ChemicalBook > CAS DataBase List > 5-Bromo-6-chloropyridin-3-amine
5-Bromo-6-chloropyridin-3-amine
- Product Name
- 5-Bromo-6-chloropyridin-3-amine
- CAS No.
- 130284-53-6
- Chemical Name
- 5-Bromo-6-chloropyridin-3-amine
- Synonyms
- 5-Amino-3-bromo-2-chL;5-BROMO-6-CHLOROPYRIDIN-3-AMINE;5-Bromo-6-chloro-3-pyridinamine;5-bromo-6-chloropyridin-3-aminr;2-chloro-3-bromopyridin-5-amine;2-Chloro-3-Bromo-5-Amiopyridine;5-AMino-2-chloro-3-broMopyridine;3-Amino-5-bromo-6-chloropyridine;5-BROMO-6-CHLORO-3-AMINOPYRIDINE;2-chloro-3-bromo-5-aminopyridine
- CBNumber
- CB8245566
- Molecular Formula
- C5H4BrClN2
- Formula Weight
- 207.46
- MOL File
- 130284-53-6.mol
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5-Bromo-6-chloropyridin-3-amine Property
- Melting point:
- 120-122°C
- Boiling point:
- 336.7±37.0 °C(Predicted)
- Density
- 1.834±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- form
- powder to crystal
- pka
- 0.86±0.10(Predicted)
- color
- Light yellow to Brown
- CAS DataBase Reference
- 130284-53-6(CAS DataBase Reference)
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 738972
- Product name
- 5-Amino-3-bromo-2-chloropyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $65.6
- Updated
- 2023/06/20
TCI Chemical
- Product number
- A2539
- Product name
- 5-Amino-3-bromo-2-chloropyridine
- Purity
- >95.0%(GC)
- Packaging
- 1g
- Price
- $17
- Updated
- 2024/03/01
TCI Chemical
- Product number
- A2539
- Product name
- 5-Amino-3-bromo-2-chloropyridine
- Purity
- >95.0%(GC)
- Packaging
- 5g
- Price
- $51
- Updated
- 2024/03/01
TRC
- Product number
- B699633
- Product name
- 5-Bromo-6-chloropyridin-3-amine
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 024809
- Product name
- 5-Amino-3-bromo-2-chloropyridine
- Purity
- 95%
- Packaging
- 25g
- Price
- $47
- Updated
- 2021/12/16
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5-Bromo-6-chloropyridin-3-amine Chemical Properties,Usage,Production
Synthesis
In a 250 mL round bottom flask, 3-bromo-2-chloro-5-nitropyridine (3 g, 12.63 mmol), ammonium chloride (1.35 g, 25.2 mmol) and zinc dust (8.79 g, 134 mmol) were suspended in MeOH (50 ml). The reaction mixture was heated for 2 hrs at 90 °C. The reaction was cooled to room temperature, filtered over celite, and concentrated in vacuo. The resulting solid was adsorbed onto silica and purified by silica gel chromatography (25-55percent EtO Ac/Heptane). 5-Bromo-6-chloropyridin-3-amine (1.85 g, 8.92 mmol, 70.6 per cent yield) was obtained as a yellow solid.
5-Bromo-6-chloropyridin-3-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-Bromo-6-chloropyridin-3-amine manufacturers
Shaanxi Dideu Medichem Co. Ltd
- Product
- 2-Chloro-3-bromo-5-aminopyridine 130284-53-6
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.0% min
- Supply Ability
- 100 tons min
- Release date
- 2021-05-06
Henan Fengda Chemical Co., Ltd
- Product
- 2-Chloro-3-bromo-5-aminopyridine 130284-53-6
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-08
Career Henan Chemical Co
- Product
- 2-Chloro-3-bromo-5-aminopyridine 130284-53-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg; 10kg; 100kg
- Release date
- 2019-08-30
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