ChemicalBook > CAS DataBase List > 3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID

3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID

Product Name
3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID
CAS No.
125483-00-3
Chemical Name
3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID
Synonyms
3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID;3-Amino-4-(trifluoromethyl)benzoicacid98%;Benzoic acid, 3-amino-4-(trifluoromethyl)-;3-Amino-4-(trifluoromethyl)benzoic acid 98%;Benzoic acid, 3-amino-4-(trifluoromethyl)- (9CI);3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID USP/EP/BP;5-Carboxy-2-(trifluoromethyl)aniline, 2-Amino-4-carboxybenzotrifluoride
CBNumber
CB9133668
Molecular Formula
C8H6F3NO2
Formula Weight
205.13
MOL File
125483-00-3.mol
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3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID Property

Melting point:
203-205°C
Boiling point:
325.4±42.0 °C(Predicted)
Density 
1.489
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
powder
pka
3.85±0.10(Predicted)
color 
Off white to cream
CAS DataBase Reference
125483-00-3(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
22
HazardClass 
IRRITANT
HS Code 
2922498590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
A576670
Product name
3-Amino-4-(trifluoromethyl)benzoicAcid
Packaging
100mg
Price
$75
Updated
2021/12/16
SynQuest Laboratories
Product number
4857-3-34
Product name
3-Amino-4-(trifluoromethyl)benzoic acid
Purity
98%
Packaging
5G
Price
$80
Updated
2021/12/16
Apolloscientific
Product number
PC9194
Product name
3-Amino-4-(trifluoromethyl)benzoicacid
Purity
97%
Packaging
10g
Price
$90
Updated
2021/12/16
Matrix Scientific
Product number
021433
Product name
3-Amino-4-(trifluoromethyl)benzoic acid
Purity
98%
Packaging
5g
Price
$91
Updated
2021/12/16
Matrix Scientific
Product number
021433
Product name
3-Amino-4-(trifluoromethyl)benzoic acid
Purity
98%
Packaging
25g
Price
$270
Updated
2021/12/16
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3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID Chemical Properties,Usage,Production

Synthesis

116965-16-3

125483-00-3

A. Synthesis of 3-nitro-4-trifluoromethylbenzoic acid. A mixture of 3-nitro-4-trifluoromethylbenzoic acid (19.5 g, 83 mmol) with 10% Pd/C (4 g) in EtOAc (300 mL) was placed in a pressure vessel and oscillated under an H2 atmosphere at 40 psi. The vessel was repeatedly replenished with H2 until the pressure stabilized at 40 psi. after continuing to oscillate the reaction for 10 minutes, the reaction was terminated by bubbling N2 into the mixture for 30 minutes. The resulting black mixture was filtered through diatomaceous earth and washed with MeOH. The filtrate was concentrated to give 3-amino-4-trifluoromethylbenzoic acid (19.5 g, 98%) in white solid form, which did not require further purification.HPLC analysis: retention time (Rt) = 5.46 min. mass spectrometry (ESI): calculated value of C8H6F3NO2, 205.1; measured value of m/z, 204.3 [M-H]-. 1H NMR (CD3OD): δ 7.51 (s, 1H), 7.45 (d, J = 8.2 Hz, 1H), 7.30 (d, J = 8.0 Hz, 1H), 5.02 (br s, 3H).

References

[1] Patent: US2008/200454, 2008, A1. Location in patent: Page/Page column 48
[2] Liebigs Annalen der Chemie, 1990, # 6, p. 569 - 579
[3] Patent: WO2008/59214, 2008, A1. Location in patent: Page/Page column 150
[4] Patent: WO2015/143653, 2015, A1. Location in patent: Page/Page column 60; 61
[5] Patent: WO2015/148344, 2015, A2. Location in patent: Page/Page column 108

3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID Suppliers

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View Lastest Price from 3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID manufacturers

Career Henan Chemical Co
Product
3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID 125483-00-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-12

125483-00-3, 3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACIDRelated Search:

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  • Benzoic acid, 3-amino-4-(trifluoromethyl)- (9CI)
  • 3-Amino-4-(trifluoromethyl)benzoic acid 98%
  • 3-Amino-4-(trifluoromethyl)benzoicacid98%
  • 3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID
  • 5-Carboxy-2-(trifluoromethyl)aniline, 2-Amino-4-carboxybenzotrifluoride
  • Benzoic acid, 3-amino-4-(trifluoromethyl)-
  • 3-AMINO-4-(TRIFLUOROMETHYL)BENZOIC ACID USP/EP/BP
  • 125483-00-3
  • C8H6NF3O2
  • Fluorine series
  • AMINOACID
  • Benzoic acid