ChemicalBook > CAS DataBase List > 4-BROMO-3-HYDROXYPYRIDINE

4-BROMO-3-HYDROXYPYRIDINE

Product Name
4-BROMO-3-HYDROXYPYRIDINE
CAS No.
161417-28-3
Chemical Name
4-BROMO-3-HYDROXYPYRIDINE
Synonyms
4-Bromopyridin-3-ol;4-BROMO-3-PYRIDINOL;3-Pyridinol, 4-bromo-;4-boro-3-hydroxypyridine;4-BROMO-3-HYDROXYPYRIDINE;4-BROMO-3-HYDROXYOPYRIDINE;4-BROMO-3-HYDROXYPYRIDINE ISO 9001：2015 REACH
CBNumber
CB5147797
Molecular Formula
C5H4BrNO
Formula Weight
174
MOL File
161417-28-3.mol
More
Less

4-BROMO-3-HYDROXYPYRIDINE Property

Melting point:
134-136°C
Boiling point:
316.2±22.0 °C(Predicted)
Density 
1.788±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,2-8°C
solubility 
Chloroform (Sparingly), Ethyl Acetate
form 
Solid
pka
6.57±0.10(Predicted)
color 
White to Off-White
More
Less

Safety

HS Code 
2933399990
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

More
Less

N-Bromosuccinimide Price

TRC
Product number
B684473
Product name
4-Bromo-3-hydroxypyridine
Packaging
250mg
Price
$65
Updated
2021/12/16
TRC
Product number
B684473
Product name
4-Bromo-3-hydroxypyridine
Packaging
5g
Price
$525
Updated
2021/12/16
Apolloscientific
Product number
OR301092
Product name
4-Bromo-3-hydroxypyridine
Purity
96%
Packaging
10g
Price
$551
Updated
2021/12/16
SynQuest Laboratories
Product number
4H01-9-04
Product name
4-Bromo-3-hydroxypyridine
Purity
96%
Packaging
10g
Price
$608
Updated
2021/12/16
ChemScene
Product number
CS-W006061
Product name
4-Bromo-3-hydroxypyridine
Purity
99.98%
Packaging
25g
Price
$705
Updated
2021/12/16
More
Less

4-BROMO-3-HYDROXYPYRIDINE Chemical Properties,Usage,Production

Chemical Properties

White Solid

Synthesis

98976-81-9

161417-28-3

The general procedure for the synthesis of 4-bromo-3-hydroxypyridine from the compound (CAS: 98976-81-9) is as follows: to a solution of 4-bromo-3-pyridinyl diethylcarbamate (1.24 g, 4.50 mmol) in methanol (10 mL) was added methanolic solution of sodium methanolate (2.04 g, 9.40 mmol) at 20°C and the resulting mixture was refluxed for 1.5 hours. Upon completion of the reaction, methanol was removed by distillation under reduced pressure, ethyl acetate (15 mL) and water (1 mL) were added, and then the pH was adjusted to 9 with 20% aqueous sulfuric acid. the organic layer was separated, and the residue was washed with ethyl acetate (3 x 5 mL). The organic layers were combined, dried and concentrated with anhydrous sodium sulfate. The crude product was purified by rapid chromatography on silica gel, eluting sequentially with hexane/ethyl acetate (1:1 and 1:2) to give 691 mg (89% yield) of 4-bromo-3-hydroxypyridine.TLC Rf value was 0.38 (1:2 hexane/ethyl acetate). Mass spectra (DCI/NH3) m/e 174 (with 79 Br) and 176 (M+H)+ (with 81 Br).1H NMR (CDCl3, 300 MHz) δ: 8.43 (d, J=1.5 Hz, 1H, ArH), 8.02 (d, J=7.2 Hz, 1H, ArH), 7.54 (dd, J=7.2,1.5 Hz. 1H, ArH).

