ChemicalBook > CAS DataBase List > Methyl 6-broMo-3-Methoxypicolinate

Methyl 6-broMo-3-Methoxypicolinate

Product Name: Methyl 6-broMo-3-Methoxypicolinate
CAS No.: 945954-94-9
Chemical Name: Methyl 6-broMo-3-Methoxypicolinate
Synonyms: Methyl 6-broMo-3-Methoxypicolinate;methyl 6-bromo-3-methoxypyridine-2-carboxylate;methyl 6-bromo-3-methoxypyridine-2-carboxylate - [AC80521];2-Pyridinecarboxylic acid, 6-bromo-3-methoxy-, methyl ester
CBNumber: CB62549552
Molecular Formula: C8H8BrNO3
Formula Weight: 246.06
MOL File: 945954-94-9.mol

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Methyl 6-broMo-3-Methoxypicolinate Property

Boiling point:: 338.2±37.0 °C(Predicted)
Density: 1.530±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: -1.56±0.10(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: HCH0369577
Product name: METHYL-6-BROMO-3-METHOXYPICOLINATE
Purity: 95.00%
Packaging: 5MG
Price: $499.8
Updated: 2021/12/16

Matrix Scientific

Product number: 143724
Product name: Methyl 6-bromo-3-methoxypicolinate
Purity: 95%
Packaging: 1g
Price: $1388
Updated: 2021/12/16

Matrix Scientific

Product number: 143724
Product name: Methyl 6-bromo-3-methoxypicolinate
Purity: 95%
Packaging: 5g
Price: $4163
Updated: 2021/12/16

Ambeed

Product number: A167550
Product name: Methyl6-bromo-3-methoxypicolinate
Purity: 98%
Packaging: 5g
Price: $754
Updated: 2021/12/16

Chemenu

Product number: CM126470
Product name: methyl6-bromo-3-methoxypicolinate
Purity: 98%
Packaging: 5g
Price: $857
Updated: 2021/12/16

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Methyl 6-broMo-3-Methoxypicolinate Chemical Properties,Usage,Production

Synthesis

321601-48-3

74-88-4

945954-94-9

General procedure for the synthesis of methyl 6-bromo-3-methoxypyridine carboxylate from methyl 6-bromo-3-hydroxypyridine-2-carboxylate and iodomethane: Methyl 6-bromo-3-hydroxypyridine-2-carboxylate (4 g, 17.2 mmol), iodomethane (7.15 g, 34.5 mmol) and potassium carbonate (4.76 g, 34.5 mmol) were dissolved in N,N- dimethylformamide (50 mL) and the reaction was stirred at room temperature for 3 hours. After completion of the reaction, the reaction mixture was concentrated under reduced pressure, diluted with water and extracted with ethyl acetate (50 mL x 3). The organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product methyl 6-bromo-3-methoxypyridinecarboxylate (4 g, yield: 90%). The product was identified by NMR hydrogen spectroscopy (CDCl3, 400 MHz): δ 7.56 (d, J = 8.0 Hz, 1H), 7.25 (d, J = 8.0 Hz, 1H), 3.94 (s, 3H), 3.90 (s, 3H). Mass spectrum (M + H)+: 256/258.

References

[1] Patent: WO2014/121418, 2014, A1. Location in patent: Page/Page column 45
[2] Patent: EP3255042, 2017, A2. Location in patent: Paragraph 0180; 0183
[3] Patent: WO2007/89031, 2007, A1. Location in patent: Page/Page column 84-85
[4] Patent: WO2014/209727, 2014, A1. Location in patent: Page/Page column 39
[5] Patent: WO2014/205593, 2014, A1. Location in patent: Page/Page column 41; 42

Methyl 6-broMo-3-Methoxypicolinate Preparation Products And Raw materials

Raw materials

Preparation Products

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945954-94-9, Methyl 6-broMo-3-MethoxypicolinateRelated Search:

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Methyl 6-broMo-3-Methoxypicolinate

methyl 6-bromo-3-methoxypyridine-2-carboxylate

2-Pyridinecarboxylic acid, 6-bromo-3-methoxy-, methyl ester

methyl 6-bromo-3-methoxypyridine-2-carboxylate - [AC80521]

945954-94-9