D(+)-10-Camphorsulfonyl chloride

Product Name: D(+)-10-Camphorsulfonyl chloride
CAS No.: 21286-54-4
Chemical Name: D(+)-10-Camphorsulfonyl chloride
Synonyms: Camphor-10-suL;D(+)CAMPHOR SULFONYL CHLORIDE;D-CAMPHOR-10-SULFONYL CHLORIDE;S-(+)-caMphorsulfonyl chloride;(+)-10-CAMPHORSULFONYL CHLORIDE;D(+)-1-CaMphorsulfonyl chloride;(+)-10-Camphorsulfonyl Chloride;(+)-CAMPHOR-10-SULFONYL CHLORIDE;D(+)-10-CAMPHORSULFONYL CHLORIDE;D-CAMPHOR-10-SULFONYL CHLORIDE 96%
CBNumber: CB5775185
Molecular Formula: C10H15ClO3S
Formula Weight: 250.74
MOL File: 21286-54-4.mol

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D(+)-10-Camphorsulfonyl chloride Property

Melting point:: 67-68 °C
alpha: 33 º (c=1, CHCl3 22 ºC)
Boiling point:: 349.4±15.0 °C(Predicted)
Density: 1.2078 (estimate)
refractive index: 32 ° (C=1, CHCl3)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), Ethyl Acetate (Slightly)
form: Crystalline Powder
color: Off-white to beige
optical activity: [α]22/D +33°, c = 1 in chloroform
Sensitive: Moisture Sensitive
BRN: 3205974
InChIKey: BGABKEVTHIJBIW-UHFFFAOYSA-N
CAS DataBase Reference: 21286-54-4(CAS DataBase Reference)
NIST Chemistry Reference: (+)-Camphor-10-sulfonyl chloride(21286-54-4)

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Safety

Hazard Codes: C
Risk Statements: 34
Safety Statements: 26-36/37/39-45
RIDADR: UN 3261 8/PG 2
WGK Germany: 3
F: 10-21
HazardClass: 8
PackingGroup: II
HS Code: 29147000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 219576
Product name: (1S)-(+)-10-Camphorsulfonyl chloride
Purity: 97%
Packaging: 5g
Price: $43.7
Updated: 2024/03/01

Sigma-Aldrich

Product number: 219576
Product name: (1S)-(+)-10-Camphorsulfonyl chloride
Purity: 97%
Packaging: 25g
Price: $159
Updated: 2024/03/01

TCI Chemical

Product number: C0998
Product name: (+)-10-Camphorsulfonyl Chloride
Purity: >97.0%(GC)(T)
Packaging: 5g
Price: $26
Updated: 2024/03/01

TCI Chemical

Product number: C0998
Product name: (+)-10-Camphorsulfonyl Chloride
Purity: >97.0%(GC)(T)
Packaging: 25g
Price: $77
Updated: 2024/03/01

Sigma-Aldrich

Product number: 219576
Product name: (1S)-(+)-10-Camphorsulfonyl chloride
Purity: 97%
Packaging: 100g
Price: $587
Updated: 2024/03/01

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D(+)-10-Camphorsulfonyl chloride Chemical Properties,Usage,Production

Chemical Properties

white to light yellow crystal powde

Uses

A chiral derivative of Camphor.

Uses

As a useful synthetic intermediate, D(+)-10-Camphorsulfonyl chloride can be used for asymmetric hydroxylation

Purification Methods

If free from OH bands in the IR, then recrystallise it from Et2O or pet ether; otherwise treat it with SOCl2 at 50o for 30minutes, evaporate, dry the residue over KOH in a vacuum and recrystallise it. The (±)-acid chloride has m 85o [Bartlett & Knox Org Synth 45 14 1965]. Itis characterised as the amide (prisms from EtOH) m 132o, [ ] 17 (+) and (-) 1.5o (EtOH). On repeated recrystallisation from EtOH the anilide has m 120.5-121o, [] 25 +76o (c 1, CHCl3). [Read & Storey J Chem Soc 2761 1930, Sutherland & Shriner J Am Chem Soc 58 62 1936, Halterman et al. J Am Chem Soc 109 8105 1987, Bartlet & Knox Org Synth 45 55 1945, Beilstein 11 IV 650.]

D(+)-10-Camphorsulfonyl chloride Preparation Products And Raw materials

Raw materials

Preparation Products

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D(+)-10-Camphorsulfonyl chloride Suppliers

Americas 1 Austria 1 Belgium 2 Canada 1 China 132 Europe 3 France 2 Germany 4 India 10 Japan 4 Switzerland 2 The Netherlands 1 United Kingdom 15 United States 35 Global 213

Shanghai Chang-Gen Chemical Technology Co., Ltd.

