4-IODO-3-NITROANISOLE
- Product Name
- 4-IODO-3-NITROANISOLE
- CAS No.
- 58755-70-7
- Chemical Name
- 4-IODO-3-NITROANISOLE
- Synonyms
- NSC 158572;3-Nitro-4-iodoanisol;3-Nitro-4-Iodoanisole;4-IODO-3-NITROANISOLE;4-Iodo-3-nitrianisole;4-IODO-3-NITROANISOLE, 98+%;1-IODO-4-METHOXY-2-NITROBENZENE;4-Iodo-3-nitrophenyl Methyl Ether;Benzene, 1-iodo-4-Methoxy-2-nitro-;4-Iodo-3-Nitroanisole 3-Nitro-4-Iodoanisole
- CBNumber
- CB8729947
- Molecular Formula
- C7H6INO3
- Formula Weight
- 279.03
- MOL File
- 58755-70-7.mol
4-IODO-3-NITROANISOLE Property
- Melting point:
- 61-62°C
- Boiling point:
- 173 °C(Press: 0.9 Torr)
- Density
- 1.893
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- color
- Light brown to brown
- Sensitive
- Light Sensitive
- BRN
- 2365592
- CAS DataBase Reference
- 58755-70-7(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39-37
- HazardClass
- IRRITANT, LIGHT SENSITIVE
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- S544981
- Product name
- 4-IODO-3-NITROANISOLE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $185
- Updated
- 2025/07/31
- Product number
- S544981
- Product name
- 4-IODO-3-NITROANISOLE
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $179
- Updated
- 2024/03/01
- Product number
- I1136
- Product name
- 1-Iodo-4-methoxy-2-nitrobenzene
- Purity
- min. 98.0 %
- Packaging
- 5G
- Price
- $41
- Updated
- 2025/07/31
- Product number
- I1136
- Product name
- 1-Iodo-4-methoxy-2-nitrobenzene
- Purity
- min. 98.0 %
- Packaging
- 25G
- Price
- $123
- Updated
- 2025/07/31
- Product number
- I737050
- Product name
- 4-Iodo-3-nitroanisole
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
4-IODO-3-NITROANISOLE Chemical Properties,Usage,Production
Synthesis
96-96-8
58755-70-7
General procedure for the synthesis of 4-iodo-3-nitroanisole from 2-nitro-4-methoxyaniline: 11.9 mmol of 2-nitro-4-methoxyaniline was dissolved in 20 mL of concentrated sulfuric acid at a mass concentration of 71%. The temperature of the system was lowered to -5°C. 10 mL of 2 mol/L sodium nitrite solution was rapidly added to the reaction system at 0 °C and under vigorous stirring. The reaction was kept at 0°C for 10 minutes. Subsequently, the reaction mixture was poured into 5 mL of 4 mol/L sodium iodide solution at 0 °C and the reaction was continued for 30 min. Upon completion of the reaction, the solid residue was collected by filtration and washed sequentially with 6N hydrochloric acid and water. The crude product was recrystallized by hexane to give a yellow solid A.
References
[1] Patent: CN105669525, 2016, A. Location in patent: Paragraph 0072; 0073; 0082
[2] Synlett, 2016, vol. 27, # 14, p. 2095 - 2100
[3] Synlett, 2005, # 16, p. 2469 - 2472
[4] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[5] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358
4-IODO-3-NITROANISOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-IODO-3-NITROANISOLE manufacturers
- Product
- 4-IODO-3-NITROANISOLE 58755-70-7
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-04-02