
- Price
- $82.4
- Updated
- 2024/03/01
- Product number
- 681180
- Product name
- Methyl 4-(bromomethyl)-3-methoxybenzoate
- Purity
- 97%
- Packaging
- 1g
- Price
- $69.8
- Updated
- 2023/06/20
- Product number
- M2356
- Product name
- Methyl 4-(Bromomethyl)-3-methoxybenzoate
- Purity
- >97.0%(GC)
- Packaging
- 5g
- Price
- $106
- Updated
- 2024/03/01
- Product number
- M2356
- Product name
- Methyl 4-(Bromomethyl)-3-methoxybenzoate
- Purity
- >97.0%(GC)
- Packaging
- 25g
- Price
- $425
- Updated
- 2024/03/01
- Product number
- M258700
- Product name
- Methyl 4-(bromomethyl)-3-methoxybenzoate
- Packaging
- 5g
- Price
- $70
- Updated
- 2021/12/16
METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Chemical Properties,Usage,Production
Preparation
Methyl 4-(bromomethyl)-3-methoxybenzoate is prepared by the following steps:A mixture of methyl 3-methoxy-4-methylbenzoate 37 (5 g, 27.8 mmol), NBS (4.94 g, 27.8 mmol), and benoyl peroxide (0.0008 g, 0.003 mmol) was refluxed in CCl4 (25 ml) for 10 hours. The reaction mixture was allowed to cool and filtered. The residue was washed with CCl4 and the combined filtrate concentrated in vacuo. Purification by column chromatography over silica gel (5-10% EtOAc-pet ether) furnished a colourless solid (7.19 g).Yield : 100%
Uses
Methyl 4-(Bromomethyl)-3-methoxybenzoate is an intermediate used to prepare heteroarylphenyloxoacetyl and heteroarylphenylsulfonyl benzoylpiperazine analogs of BMS 378806 as HIV entry inhibitors. It is also used to synthesize steroid 5α-reductase inhibiting acylpiperidines.
METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Preparation Products And Raw materials
Raw materials
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View Lastest Price from METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE manufacturers
- Product
- METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE 70264-94-7
- Price
- US $1.00/KG
- Min. Order
- 1G
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-08-15