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1-Diphenylmethylazetidine

Product Name
1-Diphenylmethylazetidine
CAS No.
107128-00-7
Chemical Name
1-Diphenylmethylazetidine
Synonyms
RMA-298;1-benzhydrylazetane;1-Benzhydrylazetidine;N-Benzhydrylazetidine;LABOTEST-BB LT00159241;N-(Diphenylmethyl)azetidine;1-(DIPHENYLMETHYL)AZETIDINE;1-(DiphenylMethyl)azetidine7.;Azetidine, 1-(diphenylmethyl)-;1-Diphenylmethylazetidine ISO 9001:2015 REACH
CBNumber
CB7184080
Molecular Formula
C16H17N
Formula Weight
223.31
MOL File
107128-00-7.mol
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1-Diphenylmethylazetidine Property

Melting point:
109-112 °C (lit.)
Boiling point:
307.7±11.0 °C(Predicted)
Density 
1.093±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
7.44±0.10(Predicted)
Appearance
White to off-white Solid
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
406031
Product name
1-(Diphenylmethyl)azetidine
Purity
98%
Packaging
25g
Price
$182
Updated
2023/06/20
TRC
Product number
B194850
Product name
1-Benzhydrylazetidine
Packaging
1g
Price
$130
Updated
2021/12/16
AK Scientific
Product number
I813
Product name
1-(Diphenylmethyl)azetidine
Packaging
5g
Price
$123
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB18193
Product name
1-Benzhydrylazetidine
Packaging
500mg
Price
$125
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB18193
Product name
1-Benzhydrylazetidine
Packaging
1g
Price
$218.1
Updated
2021/12/16
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1-Diphenylmethylazetidine Chemical Properties,Usage,Production

Uses

Azetidine derivatives as antiarrhythmic agents

Uses

1-(Diphenylmethyl)azetidine may be used in the preparation of monofunctional poly(tetrahydrofuran), (poly(THF)), having a 1-(diphenylmethyl)azetidinium end group.

Synthesis Reference(s)

Synthetic Communications, 18, p. 205, 1988 DOI: 10.1080/00397918808077346

General Description

1-(Diphenylmethyl)azetidine is a N-containing heterocyclic building block.

Synthesis

109-70-6

91-00-9

71-36-3

107128-00-7

Example 1 Synthesis of N-diphenylmethylazetidine: To a 7.5 liter aqueous solution containing 6.9 kg (50 moles) of potassium carbonate, 18.5 liters of n-butanol, 7.85 kg (50 moles) of 1-bromo-3-chloropropane, and 5.18 kg (25 moles, 97% purity, with 10% toluene as a residual solvent) of dibenzidine were sequentially added. The reaction mixture was heated to 100 °C with external steam under nitrogen protection and stirred slowly overnight. Upon completion of the reaction, about 12 liters of water were added to the mixture to dissolve the inorganic salt precipitate formed. The organic and aqueous layers were separated and about 18 liters of n-butanol and water were removed from the organic layer by distillation under reduced pressure. To the distillation residue 1.5 liters of methanol was added, slowly stirred and cooled to room temperature. The precipitated white solid was collected by filtration, washed twice with 700 mL of methanol and finally dried in a vacuum oven to give 4.2 kg (75% yield) of N-diphenylmethylazetidine with a melting point of 205°C (literature value: 107°-109°).

References

[1] Patent: US4870189, 1989, A

1-Diphenylmethylazetidine Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Diphenylmethylazetidine Suppliers

Carbosynth
Tel
--
Fax
--
Email
sales@carbosynth.com
Country
United Kingdom
ProdList
6005
Advantage
58
MOLEKULA Ltd.
Tel
--
Fax
--
Email
kevinbanks@molekula.com
Country
United Kingdom
ProdList
6140
Advantage
66
Fluorochem Ltd.
Tel
--
Fax
--
Email
enquiries@fluorochem.co.uk
Country
United Kingdom
ProdList
6401
Advantage
74
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View Lastest Price from 1-Diphenylmethylazetidine manufacturers

PNP Biotech Co. Ltd
Product
1-benzhydrylazetane 107128-00-7
Price
US $0.00/KG
Min. Order
25KG
Purity
98%
Supply Ability
Inquiry
Release date
2022-09-19
Henan Fengda Chemical Co., Ltd
Product
1-Diphenylmethylazetidine 107128-00-7
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-26

107128-00-7, 1-DiphenylmethylazetidineRelated Search:


  • LABOTEST-BB LT00159241
  • 1-(DIPHENYLMETHYL)AZETIDINE
  • N-Benzhydrylazetidine
  • 1-Benzhydrylazetidine
  • N-(Diphenylmethyl)azetidine
  • 1-(DiphenylMethyl)azetidine7.
  • Azetidine, 1-(diphenylmethyl)-
  • 1-Diphenylmethylazetidine ISO 9001:2015 REACH
  • 1-benzhydrylazetane
  • RMA-298
  • 107128-00-7
  • Building Blocks
  • Others
  • N-Containing
  • Heterocyclic Building Blocks
  • Aromatics
  • Heterocycles
  • Heterocyclic Building Blocks
  • N-Containing
  • Others