3-(METHOXYMETHYL)ANILINE
- Product Name
- 3-(METHOXYMETHYL)ANILINE
- CAS No.
- 53473-83-9
- Chemical Name
- 3-(METHOXYMETHYL)ANILINE
- Synonyms
- AKOS MSC-0194;3-(METHOXYMETHYL)ANILINE;3-(Methoxymethyl)benzenamine;Benzenamine, 3-(methoxymethyl)-;[3-(methoxymethyl)phenyl]amine sulfate (salt)
- CBNumber
- CB8380764
- Molecular Formula
- C8H11NO
- Formula Weight
- 137.18
- MOL File
- 53473-83-9.mol
3-(METHOXYMETHYL)ANILINE Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- Light yellow to yellow Liquid
Safety
- HS Code
- 2922190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P322Specific measures (see …on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P363Wash contaminated clothing before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M329153
- Product name
- 3-(Methoxymethyl)aniline
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 156386
- Product name
- [3-(Methoxymethyl)phenyl]amine sulfate (salt)
- Packaging
- 1g
- Price
- $400
- Updated
- 2021/12/16
- Product number
- OR952259
- Product name
- 3-(Methoxymethyl)aniline
- Purity
- 98%
- Packaging
- 1g
- Price
- $167
- Updated
- 2021/12/16
- Product number
- V6465
- Product name
- 3-(Methoxymethyl)aniline
- Packaging
- 1g
- Price
- $169
- Updated
- 2021/12/16
- Product number
- 156386
- Product name
- [3-(Methoxymethyl)phenyl]amine sulfate (salt)
- Packaging
- 0.500g
- Price
- $320
- Updated
- 2021/12/16
3-(METHOXYMETHYL)ANILINE Chemical Properties,Usage,Production
Synthesis
1515-84-0
53473-83-9
General procedure for the synthesis of m-(methoxymethyl)aniline from 1-(methoxymethyl)-3-nitrobenzene: 3-(methoxymethyl)nitrobenzene (4.18 g, 25 mmol) from the previous step was dissolved in 160 mL of acetic acid. Zinc powder (5 g, 76.5 mmol) was added to the solution and the reaction mixture was stirred at room temperature for 18 h until HPLC analysis showed no 3-(methoxymethyl)nitrobenzene residue. Upon completion of the reaction, the mixture was filtered through diatomaceous earth and the filtrate was subsequently concentrated under vacuum. The concentrated residue was dissolved in ethyl acetate and washed with saturated aqueous sodium bicarbonate. The organic layer was further washed with water and dried with anhydrous magnesium sulfate. Finally, the dried organic phase was concentrated under vacuum to give 3.4 g (99% yield) of the target product 3-(methoxymethyl)aniline as a brown oil.
References
[1] European Journal of Organic Chemistry, 2015, vol. 2015, # 10, p. 2282 - 2290
[2] Journal of the American Chemical Society, 2010, vol. 132, # 50, p. 17910 - 17920
[3] Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 3, p. 1430 - 1438
[4] Journal of the Chemical Society, 1954, p. 4127,4132
[5] Zhurnal Obshchei Khimii, 1955, vol. 25, p. 2290,2292; engl. Ausg. S. 2259, 2261
3-(METHOXYMETHYL)ANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
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