ChemicalBook > CAS DataBase List > 1,3,5-Trifluoro-2,4,6-triiodobenzene

1,3,5-Trifluoro-2,4,6-triiodobenzene

Product Name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
CAS No.: 84322-56-5
Chemical Name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Synonyms: 1,3,5-Trifluoro-2,4;1,3,5-Trifluoro-2,4,6-Triiodob;1,3,5-TRIFLUORO-2,4,6-TRIIODOBENZENE;1,3,5-TRILFLUORO-2,4,6-TRIIODOBENZENE;Benzene,1,3,5-trifluoro-2,4,6-triiodo-
CBNumber: CB0180452
Molecular Formula: C6F3I3
Formula Weight: 509.77
MOL File: 84322-56-5.mol

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1,3,5-Trifluoro-2,4,6-triiodobenzene Property

Melting point:: 152℃
Boiling point:: 352.4±37.0 °C(Predicted)
Density: 3.029±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
form: Solid
Appearance: Off-white to light brown Solid
Water Solubility: Slightly soluble in water.
Sensitive: Light Sensitive
InChI: InChI=1S/C6F3I3/c7-1-4(10)2(8)6(12)3(9)5(1)11
InChIKey: NTAZOPPTLZSXQH-UHFFFAOYSA-N
SMILES: C1(F)=C(I)C(F)=C(I)C(F)=C1I
CAS DataBase Reference: 84322-56-5(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: T895660
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1600-J-X0
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Packaging: 1g
Price: $15
Updated: 2021/12/16

Ark Pharm

Product number: AK-87133
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Purity: 98%
Packaging: 5g
Price: $39
Updated: 2021/12/16

SynQuest Laboratories

Product number: 1600-J-X0
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Packaging: 5G
Price: $65
Updated: 2021/12/16

Ark Pharm

Product number: AK-87133
Product name: 1,3,5-Trifluoro-2,4,6-triiodobenzene
Purity: 98%
Packaging: 10g
Price: $70
Updated: 2021/12/16

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1,3,5-Trifluoro-2,4,6-triiodobenzene Chemical Properties,Usage,Production

Uses

1,3,5-Trifluoro-2,4,6-triiodobenzene is useful for biological applications. Further, it is used as an intermediate in organic synthesis.

Synthesis

372-38-3

84322-56-5

The general procedure for the synthesis of 1,3,5-trifluoro-2,4,6-triiodobenzene from 1,3,5-trifluorobenzene was as follows: potassium iodide (KI, 7.14 g, 43.56 mmol) was slowly added to a stirring mixture of periodate (3.30 g, 14.50 mmol) and concentrated sulfuric acid (20 mL) at 0 °C. The resulting dark-colored mixture was cooled in an ice bath while 1,3,5-trifluorobenzene (1.0 mL, 9.68 mmol) was added dropwise over 25 min. Subsequently, the reaction mixture was heated to 70 °C and maintained at this temperature for 4 hours. After completion of the reaction, the mixture was cooled to room temperature and poured into ice water. Extraction was carried out with ether (3 x 50 mL) and the organic phases were combined. The organic phase was washed sequentially with saturated aqueous sodium bicarbonate (NaHCO3), aqueous sodium thiosulfate (Na2S2O3) and distilled water, and then dried with anhydrous sodium sulfate (Na2SO4). After evaporation to remove the solvent, the pure white powdery product 1,3,5-trifluoro-2,4,6-triiodobenzene was obtained in 80% yield. The product was characterized as follows: 19F NMR (CDCl3, 235MHz): δ-69.90ppm; melting point: 158-159°C; FT-IR (KBr pressed sheet, cm-1): 1561, 1401, 1325, 1048, 704, 652.

References

[1] Chemistry - A European Journal, 2018, vol. 24, # 56, p. 15003 - 15012
[2] European Journal of Organic Chemistry, 2002, # 23, p. 3927 - 3935
[3] Chemical Communications, 2008, # 14, p. 1635 - 1637
[4] Chemical Communications, 2017, vol. 53, # 69, p. 9590 - 9593
[5] Molecules, 2017, vol. 22, # 12,

1,3,5-Trifluoro-2,4,6-triiodobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,3,5-Trifluoro-2,4,6-triiodobenzene manufacturers

Shenzhen Nexcon Pharmatechs Ltd.

Product: 1,3,5-Trifluoro-2,4,6-triiodobenzene 84322-56-5
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 2000
Release date: 2025-04-17

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1,3,5-Trifluoro-2,4,6-triiodobenzene 84322-56-5
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 1,3,5-Trifluoro-2,4,6-triiodobenzene 84322-56-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons/month
Release date: 2020-01-08

84322-56-5, 1,3,5-Trifluoro-2,4,6-triiodobenzeneRelated Search:

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84322-56-5

C6F3I3