References

[1] Patent: US5914328, 1999, A
[2] Patent: US5948793, 1999, A

4-BROMO-3-HYDROXYPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

4-BROMO-3-HYDROXYPYRIDINE Suppliers

Canada 1 China 124 Europe 1 Germany 2 India 2 United Kingdom 5 United States 15 Global 150
Zhuhai Aobokai Biomedical Technology Co., Ltd.
Tel
400-0628126 15697568807;
Email
sales-team@aobchem.com.cn
Country
China
ProdList
9994
Advantage
58
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
ProdList
18207
Advantage
66
Jia Xing Isenchem Co.,Ltd
Tel
0573-85285100 18627885956
Fax
0573-85285100
Email
isenchem@163.com
Country
China
ProdList
9310
Advantage
66
Shangchem Co., Ltd.
Tel
+86-21-68182121
Fax
+86-21-68182121
Country
China
ProdList
882
Advantage
52
Chemsky（shanghai）International Co.,Ltd.
Tel
021-50135380
Email
shchemsky@sina.com
Country
China
ProdList
32321
Advantage
50
China Langchem Inc.
Tel
0086-21-58956006
Fax
0086-21-58956100
Country
China
ProdList
7811
Advantage
57
skychemical Co.Ltd
Tel
021-20958197 20965099
Fax
021-20960837
Email
sales@skychemical.com
Country
China
ProdList
1183
Advantage
57
Shanghai Sunway Pharmaceutical Technology Co., Ltd
Tel
18270980682
Fax
021 51613951
Email
mlcheng@sunwaypharm.cn
Country
China
ProdList
8669
Advantage
57
Tongchuang Pharma(Suzhou). Co., Ltd.
Tel
0512-63263366 18912765016
Fax
0512-6326 3366
Email
tongtf110@sina.com
Country
China
ProdList
993
Advantage
62
Aloespharm Co., Ltd.
Tel
021-20960837
Fax
021-20960837
Email
market@aloespharm.com
Country
China
ProdList
1302
Advantage
55
Shanghai Hekang Biotechnology Co., Ltd.
Tel
18939837085
Fax
2880152141(QQ)
Email
youchemicals@gmail.com
Country
China
ProdList
1839
Advantage
55
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Shanghai Worldyang Chemical Co.,Ltd.
Tel
021-021-56795766
Fax
+86-21-56795266
Email
sales@worldyachem.com
Country
China
ProdList
9476
Advantage
58
Shanghai YuYuan Pharmaceutical Co., Ltd.
Tel
13052276172
Fax
13052276172
Email
product@yuyuanpharm.com
Country
China
ProdList
493
Advantage
55
Mashilabs (Shanghai) Co.,Ltd.
Tel
19916721580
Fax
QQ：3154870176
Email
mafarm@126.com
Country
China
ProdList
4542
Advantage
58
Shanghai HuanChuan Industry Co.,Ltd.
Tel
021-61478794
Fax
021-61478794
Email
sales@hcshhai.com
Country
China
ProdList
9793
Advantage
50
Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66028182 18626450290
Email
yftan@aikonchem.com
Country
China
ProdList
16679
Advantage
50
Cool Pharm, Ltd
Tel
021-60455363 18019463053
Fax
50966098
Email
sales@coolpharm.com
Country
China
ProdList
12346
Advantage
58
SuZhou ShiYa Biopharmaceuticals, Inc.
Tel
0512-0512-52358471 17715136450
Fax
05125235 6881
Email
sales@shiyabiopharm.com
Country
China
ProdList
12127
Advantage
58
skychemical Co.Ltd
Tel
021-20960837,QQ1332204249
Fax
021-20960837
Email
sales@skychemical.com
Country
China
ProdList
3341
Advantage
55
Henan CoreyChem Co., Ltd
Tel
0371-86658258
Fax
0371-60996044
Email
info@coreychem.com
Country
China
ProdList
10453
Advantage
58
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
parabiochem
Tel
025-83453382-8005
Fax
025-83453382
Email
sale@parabiochem.com
Country
China
ProdList
9595
Advantage
55
WG reagent
Tel
13391486464
Fax
QQ:14748090
Email
samwjf@163.com
Country
China
ProdList
3086
Advantage
55
ChengDu TongChuangYuan Pharmaceutical Co.Ltd
Tel
028-83379370 13880556291