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Alfa Aesar

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Energy Chemical

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Beijing Ouhe Technology Co., Ltd

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JinYan Chemicals(ShangHai) Co.,Ltd.

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View Lastest Price from D(+)-10-Camphorsulfonyl chloride manufacturers

Honest Joy Holdings Limited

Product: D(+)-10-Camphorsulfonyl chloride 21286-54-4
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.9%
Supply Ability: 100 tons
Release date: 2022-01-26

Career Henan Chemical Co

Product: D(+)-10-Camphorsulfonyl chloride 21286-54-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-08

21286-54-4, D(+)-10-Camphorsulfonyl chlorideRelated Search:

4-Nitrobenzenesulfonyl chloride N-Acetylsulfanilyl chloride D-CAMPHOR Sodium chloride Benzenesulfonyl chloride Zinc chloride Potassium chloride Camphor Oxalyl chloride Choline chloride Ethanesulfonyl chloride Tosyl chloride Thionyl chloride Calcium chloride Ammonium chloride Sulfuryl chloride (1S)-(+)-Camphor-10-sulphonic acid (+)-GALLOCATECHIN

(+)-10-CAMPHORSULFONYL CHLORIDE

d-2-oxobornane-10-sulphonyl chloride

(1S)-(+)-10-CAMPHORSULFONYL CHLORIDE

(1S)-CAMPHOR-10-SULFONIC ACID CHLORIDE

(1S)-(+)-CAMPHOR-10-SULFONYL CHLORIDE

(1S)-(+)-CAMPHOR-10-SULPHONYL CHLORIDE

D-CAMPHOR-10-SULFONYL CHLORIDE

D(+)-10-CAMPHORSULFONYL CHLORIDE

(+) CAMPHOR-10-SULFONIC ACID CHLORIDE

(+)-CAMPHOR-10-SULFONYL CHLORIDE

(1S)-(+)-10-CAMPHORSULFONYL CHLORIDE, 97 %

D-CAMPHOR-10-SULFONYL CHLORIDE 96%

(S)-(+)-Camphor-10-SulfonylChloride

D(+)CAMPHOR SULFONYL CHLORIDE

[(1R,4S)-7,7-dimethyl-3-oxo-4-bicyclo[2.2.1]heptanyl]methanesulfonyl chloride

(7,7-dimethyl-3-oxo-4-bicyclo[2.2.1]heptanyl)methanesulfonyl chloride

(1S)-(+)-10-Camphorsulphonyl Chloride

(+)-Camphor-10-sulfonyl chloride, (1S)-Camphor-10-sulfonic acid chloride

Bicyclo[2.2.1]heptane-1-methanesulfonyl chloride, 7,7-dimethyl-2-oxo-

D-2-Oxobornane-10-sulfonyl chloride

D(+)-1-CaMphorsulfonyl chloride

(1S,4R)-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfochloride

[1S,4R,(+)]-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfonic acid chloride

D(+)-10-Camphorsulfonyl chloride,97%

(+)-10-CaMphorsulfonic Acid Chloride

(1S,4R)-7,7-DiMethyl-2-oxo-bicyclo[2.2.1]heptane-1-Methanesulfonyl Chloride

S-(+)-caMphorsulfonyl chloride

((1S,4R)-7,7-DiMethyl-2-oxobicyclo[2.2.1]heptan-1-yl)Methanesulfonyl chloride

Bicyclo[2.2.1]heptane-1-methanesulfonyl chloride, 7,7-dimethyl-2-oxo-, (1S)-

Dextro-10-camphorsulfonyl chloride

D(+)-10-CaMphorsulfonyl chloride, 97% 5GR

(1S)-(+)-10-Camphorsulfonyl chloride 97%

Camphor-10-suL

Bicyclo[2.2.1]heptane-1-methanesulfonyl chloride, 7,7-dimethyl-2-oxo-, (1S,4R)-

(+)-10-Camphorsulfonyl Chloride

21286-54-4

2186-54-4

C10H15ClO3S

UV-VIS

Chiral Resolving Reagents

Chiral Resolution Reagents

Optical Resolution

Asymmetric Synthesis

for Resolution of Alcohols & Thiols

Bicyclic Monoterpenes

Terpenes

for Resolution of Bases

chiral

Chiral Reagents

Bicyclic Monoterpenes

Biochemistry

for Resolution of Alcohols & Thiols

for Resolution of Bases

Optical Resolution

Synthetic Organic Chemistry

Terpenes

Intermediates & Fine Chemicals

Pharmaceuticals