4-CYANOPIPERIDINE HCL
Uses- Product Name
- 4-CYANOPIPERIDINE HCL
- CAS No.
- 240401-22-3
- Chemical Name
- 4-CYANOPIPERIDINE HCL
- Synonyms
- 4-CYANOPIPERIDINE HCL;4-Cyanopiperidine hydrochloride;4-CYANOPIPERIDINE HCL 240401-22-3;4-Piperidinecarbonitrile hydrochloride(1:1)
- CBNumber
- CB11494104
- Molecular Formula
- C6H11ClN2
- Formula Weight
- 146.62
- MOL File
- 240401-22-3.mol
4-CYANOPIPERIDINE HCL Property
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Solid
- CAS DataBase Reference
- 240401-22-3
Safety
- RIDADR
- UN2811
- HazardClass
- 6.1
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- P482510
- Product name
- Piperidine-4-carbonitrileHydrochloride
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FC153608
- Product name
- 4-Cyanopiperidine HCl
- Packaging
- 2g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- 8198BB
- Product name
- Piperidine-4-carbonitrilehydrochloride
- Packaging
- 1g
- Price
- $76
- Updated
- 2021/12/16
- Product number
- OR904481
- Product name
- Piperidine-4-carbonitrilehydrochloride
- Purity
- 95+%
- Packaging
- 25g
- Price
- $101
- Updated
- 2021/12/16
- Product number
- 3H37-5-19
- Product name
- Piperidine-4-carbonitrilehydrochloride
- Packaging
- 25g
- Price
- $111
- Updated
- 2021/12/16
4-CYANOPIPERIDINE HCL Chemical Properties,Usage,Production
Uses
Piperidine-4-carbonitrile hydrochloride is a useful research chemical.
Synthesis
39546-32-2
240401-22-3
The general procedure for the synthesis of 4-cyanopiperidine hydrochloride from piperidine-4-carboxamide: 11.9 g (75.7 mmol, 99% purity) of dibutylcarboxamide was slowly added to 10 g (75.7 mmol, 97% purity) of piperidine-4-carboxamide dissolved in 50 ml of toluene in a suspension over a period of 5 min at 20 °C. After 5 min, the reaction was started at 20 °C. After 5 min, 18.91 g (158.9 mmol) of thionyl chloride was added dropwise at 20 °C. The dropwise addition took 45 min, during which the reaction temperature was kept constant at 20 °C. The reaction temperature was kept constant at 20 °C. After the dropwise addition, the reaction mixture was stirred at 20 °C for 18 hours. After completion of the reaction, the suspension was filtered and the filter cake was washed with toluene. After drying, 9.63 g of colorless solid product was obtained. The purity of 4-cyanopiperidine hydrochloride was measured to be 99.7% (w/w) by GC analysis of the sample after methanosilylation, and the theoretical yield calculated from this was 86.5%.
References
[1] Patent: WO2016/113277, 2016, A1. Location in patent: Paragraph 8
4-CYANOPIPERIDINE HCL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-CYANOPIPERIDINE HCL manufacturers
- Product
- 4-CYANOPIPERIDINE HCL 240401-22-3
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-17
- Product
- 4-CYANOPIPERIDINE HCL 240401-22-3
- Price
- US $30.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2023-09-12
- Product
- 4-CYANOPIPERIDINE HCL 240401-22-3
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 95%-99%
- Supply Ability
- as request
- Release date
- 2018-12-23