1,3,5-Trifluoro-2,4,6-triiodobenzene

Product Name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
CAS No.: 84322-56-5
Chemical Name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Synonyms: 1,3,5-Trifluoro-2,4;1,3,5-Trifluoro-2,4,6-Triiodob;1,3,5-TRIFLUORO-2,4,6-TRIIODOBENZENE;1,3,5-TRILFLUORO-2,4,6-TRIIODOBENZENE;Benzene,1,3,5-trifluoro-2,4,6-triiodo-
CBNumber: CB0180452
Molecular Formula: C6F3I3
Formula Weight: 509.77
MOL File: 84322-56-5.mol

More

Less

1,3,5-Trifluoro-2,4,6-triiodobenzene Property

Melting point:: 152℃
Boiling point:: 352.4±37.0 °C(Predicted)
Density: 3.029±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: Solid
Appearance: Off-white to light brown Solid
Water Solubility: Slightly soluble in water.
Sensitive: Light Sensitive
InChI: InChI=1S/C6F3I3/c7-1-4(10)2(8)6(12)3(9)5(1)11
InChIKey: NTAZOPPTLZSXQH-UHFFFAOYSA-N
SMILES: C1(F)=C(I)C(F)=C(I)C(F)=C1I
CAS DataBase Reference: 84322-56-5(CAS DataBase Reference)

More

Less

Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2903998090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

More

Less

N-Bromosuccinimide Price

TRC

Product number: T895660
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1600-J-X0
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Packaging: 1g
Price: $15
Updated: 2021/12/16

Ark Pharm

Product number: AK-87133
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Purity: 98%
Packaging: 5g
Price: $39
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1600-J-X0
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Packaging: 5G
Price: $65
Updated: 2021/12/16

Ark Pharm

Product number: AK-87133
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Purity: 98%
Packaging: 10g
Price: $70
Updated: 2021/12/16

More

Less

1,3,5-Trifluoro-2,4,6-triiodobenzene Chemical Properties,Usage,Production

Uses

1,3,5-Trifluoro-2,4,6-triiodobenzene is useful for biological applications. Further, it is used as an intermediate in organic synthesis.

Synthesis

372-38-3

84322-56-5

The general procedure for the synthesis of 1,3,5-trifluoro-2,4,6-triiodobenzene from 1,3,5-trifluorobenzene was as follows: potassium iodide (KI, 7.14 g, 43.56 mmol) was slowly added to a stirring mixture of periodate (3.30 g, 14.50 mmol) and concentrated sulfuric acid (20 mL) at 0 °C. The resulting dark-colored mixture was cooled in an ice bath while 1,3,5-trifluorobenzene (1.0 mL, 9.68 mmol) was added dropwise over 25 min. Subsequently, the reaction mixture was heated to 70 °C and maintained at this temperature for 4 hours. After completion of the reaction, the mixture was cooled to room temperature and poured into ice water. Extraction was carried out with ether (3 x 50 mL) and the organic phases were combined. The organic phase was washed sequentially with saturated aqueous sodium bicarbonate (NaHCO3), aqueous sodium thiosulfate (Na2S2O3) and distilled water, and then dried with anhydrous sodium sulfate (Na2SO4). After evaporation to remove the solvent, the pure white powdery product 1,3,5-trifluoro-2,4,6-triiodobenzene was obtained in 80% yield. The product was characterized as follows: 19F NMR (CDCl3, 235MHz): δ-69.90ppm; melting point: 158-159°C; FT-IR (KBr pressed sheet, cm-1): 1561, 1401, 1325, 1048, 704, 652.

References

[1] Chemistry - A European Journal, 2018, vol. 24, # 56, p. 15003 - 15012
[2] European Journal of Organic Chemistry, 2002, # 23, p. 3927 - 3935
[3] Chemical Communications, 2008, # 14, p. 1635 - 1637
[4] Chemical Communications, 2017, vol. 53, # 69, p. 9590 - 9593
[5] Molecules, 2017, vol. 22, # 12,

1,3,5-Trifluoro-2,4,6-triiodobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

1,3,5-Trifluoro-2,4,6-triiodobenzene Suppliers

China 129 Europe 2 Germany 2 India 1 United Kingdom 7 United States 21 Global 162

Yantai ShengKailun Chemical Technology Co., Ltd.

Tel: 13356901049
Fax: QQ：1025383091
Email: 3119594100@qq.com
Country: China
ProdList: 7964
Advantage: 55

Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
ProdList: 30123
Advantage: 84

Beijing HwrkChemical Technology Co., Ltd

Tel: 18515581800 18501085097
Fax: 010-89508210
Email: sales.bj@hwrkchemical.com
Country: China
ProdList: 9400
Advantage: 55

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
Advantage: 66

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Nanjing Vital Chemical Co., Ltd.

Tel: Please Send Email 18652950785
Fax: 025-87193546
Email: chemweiao@163.com
Country: China
ProdList: 4378
Advantage: 65

ShangHai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847 13636370518
Fax: 021-55068248
Email: shyysw007@163.com
Country: China
ProdList: 4999
Advantage: 60

T&W GROUP

Tel: 021-61551611 13296011611
Fax: ＋86 21-50676805
Email: contact@trustwe.com
Country: China
ProdList: 9895
Advantage: 58

More

Less

View Lastest Price from 1,3,5-Trifluoro-2,4,6-triiodobenzene manufacturers

Shenzhen Nexcon Pharmatechs Ltd.

Product: 1,3,5-Trifluoro-2,4,6-triiodobenzene 84322-56-5
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 2000
Release date: 2025-04-17

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1,3,5-Trifluoro-2,4,6-triiodobenzene 84322-56-5
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 1,3,5-Trifluoro-2,4,6-triiodobenzene 84322-56-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons/month
Release date: 2020-01-08

84322-56-5, 1,3,5-Trifluoro-2,4,6-triiodobenzeneRelated Search:

1-Bromo-4-iodobenzene 4-Iodoanisole Trifluoroacetic acid (Trifluoromethoxy)benzene (Diacetoxyiodo)benzene Benzotrifluoride Trifluoromethanesulfonic acid Trifluoroacetic anhydride Chromium(VI) oxide 2,4,6-TRIFLUOROIODOBENZENE 1-Fluoro-2-iodobenzene 2,4-Difluoroiodobenzene 2,6-Difluoroiodobenzene 1,3,5-Trifluoro-2,4,6-triiodobenzene

1,3,5-Trifluoro-2,4

Benzene,1,3,5-trifluoro-2,4,6-triiodo-

1,3,5-Trifluoro-2,4,6-Triiodob

1,3,5-TRILFLUORO-2,4,6-TRIIODOBENZENE

1,3,5-TRIFLUORO-2,4,6-TRIIODOBENZENE

84322-56-5

C6F3I3