ChemicalBook > CAS DataBase List > 4-CYANOPIPERIDINE HCL

4-CYANOPIPERIDINE HCL

Uses

Product Name: 4-CYANOPIPERIDINE HCL
CAS No.: 240401-22-3
Chemical Name: 4-CYANOPIPERIDINE HCL
Synonyms: 4-CYANOPIPERIDINE HCL;4-Cyanopiperidine hydrochloride;4-CYANOPIPERIDINE HCL 240401-22-3;4-Piperidinecarbonitrile hydrochloride(1:1)
CBNumber: CB11494104
Molecular Formula: C6H11ClN2
Formula Weight: 146.62
MOL File: 240401-22-3.mol

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4-CYANOPIPERIDINE HCL Property

storage temp.: Inert atmosphere,Room Temperature
Appearance: White to off-white Solid
CAS DataBase Reference: 240401-22-3

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Safety

RIDADR: UN2811
HazardClass: 6.1
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: P482510
Product name: Piperidine-4-carbonitrileHydrochloride
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC153608
Product name: 4-Cyanopiperidine HCl
Packaging: 2g
Price: $70
Updated: 2021/12/16

AK Scientific

Product number: 8198BB
Product name: Piperidine-4-carbonitrilehydrochloride
Packaging: 1g
Price: $76
Updated: 2021/12/16

Apolloscientific

Product number: OR904481
Product name: Piperidine-4-carbonitrilehydrochloride
Purity: 95+%
Packaging: 25g
Price: $101
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H37-5-19
Product name: Piperidine-4-carbonitrilehydrochloride
Packaging: 25g
Price: $111
Updated: 2021/12/16

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4-CYANOPIPERIDINE HCL Chemical Properties,Usage,Production

Uses

Piperidine-4-carbonitrile hydrochloride is a useful research chemical.

Synthesis

39546-32-2

240401-22-3

The general procedure for the synthesis of 4-cyanopiperidine hydrochloride from piperidine-4-carboxamide: 11.9 g (75.7 mmol, 99% purity) of dibutylcarboxamide was slowly added to 10 g (75.7 mmol, 97% purity) of piperidine-4-carboxamide dissolved in 50 ml of toluene in a suspension over a period of 5 min at 20 °C. After 5 min, the reaction was started at 20 °C. After 5 min, 18.91 g (158.9 mmol) of thionyl chloride was added dropwise at 20 °C. The dropwise addition took 45 min, during which the reaction temperature was kept constant at 20 °C. The reaction temperature was kept constant at 20 °C. After the dropwise addition, the reaction mixture was stirred at 20 °C for 18 hours. After completion of the reaction, the suspension was filtered and the filter cake was washed with toluene. After drying, 9.63 g of colorless solid product was obtained. The purity of 4-cyanopiperidine hydrochloride was measured to be 99.7% (w/w) by GC analysis of the sample after methanosilylation, and the theoretical yield calculated from this was 86.5%.

References

[1] Patent: WO2016/113277, 2016, A1. Location in patent: Paragraph 8

4-CYANOPIPERIDINE HCL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-CYANOPIPERIDINE HCL manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 4-CYANOPIPERIDINE HCL 240401-22-3
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-17

Anhui Ruihan Technology Co., Ltd

Product: 4-CYANOPIPERIDINE HCL 240401-22-3
Price: US $30.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2023-09-12

Career Henan Chemical Co

Product: 4-CYANOPIPERIDINE HCL 240401-22-3
Price: US $1.00/kg
Min. Order: 1kg
Purity: 95%-99%
Supply Ability: as request
Release date: 2018-12-23

240401-22-3, 4-CYANOPIPERIDINE HCLRelated Search:

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4-CYANOPIPERIDINE HCL

4-Cyanopiperidine hydrochloride

4-Piperidinecarbonitrile hydrochloride(1:1)

4-CYANOPIPERIDINE HCL 240401-22-3

240401-22-3