Fax
028-87747383
Email
tcy@tcypharm.com
Country
China
ProdList
7218
Advantage
58
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Shanghai Yihe Biological Technology Co., Ltd.
Tel
021-68882955 17721395025
Fax
021-68882955
Email
2423903095@qq.com
Country
China
ProdList
4991
Advantage
58
Taian Jiaye Biotechnology Co.Ltd
Tel
13127280945
Email
285424065@qq.com
Country
China
ProdList
9976
Advantage
55
Nanijing m&m biotechnology Co. ,Ltd.
Tel
025-87782433 18021532344
Fax
025-87782433
Email
1345332203@qq.com
Country
China
ProdList
4134
Advantage
58
Hangzhou Molcore Biopharmatech Co.,Ltd
Tel
400-711-5280 86-571-81025280
Fax
86-571-85806285
Email
sales@molcore.com
Country
China
ProdList
9967
Advantage
58
Nanjing NingFan Pharm-Tech CO. LTD.
Tel
17368696818
Country
China
ProdList
1984
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 400821072
Fax
021-58955996
Email
malulu@leyan.com
Country
China
ProdList
25000
Advantage
58
Henan Aosman Biotechnology Co., LTD
Tel
0371-0371-61318675 17719817155
Fax
0371-61318675
Email
sales@xlinebio.com
Country
China
ProdList
2857
Advantage
58
Shanghai Jizhi Biochemical Technology Co. Ltd.
Tel
4009004166/18616739031 18616739031
Email
3007523370@qq.com
Country
China
ProdList
52687
Advantage
58
Shanghai Maruhua Science and Technology Co. Ltd.
Tel
021-57171708 18721745940
Fax
QQ1139783351
Email
sales@api-chem.com
Country
China
ProdList
1968
Advantage
58
Guangdong wengjiang Chemical Reagent Co., Ltd.
Tel
0751-2815688 13927872512
Fax
0751-8963795
Email
3007421951@qq.com
Country
China
ProdList
9939
Advantage
58
Shenzhen Polymeri Biochemical Technology Co., Ltd.
Tel
+86-400-002-6226 +86-13028896684;
Email
sales@rrkchem.com
Country
China
ProdList
57422
Advantage
58
ROSEWA HOLDING GROUP CO.,LIMITED
Tel
+86-023-62871537
Email
sales@rosewachem.com
Country
China
ProdList
2803
Advantage
58
Zhengzhou Alfa Chemical Co.,Ltd
Tel
+8618530059196
Email
sale04@alfachem.cn
Country
China
ProdList
11784
Advantage
58
ANHUI WITOP BIOTECH CO., LTD
Tel
+8615255079626
Email
eric@witopchemical.com
Country
China
ProdList
23541
Advantage
58
Hefei TNJ Chemical Industry Co.,Ltd.
Tel
+86-0551-65418684 +8618949823763
Fax
0086-551-65418684
Email
sales@tnjchem.com
Country
China
ProdList
25356
Advantage
58
Labnetwork lnc.
Tel
+86-27-50766799 +8618062016861
Email
contact@labnetwork.com
Country
China
ProdList
19987
Advantage
58
Dideu Industries Group Limited
Tel
+86-29-89586680 +86-15129568250
Email
1026@dideu.com
Country
China
ProdList
20284
Advantage
58
Dayang Chem (Hangzhou) Co.,Ltd.
Tel
+86-0571-88938639 +8617705817739
Fax
+86-571-88938652，+86-571- 88492614
Email
info@dycnchem.com
Country
China
ProdList
52846
Advantage
58
Hefei Hirisun Pharmatech Co., Ltd
Tel
+8615056975894
Fax
86-0551-62678551
Email
shawn@hirisunpharm.com
Country
CHINA
ProdList
9911
Advantage
58
SIMAGCHEM CORP
Tel
+86-5922680277 +86-13806087780
Email
sale@simagchem.com
Country
China
ProdList
17346
Advantage
58
Hubei Jusheng Technology Co.,Ltd.
Tel
18871490254
Fax
027-59599243
Email
linda@hubeijusheng.com
Country
CHINA
ProdList
28172
Advantage
58
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Email
sales@accelachem.com
Country
China
ProdList
10467
Advantage
58
Qi Qi hang Biotechnology Co., Ltd.
Tel
18151111370
Email
1046215251@qq.com
Country
China
ProdList
5999
Advantage
58
More
Less

