1-Chloro-3-iodobenzene
- Product Name
- 1-Chloro-3-iodobenzene
- CAS No.
- 625-99-0
- Chemical Name
- 1-Chloro-3-iodobenzene
- Synonyms
- 3-CHLOROIODOBENZENE;oroiodobenzene;3-chloroiodine;Chloriodobenzene;3-Iodochlorobenzene;M-IODOCHLOROBENZENE;M-CHLOROIODOBENZENE;m-Chlorophenyl iodide;1-CHLORO-3-IODOBENZENE;3-Chloro-1-iodobenzene
- CBNumber
- CB7286689
- Molecular Formula
- C6H4ClI
- Formula Weight
- 238.45
- MOL File
- 625-99-0.mol
1-Chloro-3-iodobenzene Property
- Melting point:
- 95-96 °C
- Boiling point:
- 103-104 °C15 mm Hg(lit.)
- Density
- 1.926 g/mL at 25 °C(lit.)
- refractive index
- n20/D 1.631(lit.)
- Flash point:
- 215 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- Liquid
- Specific Gravity
- 1.926
- color
- Clear light yellow
- Water Solubility
- Soluble in water 67.2 mg/L.
- Sensitive
- Light Sensitive
- BRN
- 1904539
- CAS DataBase Reference
- 625-99-0(CAS DataBase Reference)
- NIST Chemistry Reference
- Benzene, 1-chloro-3-iodo-(625-99-0)
- EPA Substance Registry System
- Benzene, 1-chloro-3-iodo- (625-99-0)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 242578
- Product name
- 3-Chloroiodobenzene
- Purity
- 98%
- Packaging
- 5g
- Price
- $44.2
- Updated
- 2025/07/31
- Product number
- 242578
- Product name
- 3-Chloroiodobenzene
- Purity
- 98%
- Packaging
- 25g
- Price
- $135
- Updated
- 2023/06/20
- Product number
- C0190
- Product name
- 1-Chloro-3-iodobenzene (stabilized with Copper chip)
- Packaging
- 5G
- Price
- $20
- Updated
- 2025/07/31
- Product number
- C0190
- Product name
- 1-Chloro-3-iodobenzene (stabilized with Copper chip)
- Packaging
- 25G
- Price
- $78
- Updated
- 2025/07/31
- Product number
- C349590
- Product name
- 3-Chloroiodobenzene
- Packaging
- 5g
- Price
- $45
- Updated
- 2021/12/16
1-Chloro-3-iodobenzene Chemical Properties,Usage,Production
Chemical Properties
Clear light yellow liquid
Uses
suzuki reaction
Uses
1-Chloro-3-iodobenzene is used as a pharmaceutical intermediate.
Synthesis Reference(s)
Synthetic Communications, 11, p. 639, 1981 DOI: 10.1080/00397918108063637
General Description
The multiple-quantum proton NMR spectra of 3-chloroiodobenzene was studied.
Synthesis
63503-60-6
625-99-0
General procedure for the synthesis of m-chloroiodobenzene from 3-chlorophenylboronic acid: a mixture of arylboronic acid (0.55 mmol), KF (96 mg, 1.65 mmol) and I2 (127 mg, 0.50 mmol) in 1,4-dioxane (5 mL) was stirred and reacted for 1 hr at 80 °C. After completion of the reaction, the mixture was filtered through a silica gel column and eluted with ether (10 mL). Subsequently, the solvent was removed by rotary evaporator. For further purification, the target product, m-chloroiodobenzene, was isolated by silica gel column chromatography using petroleum ether/ether (98:2) as eluent.
References
[1] Chemistry - A European Journal, 2011, vol. 17, # 20, p. 5652 - 5660
[2] Tetrahedron Letters, 2015, vol. 56, # 9, p. 1122 - 1123
[3] Synlett, 1998, # 2, p. 141 - 142
[4] Synlett, 2014, vol. 25, # 7, p. 995 - 1000
1-Chloro-3-iodobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-Chloro-3-iodobenzene manufacturers
- Product
- 1-Chloro-3-iodobenzene 625-99-0
- Price
- US $30.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 5000kg/week
- Release date
- 2024-04-24
- Product
- 1-Chloro-3-iodobenzene 625-99-0
- Price
- US $100.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-26
- Product
- 1-Chloro-3-iodobenzene 625-99-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-11