ChemicalBook > CAS DataBase List > 4-Amino-N-methylbenzamide

4-Amino-N-methylbenzamide

Product Name
4-Amino-N-methylbenzamide
CAS No.
6274-22-2
Chemical Name
4-Amino-N-methylbenzamide
Synonyms
4-(Methylc;4-Amino-N<;4-Amino-N-methylbenz;4-Amino-N-methylbenzamide;4-Aminobenzoylmethylamide;4-(Methylcarbamoyl)aniline;Benzamide, 4-amino-N-methyl-;4-Amino-N-methylbenzamide >4-Amino-N-methylbenzamide 98%;4-Amino-N-methylbenzamide
CBNumber
CB21054022
Molecular Formula
C8H10N2O
Formula Weight
150.18
MOL File
6274-22-2.mol
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4-Amino-N-methylbenzamide Property

Melting point:
181 °C
Boiling point:
364.1±25.0 °C(Predicted)
Density 
1.137
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
15.84±0.46(Predicted)
color 
White to Light yellow to Light orange
CAS DataBase Reference
6274-22-2(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
HS Code 
29242990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
A2064
Product name
4-Amino-N-methylbenzamide
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$16
Updated
2025/07/31
TCI Chemical
Product number
A2064
Product name
4-Amino-N-methylbenzamide
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$23
Updated
2025/07/31
TRC
Product number
M328590
Product name
N-Methyl4-Aminobenzamide
Packaging
1g
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA113860
Product name
4-Amino-N-methylbenzamide
Packaging
500mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA113860
Product name
4-Amino-N-methylbenzamide
Packaging
1g
Price
$170
Updated
2021/12/16
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4-Amino-N-methylbenzamide Chemical Properties,Usage,Production

Synthesis

Ammonium chloride (29.6 g, 55.4 mmol) in water (200 mL) and methanol (200 mL) was added to a solution of N-methyl-4-nitro-benzamide (10 g, 55.4 mmol) in THF (160 mL). Zinc powder (29 g, 44.4 mmol) was added portion wise and the mixture stirred for 15 minutes. The reaction mixture was filtered over celite, the filtrate was then concentrated and extracted with ethyl acetate. The organics were washed with brine solution, dried over Na2SO4 and concentrated to afford 7.2 g (86percent) of 4-Amino-N-methylbenzamide. 1H NMR: (DMSO-d6): δ 7.9 (s, 1H), 7.6 (d, 2H), 6.5 (d, 2H), 5.6 (s, 2H), 2.7 (s, 3H).

References

[1] Patent: US2009/239848, 2009, A1. Location in patent: Page/Page column 24
[2] Patent: WO2010/133672, 2010, A1. Location in patent: Page/Page column 30
[3] Journal of Chemical Research, 2006, # 4, p. 223 - 224
[4] Journal of Medicinal Chemistry, 1984, vol. 27, # 6, p. 779 - 782
[5] Journal of the American Chemical Society, 1938, vol. 60, p. 1081

4-Amino-N-methylbenzamide Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-Amino-N-methylbenzamide manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
4-Amino-N-methylbenzamide 6274-22-2
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-22
Hebei Yanxi Chemical Co., Ltd.
Product
4-Amino-N-methylbenzamide 6274-22-2
Price
US $0.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
20tons
Release date
2023-10-12
Career Henan Chemical Co
Product
4-Amino-N-methylbenzamide 6274-22-2
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
as request
Release date
2018-12-24

6274-22-2, 4-Amino-N-methylbenzamideRelated Search:

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