View Lastest Price from 4-BROMO-3-HYDROXYPYRIDINE manufacturers

Dideu Industries Group Limited
Product
4-BROMO-3-HYDROXYPYRIDINE 161417-28-3
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-09-24
Career Henan Chemical Co
Product
4-BROMO-3-HYDROXYPYRIDINE 161417-28-3
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1000kg
Release date
2020-01-13

161417-28-3, 4-BROMO-3-HYDROXYPYRIDINERelated Search:

2,4,6-TRIBROMO-3-PYRIDINOL 4-BROMO-2-HYDROXYPYRIDINE 97%,4-BROMO-2-HYDROXYPYRIDINE 4-BROMO-3-METHOXYPYRIDINE 3-Bromo-2-methoxy-5-trifluoromethylpyridine 4-BROMO-3-HYDROXYPYRIDINE 2-BROMO-3-HYDROXYPYRIDINE (2-BROMO-3-PYRIDINOL),2-Bromo-3-pyridinol(2-Bromo-3-hydroxypyridine),2-BROMO-3-HYDROXYPYRIDINE 97%,2-BROMO-3-HYDROXYPYRIDINE 4-Amino-3-bromo-2-hydroxypyridine 2-amino-5-bromopyridin-3-ol 5-Bromo-2-hydroxypyridine-4-carboxylic acid METHYL 5-BROMO-2-HYDROXYPYRIDINE-3-CARBOXYLATE 3,5-DIBROMO-2-HYDROXYPYRIDINE 2-Bromo-4-Hydroxypyridine 2-BROMO-6-HYDROXYPYRIDINE 2-BROMO-5-HYDROXYPYRIDINE,6-BROMO-3-HYDROXYPYRIDINE,2-BROMO-5-HYDROXYPYRIDINE ,98% 5-BROMO-2-HYDROXYPYRIDINE, 97%%,3-Bromo-6-hydroxypyridine,5-BROMO-2-HYDROXYPYRIDINE 5-BROMO-2-HYDROXYPYRIDINE-3-CARBOXYLIC ACID 3-AMINO-5-BROMO-2-HYDROXYPYRIDINE 3-BROMO-5-HYDROXYPYRIDINE 98.5+%,5-Bromo-3-hydroxypyridine 5-Bromo-3-pyridinol,3-BROMO-5-HYDROXYPYRIDINE,5-BROMO-3-HYDROXYPYRIDINE

  • 4-BROMO-3-HYDROXYPYRIDINE
  • 4-BROMO-3-PYRIDINOL
  • 4-BROMO-3-HYDROXYOPYRIDINE
  • 3-Pyridinol, 4-bromo-
  • 4-Bromopyridin-3-ol
  • 4-boro-3-hydroxypyridine
  • 4-BROMO-3-HYDROXYPYRIDINE ISO 9001：2015 REACH
  • 161417-28-3
  • Pyridines
  • Pyridines, Pyrimidines, Purines and Pteredines
  • pharmacetical
  • Pyridine
  • Chemical Amines
  • Amines
  • Aromatics
  • Heterocycles