5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione

Product Name: 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
CAS No.: 4664-00-0
Chemical Name: 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
Synonyms: NSC 405554;AKOS 93366;QUINOLINIMIDE;3-azaphthalimid;Moxifloxacin Imp.X;QUINOLINICACIDAMIDE;quinolinicacidimide;pyridinedicarboxamide;2,3-Pyridinedicarbimide;Pyridine-2,3-dicarbimide
CBNumber: CB4463896
Molecular Formula: C7H4N2O2
Formula Weight: 148.12
MOL File: 4664-00-0.mol

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5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Property

Melting point:: 233-234°C
Boiling point:: 268.69°C (rough estimate)
Density: 1.4015 (rough estimate)
refractive index: 1.5300 (estimate)
storage temp.: Refrigerator
solubility: Dichloromethane, Ether, Ethyl Acetate, Methanol
pka: 8.08±0.20(Predicted)
form: Solid
color: Brown

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: Q711500
Product name: Quinolinimide
Packaging: 1g
Price: $105
Updated: 2021/12/16

AK Scientific

Product number: 6385AB
Product name: 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
Packaging: 5g
Price: $164
Updated: 2021/12/16

Matrix Scientific

Product number: 157822
Product name: 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
Packaging: 0.500g
Price: $240
Updated: 2021/12/16

Matrix Scientific

Product number: 157822
Product name: 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione
Packaging: 1g
Price: $300
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0069556
Product name: 2,3-PYRIDINEDICARBOXIMIDE
Purity: 95.00%
Packaging: 1G
Price: $721.57
Updated: 2021/12/16

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5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Chemical Properties,Usage,Production

Chemical Properties

Light yellow solid

Uses

Quinolinimide (cas# 4664-00-0) is a compound useful in organic synthesis.

Synthesis

89-00-9

4664-00-0

General procedure for the synthesis of 2,3-pyridinedicarboximide from 2,3-pyridinedicarboxylic acid: 167 g of 2,3-pyridinedicarboxylic acid (1.0 mol) and 300 mL of concentrated ammonia (28%) were added to a 1000 mL three-necked flask, followed by refluxing and stirring for 6 hours at 140 °C. The reaction was carried out in a liquid mixture of 2,3-pyridinedicarboxylic acid (1.0 mol) and 300 mL of concentrated ammonia (28%). During the reaction, the liquid reaction mixture gradually changed to dark brown color. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the complete reaction of 2,3-pyridinedicarboxylic acid, the reaction mixture was cooled to room temperature. Under continuous stirring, the reaction mixture was slowly poured into 500 mL of cold water, and a large amount of gray solid precipitated immediately. The solid product was collected by filtration and the filter cake was washed with cold water and subsequently dried under vacuum at 60 °C overnight to give 125 g of gray powdery product in 84% yield.

References

[1] Patent: CN102746294, 2016, B. Location in patent: Paragraph 0077; 0078
[2] Heterocycles, 2002, vol. 57, # 10, p. 1881 - 1890
[3] Bioorganic and Medicinal Chemistry, 2001, vol. 9, # 8, p. 2061 - 2071
[4] European Journal of Medicinal Chemistry, 2012, vol. 55, p. 58 - 66,9
[5] Molecules, 2000, vol. 5, # 3, p. 481 - 482

5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Preparation Products And Raw materials

Raw materials

Acetic anhydride Ethyl acetate Quinolinic acid Methanol Ammonium acetate PETROLEUM ETHER

Preparation Products

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5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione Suppliers

Canada 2 China 114 Germany 1 India 3 The Netherlands 1 United Kingdom 1 United States 18 Global 140

Accela ChemBio Inc.

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View Lastest Price from 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione manufacturers

Dideu Industries Group Limited

Product: QUINOLINIMIDE 4664-00-0
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-26

Career Henan Chemical Co

Product: QUINOLINIMIDE 4664-00-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-03

4664-00-0, 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dioneRelated Search:

Pyrrolo[1,2-a]pyrazine-3-carboxylic acid (9CI) Pyrrolo1,2-apyrimidin-3-ylamine dihydrochloride Pyrrolo[1,2-a]pyrimidine-3,6-dicarboxylic acid N-Boc-6-azaindole Ethyl pyrrolo[1,2-a]pyrazine-3-carboxylate Pyrrolo1,2-apyrimidine-3,6-dicarboxylic acid 6-ethyl ester H-pyrrolo[1,2-a]pyrimidine-3-carboxylic acid 2-METHYLNICOTINALDEHYDE 3-METHYL-2-PYRIDINECARBOXALDEHYDE 2,3-Lutidine 3-(AMINOMETHYL)PYRIDINE 5H-Pyrrolo[3,4-b]pyridine-5,7(6H)-dione METHYLPYRIDIN-2-YLMETHYLAMINE DIHYDROCHLORIDE 6,7-Dihydro-5H-pyrrolo[3,4-b]pyridine PYRIDINE-2-CARBOXAMIDE 3-Methylpicolinamide N-METHYLNICOTINAMIDE 3,4-PYRIDINEDICARBOXIMIDE

pyridine-2,3-dicarboximide

QUINOLINICACIDAMIDE

2,3-Pyridinedicarbimide

6H-Pyrrolo[3,4-b]pyridine-5,7-dione

Pyridine-2,3-dicarbimide

3,4-Pyridinedicarboximide

NSC 405554

2,3-PYRIDINEDICARBOXAMIDE

AKOS 93366

5H-PYRROLO[3,4-B]PYRIDINE-5,7(6H)-DIONE

QUINOLINIMIDE

PYRROLO[3,4-B]PYRIDINE-5,7-DIONE

2,3-pyridinedicarboximide

3-azaphthalimid

pyridinedicarboxamide

quinolinicacidimide

3-Azaphthalimid [German]

2,3-Pyridinedicarboximide(WX619013)

5H-Pyrrolo(3,4-b)pyridine-5,7(6H)-dione (9CI)

pyrrolo[3,4-b]pyridine-5,7-quinone

Moxifloxacin Imp.X

QUINOLINIMIDE ISO 9001：2015 REACH

2,3-pyridinedicarboximidequinolinimide

4664-00-0

Heterocycle-Pyridine series

Pyridine

Miscellaneous Reagents

Aromatics

Heterocycles