2-Fluoro-5-nitroanisole

Product Name: 2-Fluoro-5-nitroanisole
CAS No.: 454-16-0
Chemical Name: 2-Fluoro-5-nitroanisole
Synonyms: 2-Fluoro-5-nitroanisole;2-Fluoro-5-nitroasinole;4-Fluoro-3-methoxynitrobenzene;3-Methoxy-4-fluoronitrobenzene;Anisole, 2-fluoro-5-nitro- (8CI);1-Fluoro-2-methoxy-4-nitrobenzene;Benzene, 1-fluoro-2-methoxy-4-nitro-;4-Fluoro-3-methoxynitrobenzene 2-Fluoro-5-nitroanisole;2-Fluoro-5-nitroanisole[4-Fluoro-3-Methoxynitrobenzene];4-Fluoro-3-methoxynitrobenzene, 1-Fluoro-2-methoxy-4-nitrobenzene, 2-Fluoro-5-nitrophenyl methyl ether
CBNumber: CB51466501
Molecular Formula: C7H6FNO3
Formula Weight: 171.13
MOL File: 454-16-0.mol

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2-Fluoro-5-nitroanisole Property

Melting point:: 69-71 °C
Boiling point:: 270.3±20.0 °C(Predicted)
Density: 1.321±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Solid
color: Light Yellow to Yellow
InChI: InChI=1S/C7H6FNO3/c1-12-7-4-5(9(10)11)2-3-6(7)8/h2-4H,1H3
InChIKey: AZNKKZHZGDZSIF-UHFFFAOYSA-N
SMILES: C1(F)=CC=C([N+]([O-])=O)C=C1OC

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Safety

Hazard Codes: Xi
HS Code: 2909309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F597580
Product name: 2-Fluoro-5-nitroanisole
Packaging: 500mg
Price: $60
Updated: 2021/12/16

TRC

Product number: F597580
Product name: 2-Fluoro-5-nitroanisole
Packaging: 1g
Price: $70
Updated: 2021/12/16

Matrix Scientific

Product number: 073101
Product name: 2-Fluoro-5-nitroanisole
Purity: 95+%
Packaging: 25g
Price: $79
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0023774
Product name: 4-FLUORO-3-METHOXYNITROBENZENE
Purity: 95.00%
Packaging: 50MG
Price: $117.6
Updated: 2021/12/16

Matrix Scientific

Product number: 073101
Product name: 2-Fluoro-5-nitroanisole
Purity: 95+%
Packaging: 100g
Price: $238
Updated: 2021/12/16

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2-Fluoro-5-nitroanisole Chemical Properties,Usage,Production

Synthesis

22510-08-3

74-88-4

454-16-0

GENERAL STEPS: Potassium carbonate (K2CO3, 5.27 g, 38.1 mmol) was added to a solution of 2-fluoro-5-nitrophenol (5.0 g, 31.84 mmol) in N,N-dimethylformamide (DMF, 50 mL), and the mixture was stirred for 15 minutes at room temperature. Subsequently, iodomethane (3 mL, 47.7 mmol) was added and the reaction mixture continued to be stirred for 2 hours at room temperature. Upon completion of the reaction, the mixture was poured into ice water and the solid product was isolated by filtration. The solid was washed well with deionized water and subsequently dried under vacuum to afford the off-white solid product 2-fluoro-5-nitroanisole (4.0 g, 73.5% yield). The structure of the product was confirmed by 1H NMR (300 MHz, CDCl3): δ 7.89-7.84 (m, 2H), 7.25-7.17 (m, 1H), 3.98 (s, 3H).

References

[1] Patent: WO2015/104653, 2015, A1. Location in patent: Page/Page column 57
[2] Patent: US2016/368906, 2016, A1. Location in patent: Paragraph 0229
[3] Patent: US2014/57911, 2014, A1. Location in patent: Paragraph 0635

2-Fluoro-5-nitroanisole Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Fluoro-5-nitroanisole Suppliers

Canada 2 China 166 India 2 United Kingdom 2 United States 8 Global 180

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View Lastest Price from 2-Fluoro-5-nitroanisole manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-Fluoro-5-nitroanisole 454-16-0
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2025-03-10

R&D Scientific Inc.

Product: 2-Fluoro-5-nitroanisole 454-16-0
Price: US $890.00/g
Min. Order: 1g
Purity: 98
Supply Ability: 5000 Kg
Release date: 2025-04-07

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Fluoro-5-nitroanisole 454-16-0
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-19

454-16-0, 2-Fluoro-5-nitroanisoleRelated Search:

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2-Fluoro-5-nitroasinole

4-Fluoro-3-methoxynitrobenzene 2-Fluoro-5-nitroanisole

454-16-0

445-93-6

Multisubstituted Benzene

Aromatic Halides (substituted)