ChemicalBook > CAS DataBase List > 2'-Fluoroacetanilide

2'-Fluoroacetanilide

Product Name
2'-Fluoroacetanilide
CAS No.
399-31-5
Chemical Name
2'-Fluoroacetanilide
Synonyms
2-FLUOROACETANILINE;2-FLUOROACETANILIDE;O-FLUOROACETANILIDE;2'-Fluoroacetanilide;2'-Fluoroacetanilide>Flurbiprofen Impurity 23;N-Acetyl 2-fluoroaniline;2-Fluorophenyl acetamide;2-Fluoroacetanilide, 98+%;N-(2-Fluorphenyl)acetamid
CBNumber
CB7776328
Molecular Formula
C8H8FNO
Formula Weight
153.15
MOL File
399-31-5.mol
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2'-Fluoroacetanilide Property

Melting point:
77-79 °C(lit.)
Boiling point:
140-142 °C14 mm Hg(lit.)
Density 
1.1655 (estimate)
Flash point:
140-142°C/14mm
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Methanol
pka
14.04±0.70(Predicted)
form 
Fine Crystalline Powder
color 
White
BRN 
2717443
CAS DataBase Reference
399-31-5(CAS DataBase Reference)
NIST Chemistry Reference
Acetamide, N-(2-fluorophenyl)-(399-31-5)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39-36
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29242998
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
F0524
Product name
2'-Fluoroacetanilide
Purity
>98.0%(GC)
Packaging
25g
Price
$53
Updated
2025/07/31
TRC
Product number
F587065
Product name
2''-Fluoroacetanilide
Packaging
5g
Price
$75
Updated
2021/12/16
TRC
Product number
F587065
Product name
2''-Fluoroacetanilide
Packaging
500mg
Price
$45
Updated
2021/12/16
SynQuest Laboratories
Product number
4648-3-02
Product name
2-Fluoroacetanilide
Purity
98%
Packaging
5G
Price
$15
Updated
2021/12/16
AK Scientific
Product number
J97987
Product name
2'-Fluoroacetanilide
Packaging
25g
Price
$18
Updated
2021/12/16
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2'-Fluoroacetanilide Chemical Properties,Usage,Production

Chemical Properties

white fine crystalline powder

Uses

2''-Fluoroacetanilide

Synthesis

348-54-9

108-24-7

399-31-5

Step 1: Synthesis of N-(2-fluorophenyl)acetamide To a solution of 2-fluoroaniline (5.0 g, 45.05 mmol) in dichloromethane (DCM, 225 mL) was sequentially added acetic anhydride (4.09 mL, 45.05 mmol) and triethylamine (7.55 mL, 54.05 mmol). The reaction mixture was stirred at room temperature for 6 hours. After completion of the reaction, the mixture was concentrated, diluted with ethyl acetate and washed with 1N hydrochloric acid (2 x 50 mL). The organic phase was dried with anhydrous sodium sulfate (Na2SO4) and concentrated to give N-(2-fluorophenyl)acetamide (6.20 g, 90% yield) as a white solid.LCMS analysis showed the molecular ion peak of the target product to be 153.99 (M + H)+.

References

[1] Journal of Medicinal Chemistry, 2003, vol. 46, # 11, p. 2187 - 2196
[2] Patent: US2008/139558, 2008, A1. Location in patent: Page/Page column 80
[3] Journal of the Chemical Society - Perkin Transactions 1, 1996, # 7, p. 669 - 673
[4] Patent: US2012/238543, 2012, A1. Location in patent: Page/Page column 13
[5] Patent: US2012/270854, 2012, A1. Location in patent: Page/Page column 20

2'-Fluoroacetanilide Preparation Products And Raw materials

Raw materials

Preparation Products

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2'-Fluoroacetanilide Suppliers

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View Lastest Price from 2'-Fluoroacetanilide manufacturers

Honest Joy Holdings Limited
Product
2'-Fluoroacetanilide 399-31-5
Price
US $0.00/KG
Min. Order
1KG
Purity
99.1%
Supply Ability
100 tons
Release date
2022-01-14
Career Henan Chemical Co
Product
2'-Fluoroacetanilide 399-31-5
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-14

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  • Building Blocks
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  • Anilines, Amides & Amines
  • Fluorine Compounds
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  • Organic Building Blocks
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