Ethyl 6-bromoindole-2-carboxylate

Product Name: Ethyl 6-bromoindole-2-carboxylate
CAS No.: 103858-53-3
Chemical Name: Ethyl 6-bromoindole-2-carboxylate
Synonyms: 6-Br-ICA-OEt;SPECS AR-437/43285096;6-BROMO-2-CARBETHOXYINDOLE;6-bromoindole-2-carboxylate;6-6-BROMO-2-INDOLECARBOXYLIC;6-Bromo-2- carboethoxyindole;Ethyl 6-bromoindole-2-carboxylat;ETHYL 6-BROMOINDOLE-2-CARBOXYLATE;Methyl 6-bromoindole-2-carboxyate;ethyl 6-broMo-1H-indol-2-carboxylate
CBNumber: CB5196593
Molecular Formula: C11H10BrNO2
Formula Weight: 268.11
MOL File: 103858-53-3.mol

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Ethyl 6-bromoindole-2-carboxylate Property

Melting point:: 178-180 °C
Boiling point:: 394.7±22.0 °C(Predicted)
Density: 1.554±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
solubility: Soluble in acetone.
form: Crystalline Powder
pka: 14.08±0.30(Predicted)
color: White
CAS DataBase Reference: 103858-53-3(CAS DataBase Reference)

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Safety

Risk Statements: 20/21/22
Safety Statements: 36/37
HazardClass: IRRITANT
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Alfa Aesar

Product number: H63187
Product name: Methyl 6-bromoindole-2-carboxylate, 97%
Packaging: 1g
Price: $69.2
Updated: 2021/12/16

Alfa Aesar

Product number: H63187
Product name: Methyl 6-bromoindole-2-carboxylate, 97%
Packaging: 5g
Price: $288
Updated: 2021/12/16

Alfa Aesar

Product number: H63187
Product name: Methyl 6-bromoindole-2-carboxylate, 97%
Packaging: 250mg
Price: $21.7
Updated: 2021/12/16

TRC

Product number: E900863
Product name: Ethyl6-bromo-1H-indole-2-carboxylate
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 046758
Product name: Ethyl 6-bromo-1H-indole-2-carboxylate
Purity: >95%
Packaging: 500mg
Price: $35
Updated: 2021/12/16

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Ethyl 6-bromoindole-2-carboxylate Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

In a 250mL three-necked flask, add 80mL of ethanol and 7.2g (40mmol) of 6-bromo-2-indolecarboxylic acid, slowly drop 1.0mL of concentrated sulfuric acid at room temperature and reflux for 30h (TLC tracking). After the reaction, concentrate to 30mL and pour into 60mL of water, extract twice with 20mL of ether, wash the ether layer once with 5% sodium carbonate solution, and then wash with water until neutral, dry with anhydrous magnesium sulfate, and evaporate the ether to obtain 7.7g of yellow to brown powder Ethyl 6-bromoindole-2-carboxylate, with a yield of 92.3%.

Ethyl 6-bromoindole-2-carboxylate Preparation Products And Raw materials

Raw materials

Xylene Hexane Sodium azide Ethanol Acetone Sodium Ammonium chloride Dichloromethane 2,5-Di-tert-butylhydroquinone 4-Bromobenzaldehyde Ethyl chloroacetate

Preparation Products

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Ethyl 6-bromoindole-2-carboxylate Suppliers

China 122 France 1 Germany 2 India 1 Switzerland 2 The Netherlands 1 United Kingdom 4 United States 18 Global 151

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View Lastest Price from Ethyl 6-bromoindole-2-carboxylate manufacturers

Career Henan Chemical Co

Product: Ethyl 6-bromoindole-2-carboxylate 103858-53-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-26

103858-53-3, Ethyl 6-bromoindole-2-carboxylateRelated Search:

Indole-3-acetic acid Diethyl 1,3-acetonedicarboxylate Indole-2-carboxylic acid Tris(trimethylsilyl)phosphate Ethylparaben Indole-3-butyric acid Ethanol Indometacin 1-Cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxo-3-quinolinecarboxylic acid ethyl ester Ethyl acetate Ethyl bromodifluoroacetate Ethyl bromoacetate ISOXADIFEN-ETHYL 6-Bromo-1H-indole 2-Ethoxyethanol RESMETHRIN 6-Bromoindole-2-carboxylic acid Trinexapac-ethyl

6-BROMOINDOLE-2-CARBOXYLIC ACID ETHYL ESTER

6-BROMO-2-CARBETHOXYINDOLE

ETHYL 6-BROMOINDOLE-2-CARBOXYLATE

SPECS AR-437/43285096

6-BROMO-2-INDOLECARBOXYLIC METHYL ESTER

6-6-BROMO-2-INDOLECARBOXYLIC

6-6-BROMO-2-INDOLECARBOXYLICMETHYLESTER

6-Br-ICA-OEt

ethyl 6-bromo-1H-indole-2-carboxylate

6-Bromoindole-2-carboxylic acid methyl ester

Ethyl 6-bromoindole-2-carboxylate ,97%

6-Bromo-2-(ethoxylcarbonyl)-1H-indole

ethyl 6-broMo-1H-indol-2-carboxylate

6-BroMo-2-Indolecarboxylic ethyl ester

1H-Indole-2-carboxylic acid, 6-broMo-, ethyl ester

Methyl 6-broMoindole-2-carboxylate, 97%

Ethyl 6-bromoindole-2-carboxylat

Methyl 6-bromoindole-2-carboxyate

6-Bromo-2- carboethoxyindole

Ethyl 6-Bromoindole-2-carboxylate≥ 98.5% (HPLC)

Ethyl 6-bromo-1H-indole-2-carboxylate 98%

6-Bromo-1H-indole-2-carboxylic acid ethyl ester

Methyl6-bromoindole-2-carboxylate,97%

6-bromoindole-2-carboxylate

1H-Indole-2-carboxylic acid, 6-bromo-, ethyl ester (9CI, ACI)

6-bromo-1H-Indole-2-carboxylic acid ethyl ester (9CI ACI)

103858-53-3

327089-59-3

Indoles

Indole/indoline/oxindole