6-CHLORO-2-CYANO-3-NITROPYRIDINE

Product Name: 6-CHLORO-2-CYANO-3-NITROPYRIDINE
CAS No.: 93683-65-9
Chemical Name: 6-CHLORO-2-CYANO-3-NITROPYRIDINE
Synonyms: 6-Chloro-3-nitropicolinonitrile;C90144;6-Chloro-2-cyano-3-nitropyidine;6-CHLORO-2-CYANO-3-NITROPYRIDIN;6-CHLORO-2-CYANO-3-NITROPYRIDINE;2-cyano-6-chloro-3-nitropyridine;6-chloro-3-nitro-2-pyridinecarbonitrile;6-CHLORO-3-NITROPYRIDINE-2-CARBONITRILE;2-Pyridinecarbonitrile, 6-chloro-3-nitro-;6-Chloro-3-nitro-2-cyanopyridine≥ 97.0% (HPLC)
CBNumber: CB8689052
Molecular Formula: C6H2ClN3O2
Formula Weight: 183.55
MOL File: 93683-65-9.mol

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6-CHLORO-2-CYANO-3-NITROPYRIDINE Property

Melting point:: 118-120 °C
Boiling point:: 347.2±42.0 °C(Predicted)
Density: 1.57±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
pka: -10.14±0.10(Predicted)
Appearance: White to light yellow Solid
InChI: InChI=1S/C6H2ClN3O2/c7-6-2-1-5(10(11)12)4(3-8)9-6/h1-2H
InChIKey: XVIHGTRTKQZJAC-UHFFFAOYSA-N
SMILES: C1(C#N)=NC(Cl)=CC=C1[N+]([O-])=O
CAS DataBase Reference: 93683-65-9(CAS DataBase Reference)

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Safety

Hazard Codes: T
RIDADR: UN2811
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR6409
Product name: 6-Chloro-3-nitropyridine-2-carbonitrile
Purity: 98%
Packaging: 1g
Price: $21
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H55-5-X2
Product name: 6-Chloro-3-nitropyridine-2-carbonitrile
Purity: 98%
Packaging: 1g
Price: $23
Updated: 2021/12/16

AK Scientific

Product number: X8410
Product name: 6-Chloro-2-cyano-3-nitropyridine
Packaging: 1g
Price: $54
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC06230
Product name: 6-Chloro-2-cyano-3-nitropyridine
Packaging: 2g
Price: $60
Updated: 2021/12/16

ChemScene

Product number: CS-0022422
Product name: 6-Chloro-3-nitropicolinonitrile
Purity: 98.85%
Packaging: 5g
Price: $69
Updated: 2021/12/16

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6-CHLORO-2-CYANO-3-NITROPYRIDINE Chemical Properties,Usage,Production

Chemical Properties

Light yellow Cryst

Synthesis

16013-85-7

544-92-3

93683-65-9

General procedure for the preparation of 2-cyano-3-nitro-6-chloropyridine: 1. 2,6-dichloro-3-nitropyridine (5.0 g, 25.9 mmol) and cuprous(I) cyanide (2.55 g, 28.5 mmol) were mixed in N-methylpyrrolidone (19 mL). 2. the mixture was heated to 180 °C and maintained for 15 min. 3. After completion of the reaction, cooled to room temperature, the reaction mixture was poured into ice water and stirred for 10 minutes. 4. The aqueous layer was separated and the organic layer was extracted with boiling toluene followed by re-extraction with ethyl acetate. 5. The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. 6. The residue was ground with ether and filtered to give 2-cyano-3-nitro-6-chloropyridine (1.76 g, 39% yield). 1H-NMR (CDCl3, 300MHz) data: δ 7.78 (d, J = 8.9Hz, 1H), 8.54 (d, J = 8.9Hz, 1H).

References

[1] Journal of Heterocyclic Chemistry, 1984, vol. 21, # 5, p. 1521 - 1525
[2] Patent: WO2005/97805, 2005, A1. Location in patent: Page/Page column 48-49
[3] Journal of Medicinal Chemistry, 1998, vol. 41, # 23, p. 4533 - 4541

6-CHLORO-2-CYANO-3-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-CHLORO-2-CYANO-3-NITROPYRIDINE Suppliers

China 144 Germany 2 India 6 United Kingdom 6 United States 19 Global 177

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View Lastest Price from 6-CHLORO-2-CYANO-3-NITROPYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 6-CHLORO-2-CYANO-3-NITROPYRIDINE 93683-65-9
Price: US $1.10/g
Min. Order: 1g
Purity: 99.0% min
Supply Ability: 100 tons min
Release date: 2021-05-12

Career Henan Chemical Co

Product: 6-CHLORO-2-CYANO-3-NITROPYRIDINE 93683-65-9
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-11

93683-65-9, 6-CHLORO-2-CYANO-3-NITROPYRIDINERelated Search:

2-Chloro-3-cyanopyridine 2-chloro-5-cyanopyridine 4-CHLORO-PYRIDINE-2-CARBONITRILE 2,3,6-Trichloropyridine 2-Chloro-3-nitropyridine 5-CHLORO-2-CYANO-3-NITROPYRIDINE,5-CHLORO-2-CYANO-3-NITROPYRIDINE 98+% 3-Amino-6-chloro-2-picoline 3-Amino-6-chloropyridine-2-carbonitrile 2-Methyl-3-nitropyridine hydrochloride 6-Chloro-2-methyl-3-nitropyridine 2-Chloro-6-cyanopyridine 3-Amino-2-pyridinecarbonitrile 6-CHLORO-2-CYANO-3-NITROPYRIDINE 2-Cyano-3-nitropyridine

6-CHLORO-2-CYANO-3-NITROPYRIDINE

6-CHLORO-3-NITROPYRIDINE-2-CARBONITRILE

6-Chloro-2-cyano-3-nitropyidine

6-Chloro-3-nitropicolinonitrile

6-chloro-3-nitro-2-pyridinecarbonitrile

C90144

6-Chloro-2-cyano-3-nitropyridine, 6-Chloro-3-nitropicolinonitrile

6-Chloro-3-nitro-2-cyanopyridine≥ 97.0% (HPLC)

2-Pyridinecarbonitrile, 6-chloro-3-nitro-

6-CHLORO-2-CYANO-3-NITROPYRIDINE ISO 9001：2015 REACH

2-cyano-6-chloro-3-nitropyridine

6-CHLORO-2-CYANO-3-NITROPYRIDIN

93683-65-9

Pyridine series

Halides

Pyridines

pyridine